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1.
Materials (Basel) ; 16(8)2023 Apr 21.
Artigo em Inglês | MEDLINE | ID: mdl-37110109

RESUMO

This study sought to evaluate the efficacy of SWEEPS in the removal of epoxy-resin-based and calcium-silicate-containing endodontic sealer combined with single-cone and carrier-based obturation techniques through a micro-CT analysis. Seventy-six single-rooted extracted human teeth with single root canal were instrumented with Reciproc instruments. Specimens were randomly divided into four groups (n = 19) according to the root canal filling material and obturation technique: (1) AH Plus sealer + Reciproc gutta-percha, (2) TotalFill BC sealer + TotalFill BC Points, (3) AH Plus sealer + Guttafusion obturator, and (4) MTA Fillapex + Guttafusion obturator. All specimens were re-treated one week later using Reciproc instruments. Following re-treatment, root canals were additionally irrigated using the Auto SWEEPS modality. The differences in the root canal filling remnants were analyzed by micro-CT scanning of each tooth after root canal obturation, after re-treatment, and after additional SWEEPS treatment. Statistical analysis was performed using an analysis of variance (p < 0.05). The additional treatment with SWEEPS significantly reduced the volume of the root canal filling materials in all experimental groups compared to the removal of root canal filling using only reciprocating instruments (p < 0.05). However, the root canal filling was not removed completely from any of the samples. SWEEPS can be used to enhance the removal of both epoxy-resin-based and calcium-silicate-containing sealers, in combination with single-cone and carrier-based obturation techniques.

2.
Materials (Basel) ; 14(21)2021 Nov 05.
Artigo em Inglês | MEDLINE | ID: mdl-34772195

RESUMO

The objective of this study was to evaluate the efficacy of reciprocating instruments in the removal of bioceramic and epoxy resin-based sealers using micro-CT analysis. Root canals of 40 extracted human teeth were instrumented with a size R25 Reciproc instrument. Specimens were randomly divided into two groups (n = 20) according to the root canal filling material. In the first group, root canals were obturated with AH Plus sealer and Reciproc R25 gutta-percha. In the second group, a combination of bioceramic gutta-percha (TotalFill BC) and bioceramic sealer (TotalFill BC) was used. After one week, the retreatment of all specimens was performed using Reciproc instruments. To analyze the differences in the filling remnants, specimens were scanned in a micro-CT device after obturation and after the retreatment procedure. Statistical analysis was performed using the Mann-Whitney U test (p < 0.05). A combination of bioceramic sealer and bioceramic gutta-percha was more effectively removed from canals using a reciprocating instrument, with a filling remnants volume of 4.01 ± 3.13 mm3, in comparison to the combination of epoxy resin-based sealer and gutta-percha (6.96 ± 2.70 mm3) (p < 0.05). A reciprocating instrument was more effective in removing bioceramic sealers than epoxy resin-based sealers, although none of the root canal filling materials were completely removed from the root canals.

3.
Iran Endod J ; 15(1): 6-11, 2020.
Artigo em Inglês | MEDLINE | ID: mdl-36704321

RESUMO

Introduction: Forces formed during root canal instrumentation could cause the crack formation in dentinal walls. Their propagation may result in vertical root fracture and eventually tooth loss. The aim of the study was to explore microcrack formation after root canal preparation with Self-adjusting File (SAF), Reciproc Blue (RB), and ProTaper Next (PTN) instruments on young premolars by means of micro-computed tomography (micro CT). Methods and Materials: Forty-five upper premolars with two canals, were extracted due to orthodontic reasons from patients aged 16 to 20 years and stored for up to two months. The teeth were scanned with a micro-CT (Nikon XT H 225, Tring, UK) at structural resolution of 20.2 µm and randomly divided into three groups: SAF, RB, and PTN. Specimens were instrumented and irrigation was performed with 12 mL of 2.5% sodium hypochlorite (NaOCl) and 4 mL of 17% ethylenediaminetetraacetic acid (EDTA) per root canal. Subsequently, the specimens were scanned under the same conditions as before, in wet condition and 24 h after drying. The presence of microcracks in dentinal walls was evaluated using the image-processing software Volume Graphics VGStudio Max 3. Results: No dentinal defect was found in any evaluated specimen, neither in pre-nor post-operative scans in wet and dry condition. Conclusion: Under the circumstances of this in vitro study instruments with improved design and metallurgy do not cause dentinal microcracks in young premolar teeth.

4.
Acta Stomatol Croat ; 54(4): 339-352, 2020 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-33642598

RESUMO

OBJECTIVES: To examine the effect of two aging protocols on the chemical and phase composition as well as the surface state of monolithic translucent zirconia ceramics. MATERIAL AND METHODS: Translucent zirconia ceramics KATANA-Zirconia STML with different surface treatments (no treatment, K1, K2; glazed, G1-G8; polished, P1-P8) underwent testing in order to examine how the two aging protocols (three-hour hydrothermal degradation in an autoclave at 134 °C and 2 bars: G1-G4, P1-P4, and sixteen-hour chemical degradation in four-percent acetic acid at 80 °C (ISO 6872): G5-G8, P5-P8) affect chemical composition, particularly the share of stabilizing yttrium oxide (Energy Dispersive X-Ray Fluorescence - EDXRF), phase composition (X-ray diffraction - XRD) and surface state in terms of roughness and gloss. RESULTS: Aging protocols did not affect the tested chemical composition stability of specimens and a high share of stabilizing yttrium-oxide (≥10% of total content), which correlates with the absence of monoclinic phase. A decrease in gloss on all specimens is statistically significant. Chemical degradation substantially increased the surface roughness of tested specimens. CONCLUSIONS: Translucent monolithic zirconia demonstrated a stable chemical composition and resistance to tetragonal-to-monoclinic transformation. Surface gloss was significantly reduced, especially in polished specimens. Contrary to glazed specimens, the tested polished specimens manifested an increase in surface roughness. Glazing the surface of translucent monolithic zirconia produces better esthetic, tribological and hygienic effects than polishing.

5.
Acta Odontol Scand ; 73(4): 241-9, 2015 May.
Artigo em Inglês | MEDLINE | ID: mdl-25643671

RESUMO

OBJECTIVE: To analyze the effect of various fluoride formulations in commercially available agents on working properties of various nickel-titanium orthodontic wires. MATERIALS AND METHODS: Uncoated (NiTi), rhodium coated (RhNiTi) and nitrified (NNiTi) wires were immersed to dH2O, MiPaste, Elmex and Mirafluor for 1 h. Unloading slope characteristics (average force, bending action of the force and average plateau length) and the percentage of useable constant force during unloading were observed. Surface roughness (Ra) was measured. SEM and EDS were used for observation of the surface. RESULTS: NiTi had decreased loading and unloading elastic modulus (E) and yield strength (YS) after immersion to MIPaste and Mirafluor. The unloading YS decreased in the RhNiTi by the MIPaste. The loading and unloading YS of the NNiTi increased in Elmex and increased average plateau force. RhNiTi showed higher average plateau length and the percentage of useful constant force during unloading in Mirafluor and the average plateau force lowered after immersion to MIPaste. The unloading slope characteristics for NiTi were affected by all three prophylactic agents, mostly by Mirafluor, and produced significantly lower forces during both loading and unloading, similarly to the NNiTi wires. The RhNiTi had the lowest forces during both loading and unloading in MIPaste. All results were at significance; p<0.05. Difference in Ra was observed for RhNiTi after immersion to the MI Paste (p<0.001; η2=0.761). CONCLUSION: The NiTi and NNiTi wires lose less working force when combined with Elmex. The RhNiTi improve their working properties with Mirafluor and deteriorate when combined with MiPaste.


Assuntos
Cariostáticos/química , Materiais Revestidos Biocompatíveis/química , Ligas Dentárias/química , Fluoretos/química , Níquel/química , Fios Ortodônticos , Titânio/química , Varredura Diferencial de Calorimetria , Caseínas/química , Diaminas/química , Módulo de Elasticidade , Humanos , Teste de Materiais , Nitrogênio/química , Maleabilidade , Ródio/química , Fluoreto de Sódio/química , Espectrofotometria Atômica , Estresse Mecânico , Propriedades de Superfície , Temperatura , Fatores de Tempo
6.
Angle Orthod ; 84(6): 1041-8, 2014 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-24654939

RESUMO

OBJECTIVE: To analyze the effect of various coating formulations on the mechanical and corrosion properties of nickel-titanium (NiTi) orthodontic wires. MATERIALS AND METHODS: Uncoated, rhodium-coated, and nitrified NiTi wires were observed with a three-point-bend test, surface roughness (Ra) measurement, scanning electron microscopy, energy dispersive spectroscopy, and electrochemical testing (open circuit potential, electrochemical impedance spectroscopy, and cyclic polarization scan). Differences in the properties of tested wire types were analyzed with analysis of variance and Tukey post hoc test. RESULTS: Uncoated and nitrified NiTi wires showed similar mechanical and anticorrosive properties, while rhodium-coated NiTi wires showed the highest Ra and significantly higher modulus of elasticity, yield strength, and delivery of forces during loading but not in unloading. Rhodium-coated NiTi wires also had the highest corrosion current density and corrosion potential, lowest impedance modulus, and two time constants on Bode plot, one related to the Rh/Au coating and the other to underlying NiTi. CONCLUSION: Working properties of NiTi wires were unaffected by various coatings in unloading. Nitrification improved corrosion resistance. Rhodium coating reduced corrosion resistance and pronounced susceptibility to pitting corrosion in artificial saliva because of galvanic coupling between the noble coating and the base alloy.


Assuntos
Materiais Revestidos Biocompatíveis/química , Ligas Dentárias/química , Níquel/química , Fios Ortodônticos , Titânio/química , Corrosão , Espectroscopia Dielétrica , Módulo de Elasticidade , Eletrólise , Ouro/química , Humanos , Teste de Materiais , Microscopia Eletrônica de Varredura , Maleabilidade , Polarografia , Ródio/química , Saliva Artificial/química , Espectrometria por Raios X , Estresse Mecânico , Propriedades de Superfície
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