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1.
Nanotechnology ; 30(10): 105601, 2019 Mar 08.
Article in English | MEDLINE | ID: mdl-30537681

ABSTRACT

The structure, magnetic and ferroelectric properties of sputtered epitaxial CoFe2O4-BiFeO3 (CFO-BFO) nanocomposite thin films grown on La0.7Sr0.3MnO3 (LSMO) layers on (001) oriented SrTiO3 (STO) substrates and on STO-buffered Si are described. The as-grown LSMO thin films were smooth and poorly conductive but the resistivity was reduced and the surfaces roughened after annealing. Cosputtered CFO and BFO on STO formed vertically aligned nanostructures consisting of epitaxial spinel CFO pillars within a perovskite BFO matrix, but the rough surface of the annealed LSMO film promoted additional CFO pillar orientations. A reorientation of the CFO magnetic easy axis to an in-plane direction occurred as the LSMO became thicker due to changes in the strain state of the CFO pillars. The LSMO underlayer enabled the ferroelectric response of the BFO to be measured. Nanocomposites were grown onto LSMO/SrTiO3/Si which provides a path towards large scale integration of electrically contacted nanocomposites on Si.

2.
J Nanosci Nanotechnol ; 13(11): 7386-90, 2013 Nov.
Article in English | MEDLINE | ID: mdl-24245260

ABSTRACT

Carbon nanotube (CNT) has excellent electrical and thermal conductivity and high aspect ratio for X-ray tube cathode. However, CNT field emission cathode has been shown unstable field emission and short life time due to field evaporation by high current density and detachment by electrostatic force. An alternative approach in this direction is the introduction of CNT yarn, which is a one dimensional assembly of individual carbon nanotubes bonded by the Van der Waals force. Because CNT yarn is composed with many CNTs, CNT yarns are expected to increase current density and life time for X-ray tube applications. In this research, CNT yarn was fabricated by spinning of a super-aligned CNT forest and was characterized for application to an X-ray tube cathode. CNT yarn showed a high field emission current density and a long lifetime of over 450 hours. Applying the CNT yarn field emitter to the X-ray tube cathode, it was possible to obtain micro-scale resolution images. The relationship between the field emission properties and the microstructure evolution was investigated and the unraveling effect of the CNT yarn was discussed.


Subject(s)
Electrodes , Microelectrodes , Nanotubes, Carbon/chemistry , Nanotubes, Carbon/ultrastructure , Radiographic Image Enhancement/instrumentation , Radiography/instrumentation , Electric Conductivity , Equipment Design , Equipment Failure Analysis , Materials Testing , Scattering, Radiation , Textiles , X-Rays
3.
Ultrasonics ; 42(1-9): 551-5, 2004 Apr.
Article in English | MEDLINE | ID: mdl-15047345

ABSTRACT

A plate of Inconel 600 was interrogated using the resonant ultrasound spectroscopy (RUS) and the reflected leaky Lamb waves (LLW). It was found that the plate used in the present work has anisotropy in its material properties by the RUS. The longitudinal and the transverse wave velocities of the Inconel 600 plate were determined by the RUS, ultrasonic pulse-echo method and cut-off frequencies of the LLWs. The wave velocities in the direction of thickness determined by the RUS under the assumption of the orthotropic symmetry were quite similar to those obtained by other methods, the pulse-echo method and from cut-off frequencies. The reflected LLW from the plate was measured with varying the incident angle. The dispersion curves obtained from the reflected LLWs show good agreement with the theoretical calculation in general. The mismatches may be caused by anisotropy of the plate.

4.
Ultrasonics ; 42(1-9): 883-8, 2004 Apr.
Article in English | MEDLINE | ID: mdl-15047401

ABSTRACT

The dispersion curves for the feeder pipes in PHWR nuclear power plants were determined. The wave modes used for the detection of notches in the feeder pipe were confirmed as F(m,2) and/or L(0,1) by an analysis of short time Fourier transformation (STFT). The axial notches in the straight pipe were not detectable, but an axial notch in a bent pipe was detected with the mode at the frequency of 500 kHz. Initial F(m,2) and/or L(0,1) modes contains a circumferential displacement and might be converted to certain complicated modes in the bent region, which is sensitive to the axial notch. The circumferential guided wave technique was also applied for quantitative evaluation of the axial notches. The waves generated by a rocking motion of the transducer along the circumferential direction were estimated as the circumferential guided waves after a review of the acquired data and the dispersion curves.

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