Portable laser-heating stand for synchrotron applications.
Rev Sci Instrum
; 80(4): 045103, 2009 Apr.
Article
em En
| MEDLINE
| ID: mdl-19405687
ABSTRACT
A compact, double-sided laser-heating system for diamond-cell synchrotron applications is described. The optical table, containing laser, spectrometer, and all optics for visual observation and measuring temperatures and pressures has an area of less than 1/2 m(2) and weighs less than 20 kg. All components can be remotely controlled at micron levels with simple dc motors and pneumatic drives. The design allows quick alignment of the laser-heated hot spot with the x-ray beam and the spectrometer. The prealigned system can be set up at most synchrotron beamlines within about 1 h. We carried out measurements on a variety of materials above one megabar and up to over 4000 K at both the x-ray diffraction beamline ID 27 and the x-ray absorption beamline ID 24 at the European Synchrotron Facility. A new measurement of the melting temperature of iron by x-ray absorption spectroscopy is presented.
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1
Coleções:
01-internacional
Base de dados:
MEDLINE
Idioma:
En
Revista:
Rev Sci Instrum
Ano de publicação:
2009
Tipo de documento:
Article
País de afiliação:
Alemanha