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Photocyclization of photoswitches with high enantioselectivity in human serum albumin in an artificial environment.
Kawamura, Koichi; Osawa, Ken; Watanobe, Yuta; Saeki, Yuri; Maruyama, Naoki; Yokoyama, Yasushi.
Afiliación
  • Kawamura K; Department of Advanced Materials Chemistry, Graduate School of Engineering, Yokohama National University, 79-5, Tokiwadai, Hodogaya, Yokohama 240-8501, Japan. yokoyama-yasushi-wp@ynu.ac.jp.
  • Osawa K; Department of Advanced Materials Chemistry, Graduate School of Engineering, Yokohama National University, 79-5, Tokiwadai, Hodogaya, Yokohama 240-8501, Japan. yokoyama-yasushi-wp@ynu.ac.jp.
  • Watanobe Y; Department of Advanced Materials Chemistry, Graduate School of Engineering, Yokohama National University, 79-5, Tokiwadai, Hodogaya, Yokohama 240-8501, Japan. yokoyama-yasushi-wp@ynu.ac.jp.
  • Saeki Y; Department of Advanced Materials Chemistry, Graduate School of Engineering, Yokohama National University, 79-5, Tokiwadai, Hodogaya, Yokohama 240-8501, Japan. yokoyama-yasushi-wp@ynu.ac.jp.
  • Maruyama N; Department of Advanced Materials Chemistry, Graduate School of Engineering, Yokohama National University, 79-5, Tokiwadai, Hodogaya, Yokohama 240-8501, Japan. yokoyama-yasushi-wp@ynu.ac.jp.
  • Yokoyama Y; Department of Advanced Materials Chemistry, Graduate School of Engineering, Yokohama National University, 79-5, Tokiwadai, Hodogaya, Yokohama 240-8501, Japan. yokoyama-yasushi-wp@ynu.ac.jp.
Chem Commun (Camb) ; 53(22): 3181-3184, 2017 Mar 14.
Article en En | MEDLINE | ID: mdl-28195280
ABSTRACT
Three photochromic bisthienylethenes exhibited 56 to >99% enantiomeric excess in photochemical ring closure upon UV irradiation when incorporated in human serum albumin dissolved in 15% acetonitrile-phosphate buffer solution and incubated for 24 h at -4 °C. The absolute stereochemistry of the major enantiomers of two bisthienylethenes has been determined by their chemical transformations.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Rayos Ultravioleta / Albúmina Sérica / Etilenos Límite: Humans Idioma: En Revista: Chem Commun (Camb) Asunto de la revista: QUIMICA Año: 2017 Tipo del documento: Article País de afiliación: Japón
Texto completo
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XML
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Rayos Ultravioleta / Albúmina Sérica / Etilenos Límite: Humans Idioma: En Revista: Chem Commun (Camb) Asunto de la revista: QUIMICA Año: 2017 Tipo del documento: Article País de afiliación: Japón