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1.
BMC Oral Health ; 24(1): 1104, 2024 Sep 17.
Artigo em Inglês | MEDLINE | ID: mdl-39289670

RESUMO

BACKGROUND: The effect of an immune-boosting beverage (SAM) containing Sambucus Nigra, an energy beverage (ENE), an in-office bleaching (BLE) agent with 25% hydrogen peroxide superior, glazing (GLA) or polishing (POL) methods, and professional dental prophylaxis (PDP) on the color of CAD-CAM restorative materials is unknown. METHODS: In total 210 specimens were prepared, consisting of CAD-CAM feldspathic (FC), zirconia-reinforced lithium disilicate ceramic (ZLS) and hybrid ceramic (HC). The ceramic specimens were divided according to the polishing methods of glazing (GLA) and mechanical polishing (POL). All materials were divided into two groups: with and without BLE. A 25% hydrogen peroxide superior (HPS) gel was used for BLE. After the baseline (BAS) measurement, the specimens were immersed in 3 different beverages (distilled water (DIS), SAM, ENE). After 28 days, a fine-grained (RDA 7) prophylaxis paste was applied. Statistical analysis of ∆E00 color difference values was performed by 3-way ANOVA and Bonferroni test (α = 0.05). RESULTS: The effect of all other actions except material-BLE-beverage on color for BAS-Day 28 was statistically different (p < 0.05). The effect of material, material-BLE, beverage on color for Day 28-PDP was statistically different (p < 0.05). After 28 days, the lowest color change was found in FC-GLA and HC immersed in DIS (p = 0.0001) and the highest in FC-POL immersed in ENE (p = 0.0002). PDP was efficient in color recovery in HC immersed to DIS, ENE and SAM (p = 0.0010). For FC, HC and ZLS, BLE caused a higher color change (p < 0.0001). Regardless of the material, the highest color change for BLE-beverage was found in BLE-treated specimens immersed in ENE (p = 0.0496) and the lowest color change was found in non-BLE-treated specimens immersed in SAM (p = 0.0074). CONCLUSIONS: In materials pre-exposed to 25% HPS, the effect of PDP on color recovery was lower than in unexposed materials. After 28 days, mechanical polishing produced higher color change in FC than glazing, however, in ZLS effects of glazing and mechanical polishing on color were similar. For material/polishing method, HC was the most effective. ENE caused higher color change than DIS and SAM. PDP was more effective than ENE in restoring color to DIS- and SAM-immersed specimens.


Assuntos
Cor , Polimento Dentário , Peróxido de Hidrogênio , Peróxido de Hidrogênio/química , Polimento Dentário/métodos , Bebidas Energéticas , Profilaxia Dentária/métodos , Clareadores Dentários , Humanos , Teste de Materiais , Restauração Dentária Permanente/métodos , Materiais Dentários/química , Clareamento Dental/métodos , Cerâmica/química
2.
Braz Oral Res ; 38: e077, 2024.
Artigo em Inglês | MEDLINE | ID: mdl-39258630

RESUMO

Borosilicate glass was developed to enhance the mechanical behavior and smoothness of dental zirconia as an alternative to conventional glaze. This study assessed the mechanical and optical properties of 3 mol% yttria-stabilized tetragonal zirconia polycrystal (3Y-TZP) coated with borosilicate glass or a commercial glaze fired for an extended period of time. Disc-shaped 3Y-TZP zirconia specimens (Zpex, Tosoh) were sintered at 1550°C for 2 hours. The specimens were divided into three groups: as-sintered (control, C); commercial glaze (G); and borosilicate glass (SL). The glaze and borosilicate glass were applied over the zirconia and fired for 20 minutes at 950°C and 1200°C, respectively. Biaxial flexural strength, fractography, X-ray diffraction (XRD), roughness (Ra and Rz), fracture toughness (Vickers indentation method), color difference (∆E00), and translucency (TP00) analyses were conducted. The t-test or the one-way ANOVA and Tukey's tests were used to analyze the data (α = 0.05). Flexural strength data were subjected to the Weibull analysis. The SL group exhibited the highest flexural strength (1025.8 MPa), whereas the C (859.41 MPa) and G (816.0 MPa) groups exhibited similar values. The SL group also had the highest characteristic strength. The fracture origin in all groups was on the zirconia surface. XRD analysis revealed that the specimens from the SL group contained tetragonal, cubic, and monoclinic phases. The SL group presented the lowest surface roughness. Fracture toughness in the SL group was lower than in the C group, but similar to that observed in the G group. The translucency and color differences observed in the G and SL groups were similar. Borosilicate glass enhanced the flexural strength of 3Y-TZP, promoted the smoothest surface, and exhibited optical properties similar to those of the glaze.


Assuntos
Vidro , Teste de Materiais , Propriedades de Superfície , Difração de Raios X , Ítrio , Zircônio , Zircônio/química , Ítrio/química , Vidro/química , Análise de Variância , Fatores de Tempo , Resistência à Flexão , Silicatos/química , Reprodutibilidade dos Testes , Valores de Referência , Estatísticas não Paramétricas , Cor , Fenômenos Ópticos , Testes de Dureza , Materiais Dentários/química
3.
BMC Oral Health ; 24(1): 1089, 2024 Sep 14.
Artigo em Inglês | MEDLINE | ID: mdl-39277736

RESUMO

BACKGROUND: To predict the long-term performance of restorative materials in the oral environment, it is important to evaluate their resistance to chemical and mechanical degradation and to know the toxic potential of the type and amount of ions eluted from the filling material. In this study, home bleaching was applied to dental materials with different contents and it was aimed to determine the type and amount of ions released from these materials. METHODS: In this study, amalgam, posterior composite resin, anterior composite resin, bulk fill composite resin, indirect composite resin, hybrid ceramic and all-ceramic were used as restorative materials. 10 specimens of each material were prepared according to the manufacturer's instructions. Each material group was divided into two subgroups as the bleached group and the control group. After bleaching, all specimens were stored in 1 ml of 75% ethanol/water solution. Solutions were renewed after 1, 14 and 28 days. The type and amount of ions released from the materials were determined using Inductively Coupled Plasma-Mass Spectrometer (ICP-MS). Data were analyzed using the Friedman, Wilcoxon Signed Ranks, and Mann-Whitney U tests (α = 0.05). RESULTS: It was determined that the amount of ions release from the restorative materials decreased over time (p < 0.05). According to the results of the Mann-Whitney U test, there was no difference between the bleaching and control groups in most of the restorative materials (p > 0.05). CONCLUSION: Within the limits of this study, home bleaching system does not have a significant effect on ion release from restorative materials.


Assuntos
Peróxido de Carbamida , Resinas Compostas , Amálgama Dentário , Materiais Dentários , Restauração Dentária Permanente , Teste de Materiais , Peróxidos , Clareadores Dentários , Ureia , Peróxido de Carbamida/farmacologia , Peróxidos/química , Resinas Compostas/química , Clareadores Dentários/química , Amálgama Dentário/química , Ureia/análogos & derivados , Ureia/química , Restauração Dentária Permanente/métodos , Materiais Dentários/química , Íons , Cerâmica/química , Humanos , Fatores de Tempo
4.
Clin Exp Dent Res ; 10(5): e930, 2024 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-39295290

RESUMO

OBJECTIVE: The demand for esthetics has increased in today's world and most parents prefer to preserve their children's primary anterior teeth until their natural exfoliation. However, an intracanal post is required to provide retention for reconstruction of severely damaged anterior teeth due to caries or trauma. Various materials and methods may be used for the fabrication of intracanal posts. This study assessed the fracture strength and fracture mode of primary canine teeth reconstructed with prefabricated and customized polyethylene and glass fiber posts. MATERIALS AND METHODS: This in vitro study evaluated 60 extracted primary canine teeth in four groups (n = 15). After pulpectomy and post space preparation with 4 mm depth, composite resin post, prefabricated glass fiber post (Whitepost), customized glass fiber post (Interlig), or customized polyethylene fiber post (Ribbond) were placed in the root canals to provide retention, and the tooth crown was restored with bulk-fill composite resin. The fracture strength was then measured in a universal testing machine. The fracture mode was also evaluated visually. RESULTS: The mean fracture strength was 22.45 ± 5.06, 33.10 ± 8.5, 30.20 ± 7.33, and 32.61 ± 5.73 N/mm2 in the composite resin post, Whitepost, Interlig, and Ribbond groups, respectively. The fracture strength was significantly lower in the composite group than in the remaining three groups (p = 0.000). No other significant differences were found (p > 0.05). Also, no significant difference was observed among the study groups in the fracture mode (p = 0.241). CONCLUSION: The composite resin post yielded a significantly lower fracture strength than the prefabricated and customized glass and polyethylene fiber posts, but the fracture mode was not significantly different among the four groups.


Assuntos
Resinas Compostas , Dente Canino , Análise do Estresse Dentário , Vidro , Técnica para Retentor Intrarradicular , Fraturas dos Dentes , Dente Decíduo , Resinas Compostas/química , Fraturas dos Dentes/prevenção & controle , Vidro/química , Técnica para Retentor Intrarradicular/instrumentação , Humanos , Técnicas In Vitro , Planejamento de Prótese Dentária , Teste de Materiais , Materiais Dentários/química , Polietileno/química , Pulpectomia/métodos , Pulpectomia/instrumentação , Polietilenos
5.
Int J Nanomedicine ; 19: 9255-9271, 2024.
Artigo em Inglês | MEDLINE | ID: mdl-39282577

RESUMO

Background: Polymeric denture materials can be susceptible to colonization by oral microorganisms. Zein-coated magnesium oxide nanoparticles (zMgO NPs) demonstrate antimicrobial activity. The aim of this study was to investigate the antimicrobial effect and adherence of different oral microorganisms on hybrid polymeric denture materials incorporated with zMgO NPs. Methods: Five types of polymeric denture materials were used. A total of 480 disc-shaped specimens were divided by material type (n=96/grp), then subdivided by zMgO NPs concentration: control with no nanoparticles and other groups with zMgO NPs concentrations of 0.3%, 0.5% and 1% by weight. Characterization of the polymeric denture materials incorporating zMgO NPs was done, and the antimicrobial activity of all groups was tested against four types of microorganisms: 1) Streptococcus mutans, 2) Staphylococcus aureus, 3) Enterococcus faecalis and 4) Candida albicans. The samples underwent an adherence test and an agar diffusion test. Experiments were done in triplicates. Results: The characterization of the hybrid samples revealed variation in the molecular composition, as well as a uniform distribution of the zMgO NPs in the polymeric denture materials. All hybrid polymeric denture materials groups induced a statistically significant antimicrobial activity, while the control groups showed the least antimicrobial activity. The agar diffusion test revealed no release of the zMgO NPs from the hybrid samples, indicating the NPs did not seep out of the matrix. Conclusion: The zMgO NPs were effective in reducing the adherence of the tested microorganisms and enhancing the antimicrobial activity of the polymeric denture materials. This antimicrobial effect with the polymeric dentures could aid in resisting microbial issues such as denture stomatitis.


Assuntos
Anti-Infecciosos , Candida albicans , Staphylococcus aureus , Streptococcus mutans , Zeína , Zeína/química , Zeína/farmacologia , Candida albicans/efeitos dos fármacos , Streptococcus mutans/efeitos dos fármacos , Staphylococcus aureus/efeitos dos fármacos , Anti-Infecciosos/farmacologia , Anti-Infecciosos/química , Óxido de Magnésio/química , Óxido de Magnésio/farmacologia , Nanopartículas/química , Enterococcus faecalis/efeitos dos fármacos , Testes de Sensibilidade Microbiana , Humanos , Materiais Dentários/farmacologia , Materiais Dentários/química , Dentaduras/microbiologia , Polímeros/química , Polímeros/farmacologia
6.
J Adhes Dent ; 26: 185-200, 2024 Sep 17.
Artigo em Inglês | MEDLINE | ID: mdl-39286910

RESUMO

PURPOSE: This German S3 clinical practice guideline offers evidence-based recommendations for the use of composite materials in direct restorations of permanent teeth. Outcomes considered were the survival rates and restoration quality and process quality of the manufacturing process. Part 1 of this two-part presentation deals with the indication classes. MATERIALS AND METHODS: A systematic literature search was conducted by two methodologists using MEDLINE and the Cochrane Library via the OVID platform, including studies up to December 2021. Six PICO questions were developed to guide the search. Recommendations were formulated by a panel of dental professionals from 20 national societies and organizations based on the collected evidence. RESULTS: Composite materials are a viable option for the direct restoration of cavity Classes I-V and may also be used for restorations with cusp replacement, and tooth shape corrections. In the posterior region, direct composite restorations should be preferred over indirect composite inlays. For Class V restorations, composite materials can be used if adequate contamination control and adhesive technique are ensured. CONCLUSION: The guideline is the first to provide comprehensive evidence on the use of direct composite materials. However, further long-term clinical studies with comparators such as (modified) glass-ionomer cements are necessary. Regular updates will detail the future scope and limitations of direct composite restorations.


Assuntos
Resinas Compostas , Restauração Dentária Permanente , Odontologia Baseada em Evidências , Humanos , Restauração Dentária Permanente/métodos , Dentição Permanente , Materiais Dentários
7.
J Indian Soc Pedod Prev Dent ; 42(3): 240-248, 2024 Jul 01.
Artigo em Inglês | MEDLINE | ID: mdl-39250209

RESUMO

INTRODUCTION: Caries in primary teeth rapidly advances owing to its thin structure, thereby requiring restoration. However, restorations often fail due to various causes such as secondary caries and reduced microtensile bond strength (µTBS), which calls for the use of antimicrobial agents such as silver diamine fluoride (SDF). AIM: This study aims to measure and analyse the effect of SDF application on the µTBS of three regularly used restorative materials to dentin of primary teeth as well as compare the types of bond failure interfaces under SEM. MATERIALS AND METHODS: The study comprised 60 samples equally divided into six groups among three restorative materials, namely, glass ionomer cement (GIC, Groups I and II), resin-modified glass ionomer cement (RMGIC, Groups III and IV), and composite resin (Groups V and VI) with subdivisions of A and B, where A represented samples with SDF application and B represented samples without SDF application. RESULTS AND OBSERVATIONS: It was observed that µTBS of RMGIC to sound and carious dentin irrespective of SDF application was found to be statistically significant (P < 0.05), and when GIC, RMGIC, and composite resins were compared to both sound and carious dentin irrespective of SDF application, it was statistically significant (P < 0.05). SEM analysis revealed predominantly cohesive failures among all the groups. CONCLUSION: Based on the results, it was concluded that SDF has no adverse effect on the µTBS of GIC, RMGIC, and composite resin to both carious and sound dentin of primary teeth.


Assuntos
Resinas Compostas , Colagem Dentária , Fluoretos Tópicos , Cimentos de Ionômeros de Vidro , Compostos de Amônio Quaternário , Compostos de Prata , Resistência à Tração , Dente Decíduo , Humanos , Fluoretos Tópicos/farmacologia , Resinas Compostas/química , Cimentos de Ionômeros de Vidro/farmacologia , Compostos de Amônio Quaternário/farmacologia , Compostos de Amônio Quaternário/química , Colagem Dentária/métodos , Microscopia Eletrônica de Varredura , Dentina/efeitos dos fármacos , Teste de Materiais , Restauração Dentária Permanente/métodos , Cárie Dentária , Materiais Dentários/química
8.
Br Dent J ; 237(5): 313, 2024 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-39271864
9.
Br Dent J ; 237(5): 400-406, 2024 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-39271876

RESUMO

This clinical paper provides an in-depth exploration of advanced techniques for bonding orthodontic attachments under special circumstances. Challenges arise when bonding brackets to non-enamel surfaces, such as dental restorations, and in conditions such as amelogenesis imperfecta, which affect enamel integrity. Distinct approaches required for bonding to different restorative materials, including glassy ceramics, zirconia, resin composites and metals, are outlined. Moreover, we describe strategies to manage bonding in conditions including amelogenesis imperfecta, hypodontia and microdontia in a multidisciplinary context.


Assuntos
Colagem Dentária , Braquetes Ortodônticos , Humanos , Colagem Dentária/métodos , Amelogênese Imperfeita/terapia , Anodontia/terapia , Resinas Compostas , Materiais Dentários
10.
BMC Oral Health ; 24(1): 1081, 2024 Sep 13.
Artigo em Inglês | MEDLINE | ID: mdl-39272090

RESUMO

BACKGROUND: Decreased salivary flow can make the patients uncomfortable with their complete dentures and affects the retention of the dentures. Milling and 3D printing have become an alternative to conventional denture construction techniques. The goal of this study was to evaluate the effect of conventional and digital techniques of the complete denture construction on the denture surface wettability with distilled water and saliva substitute before and after thermocycling. METHODS: A total of 30 specimens were utilized in the present study. Specimens were divided according to the construction techniques into 3 groups (n = 10 each). Group I: Heat-polymerized polymethylmethacrylate (PMMA) group, group II: Milled group, and group III: 3-dimensional (3D)-printed group. All the specimens were subjected to 2000 cycles of thermal aging in a thermocycler. The wettability of all specimens to water and saliva substitute was measured via a contact angle goniometer (Olympus TGHM, Rame-hart Inc, USA) before and after thermocycling. Descriptive statistical analysis, plots, and the Shapiro-Wilk test were used to verify normality for each variable. One-way ANOVA was used to compare the 3 study groups, while paired samples t-test was used to compare the differences within each group (P < .05). RESULTS: The smallest contact angle of drop of water to the denture base specimens before and after thermocycling were recorded in the milled group (53.0 ± 4.77 and 50.27 ± 2.30, respectively), followed by the heat polymerized PMMA group (85.65 ± 4.71 and 65.06 ± 2.27, respectively), and the 3D-printed group (91.34 ± 6.74 and 90.86 ± 8.57, respectively). While the smallest contact angle of drop of saliva substitute to denture base specimens was recorded in the milled group (56.82 ± 2.29 and 34.85 ± 7.51, respectively), followed by the 3D-printed group (72.87 ± 4.83 and 58.14 ± 9.58, respectively) and the heat polymerized PMMA group (83.62 ± 4.12 and 67.82 ± 4.93, respectively). There was statistically significant difference between the groups (P < .05). A significant decline in the average contact angle of drop of saliva has been reported in all groups after thermocycling. The contact angle values differed significantly between saliva substitute and distilled water in both 3D-printed and milled groups after thermocycling (P < .001). CONCLUSIONS: The milled denture base material presented the best wettability to water and saliva substitute than the 3D-printed and the heat-polymerized PMMA materials. Saliva substitutes improve the wetting ability of denture base materials manufactured by CAD/CAM compared with water.


Assuntos
Bases de Dentadura , Prótese Total , Polimetil Metacrilato , Impressão Tridimensional , Molhabilidade , Polimetil Metacrilato/química , Humanos , Técnicas In Vitro , Planejamento de Dentadura , Materiais Dentários/química , Teste de Materiais , Propriedades de Superfície , Desenho Assistido por Computador , Água
11.
Med Sci Monit ; 30: e945130, 2024 Sep 10.
Artigo em Inglês | MEDLINE | ID: mdl-39252410

RESUMO

BACKGROUND This 3-dimensional (3D) optical study aimed to evaluate the effects of microwave glazing on the surface roughness of zirconia-reinforced glass. Glazed surfaces of ceramic provide a smooth and esthetically superior restoration. There are many methods of glazing. However, this study aims to evaluate the effect of microwave glazing on ceramic restorations over conventional oven and hand polishing. MATERIAL AND METHODS A sample size of 90 ceramic material tiles was derived according to the standard sample size formula. The 3 dental ceramics used were IPS e.max CAD (lithium disilicate ceramic; IvoclarVivadent), Suprinity (zirconia-reinforced lithium silicate; VITA Zahnfabrik), and Celtra Duo zirconia-reinforced lithium silicate; Dentsply Sirona). Each group was further divided equally to undergo conventional oven glazing, hand polishing, and microwave glazing. The final glazed surfaces were then evaluated for surface roughness with the Ra parameter, using a Contour GT 3D Optical Microscope (Bruker) and 3D non-contact surface metrology with interferometry. RESULTS The ANOVA test for intergroup comparison showed microwave glazing was a significantly better glazing method than conventional oven and hand polishing (P<0.05). A statistically significant difference was shown between conventional and microwave glazing; however, the difference was greater between conventionally glazed and hand-polished specimens. Furthermore, a highly significant difference between microwave-glazed and hand-polished specimens was observed. CONCLUSIONS Results showed that irrespective of the ceramic, microwave-glazed ceramics were better than traditional oven-glazed ceramics, and hand-polishing resulted in a rougher surface than glazing. Irrespective of the surface treatment methods, IPS e.max CAD ceramic showed a relatively smoother surface than did Suprinity and Celtra Duo.


Assuntos
Cerâmica , Porcelana Dentária , Micro-Ondas , Propriedades de Superfície , Zircônio , Zircônio/química , Cerâmica/química , Porcelana Dentária/química , Teste de Materiais/métodos , Humanos , Materiais Dentários/química , Vidro/química
12.
BMC Oral Health ; 24(1): 1033, 2024 Sep 03.
Artigo em Inglês | MEDLINE | ID: mdl-39227885

RESUMO

BACKGROUND: The accuracy of intraoral scanning is critical for computer-aided design/computer-aided manufacturing workflows in dentistry. However, data regarding the scanning accuracy of various adjacent restorative materials and intraoral scanners are lacking. This in vitro study aimed to evaluate the effect of adjacent restorative material type and CEREC's intraoral scanners on the accuracy of intraoral digital impressions for inlay cavities. METHODS: The artificial tooth was prepared with an occlusal cavity depth of 2 mm, a proximal box width at the gingival floor of 1.5 mm, and an equi-gingival margin extended disto-occlusally at the transition line angle on both the lingual and buccal sides for an inlay restoration. The adjacent teeth were veneered with crowns made of gold and zirconia, and an artificial tooth (resin) was utilized as the control group. The inlay cavity and adjacent teeth (Gold, Zirconia, and resin) were scanned 10 times using Chairside Economical Restoration of Esthetic Ceramics (CEREC) Primescan (PS), Omnicam (OC), and Bluecam (BC). A reference scan was obtained using a laboratory scanner (3-shape E3). Scanning was performed according to the manufacturer's instructions, including powder application for the BC group. Standard tesselation language files were analyzed using a three-dimensional analysis software program. Experimental data were analyzed using a two-way analysis of variance and the Tukey's post-hoc comparison test. RESULTS: The restorative materials of the adjacent teeth significantly affected the accuracy of the intraoral digital impressions (p < .05). The zirconia group exhibited the highest trueness deviation, followed by the resin and gold groups, with each demonstrating a statistically significant difference (p < .05). The resin group demonstrated the highest maximum positive deviation and deviation in precision. Gold exhibited the lowest average deviation value for trueness compared with those of the other adjacent restorative materials. Intraoral scanner type significantly influenced the trueness and precision of the scan data (p < .05). The average deviation of trueness according to the intraoral scanner type increased in the following order: BC > PS > OC. The average deviation in precision increased in the following order: PS>OC>BC (p < .05). CONCLUSION: The restorative materials of the adjacent tooth and the type of intraoral scanner affect the accuracy of the intraoral digital impression. The trueness of the digital images of the BC group, obtained by spraying the powder, was comparable to that of the PS group. Among the adjacent restorative materials, zirconia exhibited the lowest trueness. In contrast, PS demonstrated the highest precision among the intraoral scanners, while resin displayed the lowest precision among the adjacent restorative materials.


Assuntos
Desenho Assistido por Computador , Restaurações Intracoronárias , Zircônio , Humanos , Técnica de Moldagem Odontológica , Técnicas In Vitro , Materiais Dentários , Coroas , Cerâmica , Planejamento de Prótese Dentária/métodos , Restauração Dentária Permanente/métodos
13.
J Clin Pediatr Dent ; 48(5): 131-137, 2024 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-39275830

RESUMO

Recently, interest in tooth-colored fluoride-releasing dental materials has increased. Although physical and mechanical properties such as surface hardness, elastic modulus and surface roughness of the restorative materials have been investigated, the effect of different immersion media on these properties is still controversial. The aim of this study was to evaluate the nanohardness, elastic modulus and surface roughness of the fluoride release of tooth-colored restorative materials after immersion in acidic beverages. Prepared samples of three restorative materials (a highly viscous glass ionomer (EQUIA Forte; GC, Tokyo, Japan), a compomer (Dyract XP; Dentsply, Weybridge, UK), and a bioactive restorative material (Activa BioACTIVE; Pulpdent, MA, USA)) were randomly divided and immersed in distilled water, a cola and an orange juice for one week. The HYSITRON T1 950 TriboIndenter device (Hysitron, USA) with the Berkovich diamond indenter tip was used for all measurements. The nanohardness and elastic modulus of the samples were measured by applying a force of 6000 µN to five different points on the sample surface. Surface roughness measurements were evaluated on random samples by scanning five random 40 × 40 µm areas. The properties were measured at the initial and one week after immersion. The values of nanohardness, elastic modulus and surface roughness were tested for significant differences using a two-way analysis of variance (ANOVA) with repeated measures (p < 0.05). Tukey's honest significant difference (HSD) test was used for multiple comparisons. AB (Activa BioACTIVE) had the highest initial mean values for nanohardness. After post-immersion, the highest mean value for elastic modulus was the initial AB value. The lowest mean value for roughness of 100.36 nm was obtained for the initial DX (Dyract XP) measurement. Acidic beverages had a negative effect on the nanohardness, elastic modulus and surface roughness of the restorative materials.


Assuntos
Bebidas Gaseificadas , Módulo de Elasticidade , Fluoretos , Dureza , Teste de Materiais , Propriedades de Superfície , Fluoretos/química , Compômeros/química , Humanos , Materiais Dentários/química , Sucos de Frutas e Vegetais , Resinas Acrílicas/química , Restauração Dentária Permanente/métodos , Água/química , Cariostáticos/química , Cimentos de Ionômeros de Vidro/química , Citrus sinensis/química , Imersão , Resinas Compostas/química , Dióxido de Silício
14.
Clin Oral Investig ; 28(9): 497, 2024 Aug 23.
Artigo em Inglês | MEDLINE | ID: mdl-39177681

RESUMO

OBJECTIVES: Oral diseases, such as dental caries, periodontitis, and oral cancers, are highly prevalent worldwide. Many oral diseases are typically associated with bacterial infections or the proliferation of malignant cells, and they are usually located superficially. MATERIALS AND METHODS: Articles were retrieved from PubMed/Medline, Web of Science. All studies focusing on stimuli-responsive materials in oral diseases were included and carefully evaluated. RESULTS: Stimulus-responsive materials are innovative materials that selectively undergo structural changes and trigger drug release based on shifts at the molecular level, such as changes in pH, electric field, magnetic field, or light in the surrounding environment. These changes lead to alterations in the properties of the materials at the macro- or microscopic level. Consequently, stimuli-responsive materials are particularly suitable for treating superficial site diseases and have found extensive applications in antibacterial and anticancer therapies. These characteristics make them convenient and effective for addressing oral diseases. CONCLUSIONS: This review aimed to summarize the classification, mechanism of action, and application of stimuli-responsive materials in the treatment of oral diseases, point out the existing limitations, and speculate the prospects for clinical applications. CLINICAL RELEVANCE: Our findings may provide useful information of stimuli-responsive materials in oral diseases for dental clinicians.


Assuntos
Doenças da Boca , Humanos , Doenças da Boca/terapia , Doenças da Boca/tratamento farmacológico , Concentração de Íons de Hidrogênio , Materiais Dentários/química
15.
Clin Oral Investig ; 28(9): 473, 2024 Aug 07.
Artigo em Inglês | MEDLINE | ID: mdl-39110133

RESUMO

PURPOSE: To investigate the effects of different surface treatments and thicknesses on the color, transparency, and surface roughness of ultra-transparent zirconia. METHODS: A total of 120 Katana ultra-translucent multi-layered zirconia specimens were divided into 12 groups according to the thickness (0.3, 0.5, and 0.7 mm) and surface treatment (control, airborne particle abrasion [APA], lithium disilicate coating, and glaze on). Color difference (ΔE00) and relative translucency parameter (RTP00) were calculated using a digital spectrophotometer. The surface roughness (Ra, Rq, Sa, and Sq) was measured using a non-contact profile scanner. The surface morphologies and microstructures of the samples were observed using a tungsten filament scanning electron microscope. Statistical analyses were performed by one-way and two-way analysis of variance (ANOVA) followed by post hoc multiple comparisons and Pearson's correlation (α = 0.05). RESULTS: The results showed that the surface treatment, ceramic thickness, and their interactions had significant effects on ΔE00 and RTP00 (p < 0.001). The surface treatment significantly altered the micromorphology and increased the surface roughness of the ceramic samples. APA exhibited the lowest transparency, largest color difference, and highest surface roughness. Zirconia with 0.3 mm and 0.7 mm thicknesses showed strong negative correlations between Sa and RTP00. CONCLUSIONS: The three internal surface treatments significantly altered the surface roughness, color difference, and transparency of ultra-transparent zirconia. As the thickness increased, the influence of the inner surface treatment on the color difference and transparency of zirconia decreased. CLINICAL IMPLICATIONS: For new zirconia internal surface treatment technologies, in addition to considering the enhancement effect on the bonding properties, the potential effects on the color and translucency of high-transparency zirconia should also be considered. Appropriately increasing the thickness of zirconia restorations helps minimize the effect of surface treatment on the optical properties.


Assuntos
Cor , Teste de Materiais , Microscopia Eletrônica de Varredura , Espectrofotometria , Propriedades de Superfície , Zircônio , Zircônio/química , Porcelana Dentária/química , Materiais Dentários/química , Colagem Dentária/métodos
16.
Oper Dent ; 49(5): 597-607, 2024 Sep 01.
Artigo em Inglês | MEDLINE | ID: mdl-39169507

RESUMO

OBJECTIVE: This study aimed to evaluate the flexural properties and two-body wear resistance of nine highly filled flowable resin composites relative to those of viscous and conventional low-filled flowable composites. In addition, scanning electron microscopy (SEM) analysis of the microstructures was performed. METHODS AND MATERIALS: For each resin composite group (n=12), 12 specimen bars (25 mm × 2 mm × 2 mm) were fabricated using a silicon mold for performing flexural strength (FS), flexural modulus (E), flexural toughness (FT), Weibull modulus (m) tests, and SEM microstructural analysis. For each group, ten bars were tested using a three-point flexural test on a universal testing machine, while the other two were embedded in acrylic resin before being observed by SEM for structural analysis. During the two-body wear test with a chewing simulator, 8 specimens (12 groups, n=8) of each resin composite group were manufactured in a specific mold and subjected to 120,000 cycles of wear against a steatite ball, and the depth loss was measured. Three one-way ANOVA tests followed by Tukey's post hoc tests were conducted to compare the flexural and wear properties among the different groups. RESULTS: The majority of highly filled composites tested in this study exhibited similar flexural strengths (between 105.68 MPa and 135.49 MPa) and superior wear resistance to those of viscous composites. The flexural moduli (between 5.12 GPa and 9.62 GPa) of these composites were in between those of the viscous and low-filled composites tested in this study. CONCLUSIONS: The highly filled flowable composites tested in this study exhibited different in vitro properties but were often superior to those of viscous resin composite suggesting their possible use for posterior restorations.


Assuntos
Resinas Compostas , Resistência à Flexão , Teste de Materiais , Microscopia Eletrônica de Varredura , Resinas Compostas/química , Análise do Estresse Dentário , Propriedades de Superfície , Desgaste de Restauração Dentária , Materiais Dentários/química , Viscosidade , Módulo de Elasticidade , Humanos , Metacrilatos/química
17.
Oper Dent ; 49(5): 551-563, 2024 Sep 01.
Artigo em Inglês | MEDLINE | ID: mdl-39169509

RESUMO

PURPOSE: This study aimed to analyze the presence of defects within the adhesive interface formed with five bioactive dental materials and caries-affected dentin concerning the timing of radiotherapy (before or after the restorative procedures) by micro-CT. METHODS AND MATERIALS: A total of 96 carious human molars were randomly allocated into the following groups based on the timing of the radiotherapy sequence: radiotherapy followed by restoration (RT1) or restoration followed by radiotherapy (RT2). Then, six subgroups were established within these groups based on the type of materials used (n=8). Following cavity preparation and caries removal, a universal adhesive (G-Premio Bond) was administered in self-etch mode or accompanied by applying suitable cavity conditioners according to the manufacturers' guidelines. Subsequently, restorations were performed using five bioactive restorative materials (resin-modified glass-ionomer [Fuji II LC], high-viscosity glass-ionomer hybrid [EQUIA Forte HT], giomer [Beautifil II], alkasite [Cention N], and dual-cure bulk-fill composite [Activa Bioactive Restorative]) and a conventional microhybrid resin composite (Filtek Z250). The radiotherapy regimen encompassed 60 Grays (Gy) administered at a rate of 2 Gy/day over 6 weeks, 5 days a week. Micro-CT analysis was employed to assess adhesive defects at the interface between caries-affected dentin and the restorations. The data were analyzed using Kruskal-Wallis, Mann-Whitney U, and Dunn tests (α=0.05). RESULTS: RT2 caused significantly higher adhesive defects than RT1 for the Filtek Z250 and Activa Bioactive Restorative subgroups (p<0.05). For RT1, no significant differences were found in adhesive defects among all tested subgroups (p>0.05). By contrast, for RT2, adhesive defects were significantly higher for the Activa Bioactive Restorative and Cention N subgroups than for the EQUIA Forte HT and Beautifil II subgroups (p<0.05). CONCLUSIONS: When using most bioactive restorative materials, the timing of radiotherapy had no significant influence on the adhesive interface. Regarding restoration following a radiotherapy protocol, a favorable impact was identified with high-viscosity glass ionomer hybrid cement and giomer bioactive restorations compared with dual-cure bioactive bulk-fill composite and alkasite restorations.


Assuntos
Resinas Compostas , Cárie Dentária , Restauração Dentária Permanente , Dentina , Microtomografia por Raio-X , Humanos , Microtomografia por Raio-X/métodos , Cárie Dentária/terapia , Resinas Compostas/uso terapêutico , Restauração Dentária Permanente/métodos , Cimentos de Ionômeros de Vidro/uso terapêutico , Adesivos Dentinários/química , Colagem Dentária/métodos , Preparo da Cavidade Dentária/métodos , Cimentos de Resina/uso terapêutico , Técnicas In Vitro , Dente Molar , Materiais Dentários/uso terapêutico , Metacrilatos , Bis-Fenol A-Glicidil Metacrilato
18.
Oper Dent ; 49(5): 531-539, 2024 Sep 01.
Artigo em Inglês | MEDLINE | ID: mdl-39187958

RESUMO

Although at-home bleaching can recover the optical properties of stained CAD-CAM monolithic materials, little is known about its impact on their surface and mechanical properties, especially when successive sessions are performed. This study evaluated the effect of successive at-home bleaching sessions on the microhardness, roughness, topography, biaxial flexural strength (BFS), and reliability of CAD-CAM monolithic materials. Disks from Lava Ultimate (LU), Vita Enamic (VE), and IPS Empress CAD (EMP) were fabricated and submitted to up to three bleaching sessions. At-home bleaching was performed with 10% carbamide peroxide, and each session consisted of one application for 10 hours/day for 14 days. The analyses of the aforementioned parameters were assessed before and after the first, second, and third bleaching sessions, except for BFS, which was evaluated at baseline and after the third session. The Weibull modulus was calculated from the BFS data. The microhardness of the three materials as well as the roughness of LU were not affected by the sessions, whereas the roughness of VE and EMP increased from the second session. All materials displayed topographic changes, which became more pronounced with the increase in the number of sessions. Although bleaching decreased the BFS of the materials, it did not adversely affect their reliability. Successive at-home bleaching sessions with the protocol used in the present study cannot be considered a safe procedure for the materials evaluated.


Assuntos
Peróxido de Carbamida , Desenho Assistido por Computador , Resistência à Flexão , Teste de Materiais , Propriedades de Superfície , Clareamento Dental , Clareamento Dental/métodos , Reprodutibilidade dos Testes , Clareadores Dentários , Materiais Dentários/química , Peróxidos , Humanos , Dureza , Porcelana Dentária/química , Cerâmica
19.
Oper Dent ; 49(5): 608-616, 2024 Sep 01.
Artigo em Inglês | MEDLINE | ID: mdl-39187962

RESUMO

OBJECTIVE: To evaluate the effects of UV postcuring times on color stability (CS), surface properties (wettability [°] and surface roughness [Ra]), and conversion of 3D-printed resins for temporary restorations. METHODS: Disc-shaped specimens (10.0×3.0 mm) and maxillary central incisors (8.2×10.3 mm) were fabricated using provisional 3D-printed resin (PriZma Bio Prov [PZ] and PrintaX AA TEMP [PX]) in A2 shade and subjected to UV postcure times of 0 (T0), 5 (T1), 10 (T2), and 15 (T3) minutes (n=15). The incisors were used for CS evaluation with a colorimeter. In contrast, discs were used to measure the contact angle using the sessile drop method, surface roughness with an optical profilometer, and degree of conversion with FT-NIR. For CS, Ra, contact angle, and degree of conversion, a two-way ANOVA with Bonferroni post-hoc test (α=0.05) was used. RESULTS: PX resin demonstrated greater color stability than PZ (p=0.001). Long UV postcuring times (10 to 15 minutes) will increase the contact angle (p=0.013) and stabilize the degree of conversion (p=0.01), while 5 to 10 minutes of UV postcuring will provide better surface smoothness (p=0.04) of both resins. CONCLUSIONS: Long UV postcuring times (10 to 15 minutes) lead to greater alterations in color, contact angle, and stability of the degree of conversion, while 5 to 10 minutes lead to a smoother surface of the 3D-printed temporary resins.


Assuntos
Cor , Resinas Compostas , Impressão Tridimensional , Propriedades de Superfície , Raios Ultravioleta , Resinas Compostas/química , Restauração Dentária Temporária , Humanos , Fatores de Tempo , Teste de Materiais , Materiais Dentários/química , Molhabilidade
20.
J Clin Pediatr Dent ; 48(4): 108-114, 2024 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-39087220

RESUMO

Dental decay is a prevalent bacterial disease affecting a significant percentage of children globally. In paediatric dentistry, various materials are available for restoring deciduous teeth, addressing both functional and aesthetic concerns. However, paediatric dentists encounter challenges related to patient compliance, limited working time, and material handling. This study aims to observe the survival rate of bulk-fill composite restorations in paediatric patients over a five-year follow-up. A total of 198 patients aged 0 to 12 years underwent 673 class II restorations on deciduous first molars (1M) and second molars (2M). All restorations were conducted performed by 1 Pediatric DDS resident students from the Paediatric Dentistry Department (Padova University), utilizing using different isolation techniques. Bulk-fill composite restorations were evaluated over a five-year follow-up, and data were collected by a single investigator. After five years, 177 patients and 611 restorations were assessed. The retention rate was higher in primary second molars than in first molars, with fewer marginal dyschromies and less formation of secondary caries. The overall failure rate was higher in primary first molars and primary lower second molars. Bulk-fill composites demonstrated significantly positive performance in terms of retention, maintenance, and marginal dyschromies. Bulk-fill composites are promising materials of choice in paediatric dentistry due to their easy handling and favorable properties. Further research is necessary to compare high and low viscosity bulk-fill composites and assess the impact of different variables on restoration success.


Assuntos
Resinas Compostas , Falha de Restauração Dentária , Restauração Dentária Permanente , Dente Molar , Humanos , Restauração Dentária Permanente/métodos , Estudos Retrospectivos , Pré-Escolar , Criança , Masculino , Feminino , Lactente , Dente Decíduo , Cárie Dentária/terapia , Odontopediatria , Materiais Dentários
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