Characterization of aluminum nitride thin films by ion beam analysis techniques.

AlN thin films have been deposited on silicon substrate by vacuum arc discharge technique at different substrate temperatures. The information regarding depth profiling of AlN thin films has been determined by applying both elastic backscattering (EBS) and nuclear reaction analysis (NRA) techniques simultaneously at optimized experimental conditions. Additionally, combined SEM/EDX techniques have been employed to gain further information regarding thickness and composition of the AlN thin films. The Al/N ratio has been determined, while the oxygen content was found to be negligible. The substrate temperature influence on depth profile of AlN thin films as well as densities has been discussed. The advantages of using ion beam analysis techniques have been reviewed.

Elemental characterization of freeze dried domestic animals' milk using ion beam analysis techniques.

Particle induced X-ray emission (PIXE) and particle induced γ-ray emission (PIGE) techniques were employed to perform elemental analysis in four milk samples of local domestic animals, namely sheep, caw, camel and goat. Additionally, Rutherford backscattering (RBS) spectra were acquired simultaneously with PIXE and PIGE to determine matrix elements. Milk samples were prepared in a simple dried base following freeze drying process. Optimization of PIXE/PIGE/RBS experimental conditions as well as data acquisition and analysis procedures were carefully addressed. Verification study was performed relying on the analysis of both IAEA-11 and IAEA-153 reference materials. Accuracies of ±5-10% together with relative standard deviations of less than 15% were mostly reported. Chemical element concentrations of 11 elements were determined, namely Na, Mg, P, S, Cl, K, Ca, Zn, Br, Rb and Sr. Obtained element concentration values were mostly in the range 1000-10000 µg/g for major elements and 5-100 µg/g for trace elements. No significant changes in elemental concentration differences for both trace and major elements were noticed in the four different milk samples. The contribution of the elements in these milk samples to the dietary recommended intakes (DRI) has been evaluated. Advantages of applying multiple ion beam analysis techniques have been discussed.

Software for standard-based analysis of thick target PIGE data.

Software, "SyrPIGE", has been developed to perform particle induced γ-ray emission (PIGE) data analysis of thick targets relying on a standard-based method. It allows self-consistent and direct analysis of PIGE data considering easy calibration of PIGE spectra, on-screen identification of every γ-ray line, manual input or evaluation of E12 values for every element at established γ-ray energies, direct generation of stopping power data based on built-in electronic stopping power calculations for protons, ability to compare results with standards and batch mode analysis capability. The software was tested on standards and showed reliable and consistent results, with PIGE data analysis performed in a very short time compared with time-consuming traditional analysis.

Surgical removal of a dislocated lower third molar from the condyle region: case report.

INTRODUCTION: Migration of dislocated lower third molar into the condylar region is quite rare. Attention should be taken to avoid condyle fracture. METHODS: 49-year-old patient had an ectopic lower left third molal in the condylar region, suffered from a submandibular and masseter space abscess. Removal of the molar via intraoral approach was chosen avoiding facial nerve branches and unnecessary scar formation. Coronoid process is removed, the tooth is separated and removed. The defect is filled with iliac cancellous bone. The coronoid process was fixed as a cover with a resorbable plate and screws (BIONX). RESULTS: Removal via intraoral approach is possible. Hypesthesia existed postoperatively, became normal later. CONCLUSION: Annual observation is strongly recommended. Intraoral approach is superior to the extraoral approach. Removal of the coronoid process minimizes the masticator forces. Separation of the tooth is essential. Filling the defect with cancellous bone accelerates the healing.