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Direct Csp3-H methylenation of 2-arylacetamides using DMF/Me2NH-BH3 as the methylene source.

Org Biomol Chem; 17(25): 6153-6157, 2019 Jun 26.
Artigo em Inglês | MEDLINE | ID: mdl-31169277
A direct Csp3-H methylenation of 2-arylacetamides using DMF/Me2NH-BH3 as the methylene source was developed. The formyl group of DMF delivered the carbon and one hydrogen atoms, and the Me2NH-BH3 donated the remaining one hydrogen atom. This protocol offers a new alternative to make useful 2-arylacrylamides from simple starting materials.