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Photoinduced Synthesis of Thiocyanates through Hydrogen Atom Transfer and One-Pot Derivatization to Isothiocyanates.
Maeda, Bumpei; Aihara, Yusuke; Sato, Ayato; Kinoshita, Toshinori; Murakami, Kei.
Afiliación
  • Maeda B; Department of Chemistry, School of Science, Kwansei Gakuin University, 2-1 Gakuin, Sanda, Hyogo 669-1337, Japan.
  • Aihara Y; Graduate School of Science, Nagoya University, Chikusa, Nagoya 464-8602, Japan.
  • Sato A; Institute of Transformative Bio-Molecules (WPI-ITbM) and Graduate School of Science, Nagoya University, Chikusa, Nagoya 464-8601, Japan.
  • Kinoshita T; Institute of Transformative Bio-Molecules (WPI-ITbM) and Graduate School of Science, Nagoya University, Chikusa, Nagoya 464-8601, Japan.
  • Murakami K; Department of Chemistry, School of Science, Kwansei Gakuin University, 2-1 Gakuin, Sanda, Hyogo 669-1337, Japan.
Org Lett ; 24(40): 7366-7371, 2022 10 14.
Article en En | MEDLINE | ID: mdl-36194477
ABSTRACT
Photoinduced benzylic C-H thiocyanation is described. A series of alkyl thiocyanates were efficiently obtained by using Selectfluor as the oxidant. Moreover, we accomplished the one-pot isothiocyanation following the C-H thiocyanation. The thiocyanates and isothiocyanates were applied to the divergent transformation of pharmaceuticals.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Tiocianatos / Hidrógeno Idioma: En Revista: Org Lett Asunto de la revista: BIOQUIMICA Año: 2022 Tipo del documento: Article País de afiliación: Japón
Texto completo
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XML
PubMed Links
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Tiocianatos / Hidrógeno Idioma: En Revista: Org Lett Asunto de la revista: BIOQUIMICA Año: 2022 Tipo del documento: Article País de afiliación: Japón