RESUMO
The novel assingment of 13C and 1HNMR data for cadina-4,10(15)-dien-3-one obtained from Hyptis verticillata is presented. The study revealed that cadina-4,10(15)-dien-3-one possesses chemosterilant activities against the economically important cattle tick, Boophilus microplus, and toxic action against adult Cylas formicarius the most destructive pest of sweet potato (I pomoea sp.) (AU)
Assuntos
21003 , Feminino , Masculino , Besouros , Inseticidas , Naftalenos/química , Carrapatos , Isótopos de Carbono , Bovinos , Hidrogênio , Estrutura Molecular , Naftalenos/isolamento & purificação , Naftalenos/toxicidade , Espectroscopia de Ressonância Magnética , PlantasRESUMO
A procedure for detection and measurement of Hypoglycin A in biological material is described, based on reaction of the amino acid with 1-dimethylaminonaphthalene-5-sulphonyl chloride (Dansyl chloride). The desired flourescent derivative can be separated from others by paper chromatography and measured by flourimetry after elution. Less than 0.2 microgram of hypoglycin A is detectable on chromatograms (AU)