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Investigating the effect of polarity of stationary and mobile phases on retention of cannabinoids in normal phase liquid chromatography.
De Luca, Chiara; Buratti, Alessandro; Krauke, Yannick; Stephan, Svea; Monks, Kate; Brighenti, Virginia; Pellati, Federica; Cavazzini, Alberto; Catani, Martina; Felletti, Simona.
Afiliación
  • De Luca C; Department of Chemical, Pharmaceutical and Agricultural Sciences, University of Ferrara, via L. Borsari 46, 44121, Ferrara, Italy.
  • Buratti A; Department of Chemical, Pharmaceutical and Agricultural Sciences, University of Ferrara, via L. Borsari 46, 44121, Ferrara, Italy.
  • Krauke Y; KNAUER Wissenschaftliche Geräte GmbH, Hegauer Weg 38, 14163, Berlin, Germany.
  • Stephan S; KNAUER Wissenschaftliche Geräte GmbH, Hegauer Weg 38, 14163, Berlin, Germany.
  • Monks K; KNAUER Wissenschaftliche Geräte GmbH, Hegauer Weg 38, 14163, Berlin, Germany.
  • Brighenti V; Department of Life Sciences, University of Modena and Reggio Emilia, Via G. Campi 103, Modena, 41125, Italy.
  • Pellati F; Department of Life Sciences, University of Modena and Reggio Emilia, Via G. Campi 103, Modena, 41125, Italy.
  • Cavazzini A; Department of Chemical, Pharmaceutical and Agricultural Sciences, University of Ferrara, via L. Borsari 46, 44121, Ferrara, Italy.
  • Catani M; Department of Chemical, Pharmaceutical and Agricultural Sciences, University of Ferrara, via L. Borsari 46, 44121, Ferrara, Italy. ctnmtn@unife.it.
  • Felletti S; Department of Chemical, Pharmaceutical and Agricultural Sciences, University of Ferrara, via L. Borsari 46, 44121, Ferrara, Italy. simona.felletti@unife.it.
Anal Bioanal Chem ; 414(18): 5385-5395, 2022 Jul.
Article en En | MEDLINE | ID: mdl-35146546
ABSTRACT
This work reports about a screening of four adsorbents with different polarity employed for the separation of the main phytocannabinoids contained in Cannabis sativa L., under normal phase liquid chromatography (NPLC). The effect of polarity and type of interaction mechanisms of the adsorbents (namely Si-, CN-, Diol-, and NH2-based SPs) on retention has been investigated under a variety of conditions either by using different combinations of apolar solvents (heptane or hexane) and alcohols (ethanol or isopropanol). The columns have also been employed for the separation of a real cannabis sample. Graphical Abstract Investigating the effect of polarity of stationary and mobile phases on retention of cannabinoids in normal phase liquid chromatography.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Cannabinoides / Cannabis Idioma: En Revista: Anal Bioanal Chem Año: 2022 Tipo del documento: Article País de afiliación: Italia
Texto completo
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Imprimir
XML
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Cannabinoides / Cannabis Idioma: En Revista: Anal Bioanal Chem Año: 2022 Tipo del documento: Article País de afiliación: Italia