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Dynamic vapor generator that simulates transient odor emissions of victims entrapped in the voids of collapsed buildings.
Statheropoulos, M; Pallis, G C; Mikedi, K; Giannoukos, S; Agapiou, A; Pappa, A; Cole, A; Vautz, W; Thomas, C L Paul.
Afiliación
  • Statheropoulos M; School of Chemical Engineering, National Technical University of Athens, Field Analytical Chemistry and Technology Unit , 9 Iroon Polytechniou Street, Athens, 157 73, Greece.
Anal Chem ; 86(8): 3887-94, 2014 Apr 15.
Article en En | MEDLINE | ID: mdl-24697615
ABSTRACT
The design, development, and validation of a dynamic vapor generator are presented. The generator simulates human scent (odor) emissions from trapped victims in the voids of collapsed buildings. The validation of the device was carried out using a reference detector a quadrupole mass spectrometer equipped with a pulsed sampling (PS-MS) system. A series of experiments were conducted for evaluating the simulator's performance, defining types and weights of different factors, and proposing further optimization of the device. The developed device enabled the production of stable and transient odor profiles in a controllable and reproducible way (relative standard deviation, RSD < 11%) at ppbv to low ppmv concentrations and allowed emission durations up to 30 min. Moreover, the factors affecting its optimum performance (i.e., evaporation chamber temperature, air flow rate through the mixing chamber, air flow rate through the evaporation chamber, and type of compound) were evaluated through an analysis of variance (ANOVA) tool revealing the next steps toward optimizing the generator. The developed simulator, potentially, can also serve the need for calibrating and evaluating the performance of analytical devices (e.g., gas chromatographers, ion mobility spectrometers, mass spectrometers, sensors, e-noses) in the field. Furthermore, it can contribute in better training of urban search and rescue (USaR) canines.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Trabajo de Rescate / Odorantes Límite: Animals / Humans Idioma: En Revista: Anal Chem Año: 2014 Tipo del documento: Article País de afiliación: Grecia

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Trabajo de Rescate / Odorantes Límite: Animals / Humans Idioma: En Revista: Anal Chem Año: 2014 Tipo del documento: Article País de afiliación: Grecia
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