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1.
Nano Lett ; 16(2): 1173-8, 2016 Feb 10.
Artículo en Inglés | MEDLINE | ID: mdl-26788964

RESUMEN

Transport measurements were made to study the superconducting transition of four 6 mm long niobium nanowires with different cross-sectional dimensions. A low-temperature residual resistance tail measured with an excitation current of 5 nA is found in the thinnest wire down to 50 mK or 7.7% of Tc of Nb. The functional form of the residual resistance is consistent with quantum phase slip (QPS) processes. Resistance measured at high bias excitation current switches among many discrete values that are well below the normal state resistance. These discrete resistance values as a function of temperature fall into several parallel curves all showing QPS-like decay in the low temperature limit similar to that found at low current. The coexistence of QPS-like resistance tails and resistance jumps found in the same wire unifies results from previous experiments where these two distinct sets of evidence for QPS are exclusive of each other.

2.
Nano Lett ; 15(1): 153-8, 2015 Jan 14.
Artículo en Inglés | MEDLINE | ID: mdl-25426926

RESUMEN

The ability to manipulate a single quantum object, such as a single electron or a single spin, to induce a change in a macroscopic observable lies at the heart of nanodevices of the future. We report an experiment wherein a single superconducting flux quantum, or a fluxon, can be exploited to switch the resistance of a nanowire between two discrete values. The experimental geometry consists of centimeter-long nanowires of superconducting Ga-In eutectic, with spontaneously formed Ga nanodroplets along the length of the nanowire. The nonzero resistance occurs when a Ga nanodroplet traps one or more superconducting fluxons, thereby driving a Josephson weak-link created by a second nearby Ga nanodroplet normal. The fluxons can be inserted or flipped by careful manipulation of the magnetic field or temperature to produce one of many metastable states of the system.

3.
Phys Rev Lett ; 102(24): 247003, 2009 Jun 19.
Artículo en Inglés | MEDLINE | ID: mdl-19659039

RESUMEN

We study proximity-induced superconductivity in gold nanowires as a function of the length of the nanowire, magnetic field, and excitation current. Short nanowires exhibit a sharp superconducting transition, whereas long nanowires show nonzero resistance. At intermediate lengths, however, we observe two sharp transitions; the normal and superconducting regions are separated by what we call the minigap phase. Additionally, we detect periodic oscillations in the differential magnetoresistance. We suggest that the minigap phase as well as the periodic oscillations originate from a coexistence of proximity-induced superconductivity with a normal region near the center of the wire, created either by temperature or the application of a magnetic field.

4.
Phys Rev Lett ; 102(18): 185302, 2009 May 08.
Artículo en Inglés | MEDLINE | ID: mdl-19518884

RESUMEN

We have carried out torsional oscillator and heat capacity measurements on solid 4He samples grown within a geometry which restricts the helium to thin (150 microm) cylindrical disks. In contrast with previously reported values from Rittner and Reppy of 20% nonclassical rotational inertia for similar confining dimensions, 0.9% nonclassical rotational inertia (consistent with that found in bulk samples and samples embedded in porous media) was observed in our torsional oscillator cell. In this confined geometry, the heat capacity peak is consistent with that found in bulk solid samples of high crystalline quality.

5.
Phys Rev Lett ; 102(12): 125302, 2009 Mar 27.
Artículo en Inglés | MEDLINE | ID: mdl-19392292

RESUMEN

Heat capacity measurements with significantly improved resolution find the presence of a peak in a solid 4He sample in coexistence with liquid. With improved crystallinity, the peak decreases in height and moves to lower temperature. A hysteretic heat capacity signature consistent with 3He-4He phase separation, not detected in an earlier work is clearly observed.

6.
Phys Rev Lett ; 101(16): 165303, 2008 Oct 17.
Artículo en Inglés | MEDLINE | ID: mdl-18999682

RESUMEN

X-ray diffraction experiments show that solid 4He grown in aerogel is highly polycrystalline, with an hcp crystal structure (as in bulk) and a crystallite size of approximately 100 nm. In contrast to the expectation that the highly disordered solid will have a large supersolid fraction, torsional oscillator measurements show a behavior that is strikingly similar to high purity crystals grown from the superfluid phase. The low temperature supersolid fraction is only approximately 3 x 10(-4), and the onset temperature is approximately 100 mK.

7.
Phys Rev Lett ; 100(6): 065301, 2008 Feb 15.
Artículo en Inglés | MEDLINE | ID: mdl-18352487

RESUMEN

We have investigated the influence of impurities on the possible supersolid transition in 4He by systematically enriching isotopically pure samples with 3He. The addition of 3He broadens the onset of nonclassical rotational inertia and shifts it to higher temperature, suggesting that the phenomenon is correlated with the condensation of 3He atoms onto the dislocation network in solid 4He.

8.
Science ; 319(5867): 1207-9, 2008 Feb 29.
Artículo en Inglés | MEDLINE | ID: mdl-18309075

RESUMEN

The observation of nonclassical rotational inertia (NCRI) by the torsional oscillator in 2004 gave rise to a renaissance in the study of solid helium-4. Recent theoretical and experimental studies found evidence that disorder in the solid plays a key role in enabling superfluidity. A recent experiment found a marked increase in the shear modulus that shares the same temperature and helium-3 impurity concentration dependence as that of NCRI. This correlation indicates that the onset of superfluidity requires the pinning and stiffening of the dislocation network by helium-3.

9.
Nanotechnology ; 19(36): 365704, 2008 Sep 10.
Artículo en Inglés | MEDLINE | ID: mdl-21828885

RESUMEN

We have fabricated intermetallic AuSn nanowires by electrochemical deposition in porous polycarbonate membranes. By controlling the deposition parameters, nanowires of a single intermetallic phase, namely AuSn, can be fabricated. AuSn nanowires are found to be crystalline and fairly resistant to oxidation. Electrical transport measurements on arrays of nanowires showed a superconducting transition temperature, T(c)∼1.5 K. In addition, four-probe measurements were made on individual freestanding nanowires with electrodes formed by a focused ion beam (FIB). Results from the two sets of measurements are found to be in close agreement.

10.
Nature ; 449(7165): 1025-8, 2007 Oct 25.
Artículo en Inglés | MEDLINE | ID: mdl-17960238

RESUMEN

Liquid 4He enters the superfluid state and flows without friction below 2.176 K. Thin liquid films adsorbed on solid substrates undergo the same transformation, although at a lower temperature. When the substrate is subjected to oscillatory motion a portion of the film, known as the superfluid fraction, decouples from the oscillation. A similar phenomenon has been observed in solid 4He, in which a fraction of the solid seems to decouple from the motion of the surrounding lattice. Although this observation has been replicated in various laboratories, no thermodynamic signature of the possible supersolid transition has been seen. Here we report the finding of a heat capacity peak that coincides with the onset of mass decoupling. This complementary experimental evidence supports the existence of a genuine transition between the normal solid and supersolid phases of 4He.

11.
Phys Rev Lett ; 99(13): 135302, 2007 Sep 28.
Artículo en Inglés | MEDLINE | ID: mdl-17930606

RESUMEN

It has been proposed that the observed nonclassical rotational inertia (NCRI) in solid helium results from the superflow of thin liquid films along interconnected grain boundaries within the sample. We have observed NCRI in large (4)He crystals grown at constant temperature and pressure, demonstrating that the superfluid grain boundary model cannot explain the phenomenon.

12.
Phys Rev E Stat Nonlin Soft Matter Phys ; 76(1 Pt 1): 011506, 2007 Jul.
Artículo en Inglés | MEDLINE | ID: mdl-17677449

RESUMEN

Small-angle x-ray scattering (SAXS) was used to measure the microstructure of isotopic mixtures of 3He and 4He adsorbed into silica aerogels as a function of temperature and 3He concentration. The SAXS measurements could be well described by the formation of a nearly pure film of 4He which separates from the bulk mixture onto the aerogel strands and which thickens with decreasing temperature. Previous observations of a superfluid 3He -rich phase are consistent with superfluidity existing within this film phase. Observed differences between different density aerogels are explained in terms of the depletion of 4He from the bulk mixture due to film formation.

13.
Phys Rev Lett ; 97(11): 115302, 2006 Sep 15.
Artículo en Inglés | MEDLINE | ID: mdl-17025896

RESUMEN

We have measured the pressure dependence of the supersolid fraction by a torsional oscillator technique. Superflow is found from 25.6 bar up to 136.9 bar. The supersolid fraction in the low temperature limit increases from 0.6% at 25.6 bar near the melting boundary up to a maximum of 1.5% near 55 bar before showing a monotonic decrease with pressure extrapolating to zero near 170 bar.

14.
Phys Rev Lett ; 97(7): 075301, 2006 Aug 18.
Artículo en Inglés | MEDLINE | ID: mdl-17026241

RESUMEN

We present new capacitance measurements of critical Casimir force-induced thinning of 4He films near the superfluid transition, focused on the region below Tlambda where the effect is the greatest. 4He films of 238, 285, and 340 A thickness are adsorbed on atomically smooth, N-doped silicon substrates. The Casimir force scaling function theta, deduced from the thinning of these three films, collapses onto a single universal curve, attaining a minimum theta=-1.30+/-0.03 at x=td1/nu=-9.7+/-0.8 A1/nu. The collapse confirms the finite-size scaling origin of the dip in the film thickness. Separately, we also confirm the presence down to 2.13 K of the Goldstone or surface fluctuation force, which makes the superfluid film approximately 2 A thinner than the normal film.

15.
Phys Rev Lett ; 97(24): 245301, 2006 Dec 15.
Artículo en Inglés | MEDLINE | ID: mdl-17280295

RESUMEN

A torsional oscillator study of solid para-hydrogen has been carried out down to 20 mK in a search for evidence of superfluidity. We found evidence of a possible phase transition, marked by an abrupt increase in the resonant period of oscillation and onset of extremely long relaxation times as the temperature was raised above 60 mK. In contrast to solid 4He, the change in the period for para-hydrogen is not a consequence of irrotational superflow. The long relaxation times observed suggest the effect is related to the motion of residual ortho-hydrogen molecules in the solid.

16.
Phys Rev Lett ; 95(7): 076802, 2005 Aug 12.
Artículo en Inglés | MEDLINE | ID: mdl-16196810

RESUMEN

Transport measurements were made on a system consisting of a zinc nanowire array sandwiched between two bulk superconducting electrodes (Sn or In). It was found that the superconductivity of Zn nanowires of 40 nm diameter is suppressed either completely or partially by the superconducting electrodes. When the electrodes are driven into their normal state by a magnetic field, the nanowires switch back to their superconducting state. This phenomenon is significantly weakened when one of the two superconducting electrodes is replaced by a normal metal. The phenomenon is not seen in wires with diameters equal to or thicker than 70 nm.

17.
Science ; 305(5692): 1941-4, 2004 Sep 24.
Artículo en Inglés | MEDLINE | ID: mdl-15345778

RESUMEN

We report on the observation of nonclassical rotational inertia in solid helium-4 confined to an annular channel in a sample cell under torsional motion, demonstrating superfluid behavior. The effect shows up as a drop in the resonant oscillation period as the sample cell is cooled below 230 millikelvin. Measurement of 17 solid samples allows us to map out the boundary of this superfluid-like solid or supersolid phase from the melting line up to 66 bars. This experiment indicates that superfluid behavior is found in all three phases of matter.

18.
Nature ; 427(6971): 225-7, 2004 Jan 15.
Artículo en Inglés | MEDLINE | ID: mdl-14724632

RESUMEN

When liquid (4)He is cooled below 2.176 K, it undergoes a phase transition-Bose-Einstein condensation-and becomes a superfluid with zero viscosity. Once in such a state, it can flow without dissipation even through pores of atomic dimensions. Although it is intuitive to associate superflow only with the liquid phase, it has been proposed theoretically that superflow can also occur in the solid phase of (4)He. Owing to quantum mechanical fluctuations, delocalized vacancies and defects are expected to be present in crystalline solid (4)He, even in the limit of zero temperature. These zero-point vacancies can in principle allow the appearance of superfluidity in the solid. However, in spite of many attempts, such a 'supersolid' phase has yet to be observed in bulk solid (4)He. Here we report torsional oscillator measurements on solid helium confined in a porous medium, a configuration that is likely to be more heavily populated with vacancies than bulk helium. We find an abrupt drop in the rotational inertia of the confined solid below a certain critical temperature. The most likely interpretation of the inertia drop is entry into the supersolid phase. If confirmed, our results show that all three states of matter-gas, liquid and solid-can undergo Bose-Einstein condensation.

19.
Phys Rev E Stat Nonlin Soft Matter Phys ; 68(5 Pt 2): 056111, 2003 Nov.
Artículo en Inglés | MEDLINE | ID: mdl-14682850

RESUMEN

A fluid's density profile near a wall is predicted to assume a universal shape near the liquid-vapor critical point, a phenomenon termed critical adsorption. This universal shape is predicted to depend on the boundary conditions of the fluid at the walls and is predicted to be a function of the ratio z/xi, where z is the distance from the wall and xi is the bulk correlation length. A body of evidence confirms the analogous phenomenon of critical adsorption in binary fluids near the critical demixing point, but in the simple liquid-vapor system the experimental situation is not as clear. For example, critical adsorption of SF6 was observed in porous glass for reduced temperature t=T/T(c)-1>10(-3). However, for t<10(-3) a desorption behavior is seen. This desorption has so far resisted rigorous theoretical explanation. We report measurements of the critical adsorption of nitrogen inside a capacitor gap with a simple parallel plate geometry and open gap of 3 microm. Unlike the previous experiments with SF6, the data show a monotonic increase in the adsorption between t=5 x 10(-4) and t=10(-6), consistent with theoretical prediction and without any indication of desorption.

20.
Phys Rev Lett ; 91(23): 235301, 2003 Dec 05.
Artículo en Inglés | MEDLINE | ID: mdl-14683190

RESUMEN

We have studied the influence of the substrate on superfluidity in thin 4He films. The inert coverage, the amount of nonsuperfluid 4He localized by the substrate, is found to scale with the well depth of the 4He-substrate interaction potential for six different substrates. Although the inert coverages for these substrates differ by more than a factor of 4, the phase boundary in the temperature-coverage plane is found to have a universal shape.

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