Effect of Solvent on the Rate of Ozonolysis: Development of a Homogeneous Flow Ozonolysis Protocol.

Arriaga, Danniel K; Kang, Seokmin; Thomas, Andy A

Arriaga, Danniel K; Kang, Seokmin; Thomas, Andy A.

Afiliação

Arriaga DK; Department of Chemistry, Texas A&M University, College Station, Texas 77842-0001, United States.
Kang S; Department of Chemistry, Texas A&M University, College Station, Texas 77842-0001, United States.
Thomas AA; Department of Chemistry, Texas A&M University, College Station, Texas 77842-0001, United States.

J Org Chem ; 88(19): 13720-13726, 2023 Oct 06.

Article em En | MEDLINE | ID: mdl-37747787

ABSTRACT

ABSTRACT

Herein, we describe the effect of organic solvents on ozone solubility and the rate of ozonolysis reactions using rapid injection NMR spectroscopy. The tabulated solubility and kinetic data allowed for the design of a homogeneous ozonolysis flow reactor capable of delivering precise quantities of dissolved ozone to various olefin substrates.

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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: J Org Chem Ano de publicação: 2023 Tipo de documento: Article País de afiliação: Estados Unidos

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