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1.
Acta Crystallogr Sect E Struct Rep Online ; 70(Pt 9): o928-9, 2014 Sep 01.
Artículo en Inglés | MEDLINE | ID: mdl-25309259

RESUMEN

In the title compound, C13H12N2OS, the planes of the thio-phene and phenyl rings are nearly perpendicular to each other, making a dihedral angle of 86.42 (12)°. In the crystal, mol-ecules are linked by C-H⋯O hydrogen bonds, forming a helical chain along the b-axis direction.

2.
Acta Crystallogr Sect E Struct Rep Online ; 70(Pt 3): o286, 2014 Mar 01.
Artículo en Inglés | MEDLINE | ID: mdl-24764995

RESUMEN

In the title compound, C14H11FO2, the dihedral angles beteen the central C3O ketone residue and the fluoro- and hy-droxy-substituted benzene rings are 50.44 (9) and 12.63 (10)°, respectively. The planes of the benzene rings subtend a dihedral angle of 58.88 (9)° and an intra-molecular O-H⋯O hydrogen bond closes an S(6) ring. No directional inter-actions beyond van der Waals packing contacts were identified in the crystal structure.

3.
Acta Crystallogr Sect E Struct Rep Online ; 70(Pt 1): o76, 2014 Jan 01.
Artículo en Inglés | MEDLINE | ID: mdl-24527008

RESUMEN

In the title compound, C14H11FO2, the two benzene rings are not coplanar, with a dihedral angle of 57.45 (12)° between their planes. In the crystal, mol-ecules are linked by an O-H⋯O hydrogen bond, forming a 21 helical chain along the b axis.

4.
Artículo en Inglés | MEDLINE | ID: mdl-24098234

RESUMEN

In the title compound, C14H12O2, the benzene rings make a dihedral angle of 58.84 (12)°. In the crystal, mol-ecules are linked into chains along the b-axis direction by O-H⋯O hydrogen bonds. These chains are further linked by C-H⋯O hydrogen bonds, forming layers parallel to the bc plane.

5.
Acta Crystallogr Sect E Struct Rep Online ; 69(Pt 11): o1676, 2013 Oct 19.
Artículo en Inglés | MEDLINE | ID: mdl-24454109

RESUMEN

In the mol-ecule of the title compound, C15H14O2, the dihedral angle between the benzene and phenyl rings is 61.27 (8)°. In the crystal, O-H⋯O and weak C-H⋯O hydrogen bonds link the mol-ecules into chains extending along the c-axis direction.

6.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 10): o2972, 2012 Oct 01.
Artículo en Inglés | MEDLINE | ID: mdl-23125752

RESUMEN

In the title compound, C(12)H(11)N(3)OS, the dihedral angle between the pyridine and thio-phene rings is 46.70 (9)° and the C-N-N-C torsion angle is 178.61 (15)°. In the crystal, inversion dimers linked by pairs of N-H⋯O hydrogen bonds generate R(2) (2)(8) loops.

7.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 11): o3135, 2012 Nov 01.
Artículo en Inglés | MEDLINE | ID: mdl-23284457

RESUMEN

In the title compound, C(9)H(7)NO, the benzene ring forms a dihedral angle of 3.98 (12)° with the pyrrole ring. In the crystal, N-H⋯O hydrogen bonds links the mol-ecules into chains which run parallel to [02-1].

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