Your browser doesn't support javascript.
loading
Mostrar: 20 | 50 | 100
Resultados 1 - 20 de 205
Filtrar
Mais filtros

País/Região como assunto
Tipo de documento
Intervalo de ano de publicação
1.
Philos Trans A Math Phys Eng Sci ; 382(2277): 20230297, 2024 Aug 23.
Artigo em Inglês | MEDLINE | ID: mdl-39005016

RESUMO

We investigate a physical characterization of the gradient flow structure of variational fracture models for brittle materials: a Griffith-type fracture model and an irreversible fracture phase field model. We derive the Griffith-type fracture model by assuming that the fracture energy in Griffith's theory is an increasing function of the crack tip velocity. Such a velocity dependence of the fracture energy is typically observed in polymers. We also prove an energy dissipation identity of the Griffith-type fracture model, in other words, its gradient flow structure. On the other hand, the irreversible fracture phase field model is derived as a unidirectional gradient flow of a regularized total energy. We have considered the time relaxation parameter a mathematical approximation parameter, which we should choose as small as possible. In this research, however, we reveal the physical origin of the gradient flow structure of the fracture phase field model (F-PFM) and show that the small time relaxation parameter is characterized as the rate of velocity dependence of the fracture energy. It is verified by comparing the energy dissipation properties of those two models and by analysing a travelling wave solution of the irreversible F-PFM. This article is part of the theme issue 'Non-smooth variational problems with applications in mechanics'.

2.
Proc Natl Acad Sci U S A ; 118(23)2021 06 08.
Artigo em Inglês | MEDLINE | ID: mdl-34083445

RESUMO

Data-driven approaches promise to usher in a new phase of development in fracture mechanics, but very little is currently known about how data-driven knowledge extraction and transfer can be accomplished in this field. As in many other fields, data scarcity presents a major challenge for knowledge extraction, and knowledge transfer among different fracture problems remains largely unexplored. Here, a data-driven framework for knowledge extraction with rigorous metrics for accuracy assessments is proposed and demonstrated through a nontrivial linear elastic fracture mechanics problem encountered in small-scale toughness measurements. It is shown that a tailored active learning method enables accurate knowledge extraction even in a data-limited regime. The viability of knowledge transfer is demonstrated through mining the hidden connection between the selected three-dimensional benchmark problem and a well-established auxiliary two-dimensional problem. The combination of data-driven knowledge extraction and transfer is expected to have transformative impact in this field over the coming decades.

3.
Philos Trans A Math Phys Eng Sci ; 381(2260): 20220386, 2023 Nov 13.
Artigo em Inglês | MEDLINE | ID: mdl-37742712

RESUMO

Additive manufacturing (AM) has attracted many attentions because of its design freedom and rapid manufacturing; however, it is still limited in actual application due to the existing defects. In particular, various defect features have been proved to affect the fatigue performance of components and lead to fatigue scatter. In order to properly assess the influences of these defect features, a defect driven physics-informed neural network (PiNN) is developed. By embedding the critical defects information into loss functions, the defect driven PiNN is enhanced to capture physical information during training progress. The results of fatigue life prediction for different AM materials show that the proposed PiNN effectively improves the generalization ability under small samples condition. Compared with the fracture mechanics-based PiNN, the proposed PiNN provides physically consistent and higher accuracy without depending on the choice of fracture mechanics-based model. Moreover, this work provides a scalable framework being able to integrate more prior knowledge into the proposed PiNN. This article is part of the theme issue 'Physics-informed machine learning and its structural integrity applications (Part 1)'.

4.
Proc Natl Acad Sci U S A ; 117(31): 18178-18185, 2020 08 04.
Artigo em Inglês | MEDLINE | ID: mdl-32680966

RESUMO

Plato envisioned Earth's building blocks as cubes, a shape rarely found in nature. The solar system is littered, however, with distorted polyhedra-shards of rock and ice produced by ubiquitous fragmentation. We apply the theory of convex mosaics to show that the average geometry of natural two-dimensional (2D) fragments, from mud cracks to Earth's tectonic plates, has two attractors: "Platonic" quadrangles and "Voronoi" hexagons. In three dimensions (3D), the Platonic attractor is dominant: Remarkably, the average shape of natural rock fragments is cuboid. When viewed through the lens of convex mosaics, natural fragments are indeed geometric shadows of Plato's forms. Simulations show that generic binary breakup drives all mosaics toward the Platonic attractor, explaining the ubiquity of cuboid averages. Deviations from binary fracture produce more exotic patterns that are genetically linked to the formative stress field. We compute the universal pattern generator establishing this link, for 2D and 3D fragmentation.

5.
Sensors (Basel) ; 23(11)2023 May 25.
Artigo em Inglês | MEDLINE | ID: mdl-37299793

RESUMO

The fatigue cracking of orthotropic steel bridge decks (OSDs) is a difficult problem that hinders the development of steel structures. The most important reasons for the occurrence of fatigue cracking are steadily growing traffic loads and unavoidable truck overloading. Stochastic traffic loading leads to the random propagation behavior of fatigue cracks, which increases the difficulty of the fatigue life evaluations of OSDs. This study developed a computational framework for the fatigue crack propagation of OSDs under stochastic traffic loads based on traffic data and finite element methods. Stochastic traffic load models were established based on site-specific, weigh-in-motion measurements to simulate fatigue stress spectra of welded joints. The influence of the transverse loading positions of the wheel tracks on the stress intensity factor of the crack tip was investigated. The random propagation paths of the crack under stochastic traffic loads were evaluated. Both ascending and descending load spectra were considered in the traffic loading pattern. The numerical results indicated that the maximum value of KI was 568.18 (MPa·mm1/2) under the most critical transversal condition of the wheel load. However, the maximum value decreased by 66.4% under the condition of transversal moving by 450 mm. In addition, the propagation angle of the crack tip increased from 0.24° to 0.34°-an increase ratio of 42%. Under the three stochastic load spectra and the simulated wheel loading distributions, the crack propagation range was almost limited to within 10 mm. The migration effect was the most obvious under the descending load spectrum. The research results of this study can provide theoretical and technical support for the fatigue and fatigue reliability evaluation of existing steel bridge decks.


Assuntos
Fadiga , Reprodução , Humanos , Reprodutibilidade dos Testes , Movimento (Física) , Aço
6.
Exp Mech ; 63(7): 1255-1270, 2023.
Artigo em Inglês | MEDLINE | ID: mdl-37780097

RESUMO

Background: Obtaining accurate displacement measurements for large material deformation and/or rotation presents a distinct challenge to digital image correlation (DIC) due to cumulative and decorrelation errors, particularly near material boundaries. Objective: We aim to accurately measure the deformation gradient tensor near boundary discontinuities in situations of large deformation and large deformation gradients. Methods: To achieve this goal, the locations of randomly distributed particles are tracked using an open-source particle-tracking software, Trackpy. A least-squares estimate of the deformation gradient tensor field uses nearest-neighbor material vectors and a first-order Finite Difference (FD) approximation, circumventing common errors in other methods. The error caused by FD approximation and that incurred by measurement are derived and tested with exhaustive numerical simulations. Furthermore, a uniaxial tensile test and mode-I fracture experiment are conducted with particle-embedded hydrogels to validate the method. Results: Numerical results corroborate a theoretical expression of measurement error. They show that the FD error increases while the measurement error decreases for a growing estimating radius. Moreover, measurement error is linearly correlated to displacement noise. A benchmark uniaxial tensile test validates the accuracy of the proposed estimator, and the near-crack-tip measurements in a tensile fracture experiment demonstrate the estimator's capabilities near a free surface, when a material undergoes large deformation and rotation. The results of the displacement and strain data are benchmarked against kinematic data obtained using an open-source DIC software, Ncorr. Computation time for both methods is compared. Conclusions: A deformation gradient tensor estimator is developed based on a particle tracking technique and a least squares routine. Theoretical error bounds on the estimator are verified by numerical simulations, and the method's capability is confirmed by physical experiments in evaluating large deformation and rotation near a free boundary. The proposed estimator is expected to open a door towards future material tests and experimental mechanics studies, especially in large deformation and large rotation scenarios.

7.
J Exp Bot ; 73(4): 1204-1221, 2022 02 24.
Artigo em Inglês | MEDLINE | ID: mdl-34849736

RESUMO

The European mistletoe (Viscum album) is an epiphytic hemiparasite that attaches to its host by an endophytic system. Two aspects are essential for its survival: the structural integrity of the host-parasite interface must be maintained during host growth and the functional integrity of the interface must be maintained during ontogeny and under mechanical stress. We investigated the mechanical properties of the mistletoe-host interaction. Intact and sliced mistletoe-host samples, with host wood as reference, were subjected to tensile tests up to failure. We quantified the rough fractured surface by digital microscopy and analysed local surface strains by digital image correlation. Tensile strength and deformation energy were independent of mistletoe age but exhibited markedly lower values than host wood samples. Cracks initiated at sites with a major strain of about 30%, especially along the mistletoe-host interface. The risk of sudden failure was counteracted by various sinkers and a lignification gradient that smooths the differences in the mechanical properties between the two species. Our results improve the understanding of the key mechanical characteristics of the host-mistletoe interface and show that the mechanical connection between the mistletoe and its host is age-independent. Thus, functional and structural integrity is ensured over the lifetime of the mistletoe.


Assuntos
Viscum album , Fenômenos Biomecânicos , Interações Hospedeiro-Parasita , Viscum album/química , Madeira
8.
Sensors (Basel) ; 22(4)2022 Feb 17.
Artigo em Inglês | MEDLINE | ID: mdl-35214480

RESUMO

Fatigue of steel bridges is a major concern for bridge engineers. Previous fatigue-based weight-limiting method of steel bridges is founded on the Palmgren-Miner's rule and S-N curves, which overlook the effect of existing cracks on the fatigue life of in-service steel bridges. In the present study, based on the theory of linear elastic fracture mechanics, a framework combining the artificial neural networks and Monte Carlo simulations is proposed to analyze the fatigue reliability of steel bridges with the effects of cracks and truck weight limits considered. Using the framework, a new method of setting the gross vehicle weight limit for in-service steel bridges with cracks is proposed. The influences of four key parameters, including the average daily truck traffic, the gross vehicle weight limit, the violation rate, and the detected crack size, on the fatigue reliability of a steel bridge are analyzed quantitatively with the new framework. Results show that the suggested framework can enhance the fatigue reliability assessment process in terms of accuracy and efficiency. The method of setting gross vehicle weight limits can effectively control the fatigue failure probability to be within 2.3% according to the desired remaining service time and the detected crack size.

9.
Sensors (Basel) ; 22(18)2022 Sep 07.
Artigo em Inglês | MEDLINE | ID: mdl-36146126

RESUMO

Orthotropic steel decks (OSDs) are inevitably subjected to fatigue damage caused by cycled vehicle loads in long-span bridges. This study establishes a probabilistic analysis framework integrating the dynamic Bayesian network (DBN) and fracture mechanics to model the fatigue crack propagation considering mutual correlations among multiple fatigue details. Both the observations of fatigue crack length from field inspection and monitoring data of vehicle loads from the weight-in-motion (WIM) system are utilized. First, fracture mechanics-based uncertainty analysis is performed to determine the multiple uncertainty sources in the Paris crack propagation model, material property, and observation data of crack length. The uncertainty of monitoring data of vehicle loads is ignored because of its high accuracy; consequently, the vehicle-load-related uncertainty is spontaneously ignored, which is also demonstrated to be very small on the investigated actual bridges. Second, a hierarchical DBN model is introduced to construct mutual dependencies among various uncertainties and intra-correlations in the propagation process of multiple fatigue cracks at different components. Third, a stochastic traffic model is established based on the WIM monitoring data and multi-scale finite element analysis via substructure techniques to determine the probability distribution of vehicle-load-related parameters. After variable discretization, a refined exact inference algorithm in a forward-backward-forward manner is adopted to estimate the posterior distribution of equivalent initial crack length and update the established DBN model. Finally, the proposed method is demonstrated by a numerical case study and a typical application on an actual cable-stayed bridge with steel box girders using OSDs in China. The results show that the probability distribution of equivalent initial crack size can be spontaneously derived with a larger mean value than the results of conventional empirical analysis. Furthermore, the component-level fatigue reliability is tracked and predicted based on the established crack propagation model.

10.
Small ; 17(51): e2102739, 2021 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-34643318

RESUMO

Grain boundaries (GBs) play a central role in the fracture of polycrystals. However, the complexity of GBs and the difficulty in monitoring the atomic structure evolution during fracture greatly limit the understanding of the GB mechanics. Here, in situ aberration-corrected scanning transmission electron microscopy and density functional theory calculations are combined to investigate the fracture mechanics in low-symmetry, polycrystalline, 2D rhenium disulfide (ReS2 ), unveiling the distinctive crack behaviors at different GBs with atomic resolution. Brittle intergranular fracture prefers to rip through the GBs that are parallel to the Re chains of at least one side of the GBs. In contrast, those GBs, which do not align with Re chains on either side of the GBs, are highly resistant to fracture, impeding or deflecting the crack propagation. These results disclose the GB type-dependent mechanical failure of anisotropic 2D polycrystals, providing new ideas for material reinforcement and controllable cutting via GB engineering.

11.
Philos Trans A Math Phys Eng Sci ; 379(2203): 20210021, 2021 Aug 09.
Artigo em Inglês | MEDLINE | ID: mdl-34148411

RESUMO

The phase field paradigm, in combination with a suitable variational structure, has opened a path for using Griffith's energy balance to predict the fracture of solids. These so-called phase field fracture methods have gained significant popularity over the past decade, and are now part of commercial finite element packages and engineering fitness- for-service assessments. Crack paths can be predicted, in arbitrary geometries and dimensions, based on a global energy minimization-without the need for ad hoc criteria. In this work, we review the fundamentals of phase field fracture methods and examine their capabilities in delivering predictions in agreement with the classical fracture mechanics theory pioneered by Griffith. The two most widely used phase field fracture models are implemented in the context of the finite element method, and several paradigmatic boundary value problems are addressed to gain insight into their predictive abilities across all cracking stages; both the initiation of growth and stable crack propagation are investigated. In addition, we examine the effectiveness of phase field models with an internal material length scale in capturing size effects and the transition flaw size concept. Our results show that phase field fracture methods satisfactorily approximate classical fracture mechanics predictions and can also reconcile stress and toughness criteria for fracture. The accuracy of the approximation is however dependent on modelling and constitutive choices; we provide a rationale for these differences and identify suitable approaches for delivering phase field fracture predictions that are in good agreement with well-established fracture mechanics paradigms. This article is part of a discussion meeting issue 'A cracking approach to inventing new tough materials: fracture stranger than friction'.

12.
Philos Trans A Math Phys Eng Sci ; 379(2196): 20200129, 2021 May 03.
Artigo em Inglês | MEDLINE | ID: mdl-33715418

RESUMO

Propagation of a slip transient on a fault with rate- and state-dependent friction resembles a fracture whose near tip region is characterized by large departure of the slip velocity and fault strength from the steady-state sliding. We develop a near tip solution to describe this unsteady dynamics, and obtain the fracture energy Gc, dissipated in overcoming strength-excursion away from steady state, as a function of the rupture velocity vr. This opens a possibility to model slip transients on rate-and-state faults as singular cracks characterized by approximately steady-state frictional resistance in the fracture bulk, and by a stress singularity with the intensity defined in terms of Gc(vr) at the crack tip. In pursuing this route, we develop and use an analytical equation of motion to study 1-D slip driven by a combination of uniform background stress and a localized perturbation of the fault strength with the net Coulomb force ΔT. In the context of fluid injection, ΔT is a proxy for the injection volume Vinj. We then show that, for ongoing fluid injection, the propagation speed of a transient induced on a frictionally stable fault is bounded by a large-time limiting value proportional to the injection rate dVinj/dt, while, for stopped injection, the maximum slip run-out distance is proportional to [Formula: see text]. This article is part of the theme issue 'Fracture dynamics of solid materials: from particles to the globe'.

13.
Proc Natl Acad Sci U S A ; 115(50): 12698-12703, 2018 12 11.
Artigo em Inglês | MEDLINE | ID: mdl-30478055

RESUMO

The nacreous layer of mollusk shells holds design concepts that can effectively enhance the fracture resistance of lightweight brittle materials. Mineral bridges are known to increase the fracture resistance of nacre-inspired materials, but their role is difficult to quantify due to the lack of experimental systems where only this parameter is controllably varied. In this study, we fabricate tunable nacre-like composites that are used as a model to experimentally quantify the influence of the density of mineral bridges alone on the fracture properties of nacre-like architectures. The composites exhibit a brick-and-mortar architecture comprising highly aligned alumina platelets that are interconnected by titania mineral bridges and infiltrated by an epoxy organic phase. By combining experimental mechanical data with image analysis of such composite microstructures, an analytical model is put forward based on a simple balance of forces acting on an individual bridged platelet. Based on this model, we predict the flexural strength of the nacre-like composite to scale linearly with the density of mineral bridges, as long as the mineral interconnectivity is low enough to keep fracture in a platelet pullout mode. Increasing the mineral interconnectivity beyond this limit leads to platelet fracture and catastrophic failure of the composite. This structure-property correlation provides powerful quantitative guidelines for the design of lightweight brittle materials with enhanced fracture resistance. We illustrate this potential by fabricating nacre-like bulk composites with unparalleled flexural strength combined with noncatastrophic failure.

14.
Curr Osteoporos Rep ; 18(5): 568-576, 2020 10.
Artigo em Inglês | MEDLINE | ID: mdl-32740775

RESUMO

PURPOSE OF REVIEW: The goal of this review is to summarize recent advances in modeling of bone fracture using fracture mechanics-based approaches at multiple length scales spanning nano- to macroscale. RECENT FINDINGS: Despite the additional information that fracture mechanics-based models provide over strength-based ones, the application of this approach to assessing bone fracture is still somewhat limited. Macroscale fracture models of bone have demonstrated the potential of this approach in uncovering the contributions of geometry, material property variation, as well as loading mode and rate on whole bone fracture response. Cortical and cancellous microscale models of bone have advanced the understanding of individual contributions of microstructure, microarchitecture, local material properties, and material distribution on microscale fracture resistance of bone. Nano/submicroscale models have provided additional insight into the effect of specific changes in mineral, collagen, and non-collagenous proteins as well as their interaction on energy dissipation and fracture resistance at small length scales. Advanced modeling approaches based on fracture mechanics provide unique information about the underlying multiscale fracture mechanisms in bone and how these mechanisms are influenced by the structural and material constituents of bone at different length scales. Fracture mechanics-based modeling provides a powerful approach that complements experimental evaluations and advances the understanding of critical determinants of fracture risk.


Assuntos
Osso Esponjoso/fisiopatologia , Osso Cortical/fisiopatologia , Análise de Elementos Finitos , Fraturas Ósseas/fisiopatologia , Modelos Teóricos , Fenômenos Biomecânicos , Humanos , Modelos Biológicos
15.
Proc Natl Acad Sci U S A ; 114(22): E4344-E4353, 2017 05 30.
Artigo em Inglês | MEDLINE | ID: mdl-28507143

RESUMO

For adhering to three-dimensional (3D) surfaces or objects, current adhesion systems are limited by a fundamental trade-off between 3D surface conformability and high adhesion strength. This limitation arises from the need for a soft, mechanically compliant interface, which enables conformability to nonflat and irregularly shaped surfaces but significantly reduces the interfacial fracture strength. In this work, we overcome this trade-off with an adhesion-based soft-gripping system that exhibits enhanced fracture strength without sacrificing conformability to nonplanar 3D surfaces. Composed of a gecko-inspired elastomeric microfibrillar adhesive membrane supported by a pressure-controlled deformable gripper body, the proposed soft-gripping system controls the bonding strength by changing its internal pressure and exploiting the mechanics of interfacial equal load sharing. The soft adhesion system can use up to ∼26% of the maximum adhesion of the fibrillar membrane, which is 14× higher than the adhering membrane without load sharing. Our proposed load-sharing method suggests a paradigm for soft adhesion-based gripping and transfer-printing systems that achieves area scaling similar to that of a natural gecko footpad.

16.
Proc Natl Acad Sci U S A ; 114(49): 12900-12905, 2017 12 05.
Artigo em Inglês | MEDLINE | ID: mdl-29180402

RESUMO

Nacre, the iridescent material of the shells of pearl oysters and abalone, consists mostly of aragonite (a form of CaCO3), a brittle constituent of relatively low strength ([Formula: see text]10 MPa). Yet it has astonishing mean tensile strength ([Formula: see text]150 MPa) and fracture energy ([Formula: see text]350 to 1,240 J/m2). The reasons have recently become well understood: (i) the nanoscale thickness ([Formula: see text]300 nm) of nacre's building blocks, the aragonite lamellae (or platelets), and (ii) the imbricated, or staggered, arrangement of these lamellea, bound by biopolymer layers only [Formula: see text]25 nm thick, occupying [Formula: see text] of volume. These properties inspire manmade biomimetic materials. For engineering applications, however, the failure probability of [Formula: see text] is generally required. To guarantee it, the type of probability density function (pdf) of strength, including its tail, must be determined. This objective, not pursued previously, is hardly achievable by experiments alone, since [Formula: see text] tests of specimens would be needed. Here we outline a statistical model of strength that resembles a fishnet pulled diagonally, captures the tail of pdf of strength and, importantly, allows analytical safety assessments of nacreous materials. The analysis shows that, in terms of safety, the imbricated lamellar structure provides a major additional advantage-∼10% strength increase at tail failure probability [Formula: see text] and a 1 to 2 orders of magnitude tail probability decrease at fixed stress. Another advantage is that a high scatter of microstructure properties diminishes the strength difference between the mean and the probability tail, compared with the weakest link model. These advantages of nacre-like materials are here justified analytically and supported by millions of Monte Carlo simulations.

17.
J Res Natl Inst Stand Technol ; 125: 125010, 2020.
Artigo em Inglês | MEDLINE | ID: mdl-36474860

RESUMO

Instrumented impact testing allows the applicability of conventional Charpy tests to be extended toward assessing mechanical properties such as dynamic fracture toughness and dynamic tensile properties. In this work, we present design considerations for engineering instrumented strikers for Charpy V-notch impact testing. Specific attention is given to the mechanical and geometric features, as well as the placement of strain gauges and corresponding bridge circuits for instrumentation. These design considerations are intended to make the sensitivity invariant to the location and distribution of impact forces. The concepts presented in this work were applied to an actual instrumented striker, which was then statically calibrated. Data from this calibration indicate that the device has good repeatability, shows a linear response, and is relatively insensitive to impact location.

18.
Molecules ; 25(9)2020 Apr 30.
Artigo em Inglês | MEDLINE | ID: mdl-32365966

RESUMO

Biodegradable pectin polymers have been recommended for a variety of biomedical applications, ranging from the delivery of oral drugs to the repair of injured visceral organs. A promising approach to regulate pectin biostability is the blending of pectin films. To investigate the development of conjoined films, we examined the physical properties of high-methoxyl pectin polymer-polymer (homopolymer) interactions at the adhesive interface. Pectin polymers were tested in glass phase (10-13% w/w water content) and gel phase (38-41% w/w water content). The tensile strength of polymer-polymer adhesion was measured after variable development time and compressive force. Regardless of pretest parameters, the adhesive strength of two glass phase films was negligible. In contrast, adhesion testing of two gel phase films resulted in significant tensile adhesion strength (p < 0.01). Adhesion was also observed between glass phase and gel phase films-likely reflecting the diffusion of water from the gel phase to the glass phase films. In studies of the interaction between two gel phase films, the polymer-polymer adhesive strength increased linearly with increasing compressive force (range 10-80 N) (R2 = 0.956). In contrast, adhesive strength increased logarithmically with time (range 10-10,000 s) (R2 = 0.913); most of the adhesive strength was observed within minutes of contact. Fracture mechanics demonstrated that the adhesion of two gel phase films resulted in a conjoined film with distinctive physical properties including increased extensibility, decreased stiffness and a 30% increase in the work of cohesion relative to native polymers (p < 0.01). Scanning electron microscopy of the conjoined films demonstrated cross-grain adhesion at the interface between the adhesive homopolymers. These structural and functional data suggest that blended pectin films have emergent physical properties resulting from the cross-grain intermingling of interfacial pectin chains.


Assuntos
Biopolímeros/química , Membranas Artificiais , Pectinas/química , Água/química , Difusão , Géis , Vidro , Polissacarídeos/química
19.
J Prosthodont ; 29(1): 34-41, 2020 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-31702090

RESUMO

PURPOSE: To determine and compare the fracture toughness, flexural strength and flexural modulus of four new, commercially available CAD/CAM resin composite blocks and one new CAD/CAM lithium disilicate glass-ceramic block, tested under dry and aged conditions. MATERIALS AND METHODS: Three dispersed-fillers resin composite blocks, CERASMART, KZR-CAD-HR2, and CAMouflage NOW, one polymer-infiltrated ceramic network resin composite block, Enamic, along with Obsidian, a lithium disilicate glass-ceramic block, were characterized. Fracture toughness was determined through the notchless triangular prism specimen test, while flexural strength and flexural modulus were determined by three-point bend testing. Blocks were cut and ground to obtain (6 × 6 × 6 × 12) mm prisms and 10:1 span-to-thickness ratio bars (n = 25/group); half of the resin composite specimens were aged in 37°C distilled water for 30 days before testing. Fractured surfaces were characterized using a scanning electron microscope. Results were analyzed using Weibull statistics and two-way ANOVA, followed by Scheffé multiple means comparisons (α = 0.05). RESULTS: With regards to fracture toughness, KZR stood out among resin composites with a dry value of 1.37 MPa·m1/2 ; this was significantly affected by ageing, while the fracture toughness of the other dispersed-fillers resin composite blocks was not. Obsidian had the highest fracture toughness at 1.47 MPa·m1/2 . With regards to flexural strength, Obsidian > CERASMART = KZR > CAMouflage > Enamic. The flexural strength of the resin composites was lowered by ageing. Enamic was found to have the highest flexural modulus among the resin composites (33.02 GPa), but its value was significantly lower than that of Obsidian (76.46 GPa); flexural modulus was not affected by ageing. CONCLUSION: There was a significant difference in flexural strength between the materials, but not unanimously in flexural modulus and fracture toughness. The tested resin composite block materials had inferior flexural strength, flexural modulus and fracture toughness compared with the tested lithium disilicate glass-ceramic block (Obsidian). Enamic, the polymer infiltrated ceramic network material, had a significantly higher flexural modulus than the dispersed-fillers materials. Ageing had a deleterious impact on the flexural strength of all RCB, while its effect on the flexural modulus was insignificant. The selection of any restorative material requires a thorough analysis of its advantages and limitations to inform the clinical decision in a case-by-case approach.


Assuntos
Cerâmica , Resistência à Flexão , Resinas Compostas , Desenho Assistido por Computador , Materiais Dentários , Teste de Materiais , Propriedades de Superfície
20.
Planta ; 250(4): 1293-1305, 2019 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-31254101

RESUMO

MAIN CONCLUSION: Applying principles of shell theory, we found that grape berries rapidly change their behavior from thick-walled spheres to pressurized thin-walled spheres and become susceptible to splitting during berry softening. Knowledge of the rheological properties of the skin of berry fruits is needed to make decisions concerning berry splitting prevention. However, how these properties and splitting resistance respond to varietal differences and developmental changes is poorly understood. In a customized injection test, pressurized water was injected into the berries of four grape varieties until they split. In a compression test, the deformation of berries in response to berry softening or dehydration was measured. Shell theory was applied to estimate how the internal pressure translates to tensile stress on the skin. The results suggested that berry softening at the onset of ripening drastically alters berry rheological properties; berries rapidly changed from brittle to ductile materials. The skin became the major stress-bearing structure during berry softening and became vulnerable to tensile stress, which was associated with a rapid decline in splitting resistance. The rate of decline and the absolute extent of the skin's ability to bear stress varied by variety. Dehydration of overripe or water-stressed berries did not alter the skin properties but reduced the risk of berry splitting. These results indicate that the vulnerability to berry splitting is closely related to developmentally regulated changes in fruit rheological properties and water relations.


Assuntos
Frutas/fisiologia , Vitis/fisiologia , Desidratação , Frutas/crescimento & desenvolvimento , Reologia , Vitis/crescimento & desenvolvimento , Água/fisiologia
SELEÇÃO DE REFERÊNCIAS
DETALHE DA PESQUISA