RESUMO
The uncertainties of spot size and position need to be clarified for x-ray sources as they can affect the detecting precision of the x-ray probe beam in applications such as radiography. In particular, for laser-driven x-ray sources, they would be more significant as they influence the inevitable fluctuation of the driving laser pulses. Here, we have employed the penumberal coded aperture imaging technique to diagnose the two-dimensional spatial distribution of an x-ray emission source spot generated from a Cu solid target irradiated by an intense laser pulse. Taking advantage of the high detection efficiency and high spatial resolution of this technique, the x-ray source spot is characterized with a relative error of â¼5% in the full width at half maximum of the intensity profile in a single-shot mode for general laser parameters, which makes it possible to reveal the information of the unfixed spot size and position precisely. Our results show the necessity and feasibility of monitoring the spot of these novel laser-driven x-ray sources via the penumbral coded aperture imaging technique.
RESUMO
Herein, synthetic graphite materials with hierarchical pores and large specific surface area were successfully prepared by one-step impregnation with lignite as the carbon source, sulfuric acid (H2SO4) as the oxidant, and phosphoric acid (H3PO4) as the activator. The microstructural characteristics of synthetic graphite were investigated via X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Moreover, the pore parameters were studied by nitrogen adsorption-desorption. The results showed that synthetic graphite had a perfect orderly layered structure with high graphitization degree and a well-developed multistage pore structure with pore sizes ranging from nanometer to micrometer. The specific surface area and pore volume were 415.29 m2 g-1 and 0.67 cm3 g-1, respectively. The results of Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS) showed that the impregnation pretreatment provided polar groups containing oxygen to the surfaces. These unique characteristics make synthetic graphite possess good adsorption capacity for dye pollutants (the adsorption rate of the methyl orange solution was 99.9% within 60 min at 50 °C, and the pH value of the solution was 3). The effects of temperature and pH value on the adsorption capacity were studied. The repeatability of the adsorption performance was also tested, and the adsorption rate was 84.6% of the initial adsorption rate after five cycles.
RESUMO
The aim of this study was to delineate the structure of the pancreatic and biliary ducts in premature infants using a novel imaging method. The duodenal papillae of 30 premature infant cadavers were dissected. The pancreatic and biliary ducts were visualized using 64-detector multislice spiral computed tomography (MSCT). Contrast agent was injected into the duodenal papilla via the hepatopancreatic ampulla of Vater. MSCT scanning revealed both the pancreatic and biliary ducts as well as the common channel in 18 cases. The bile duct was visualized in the remaining 12 cases. Four patterns of the pancreaticobiliary ductal junction were noted: Y-type (73.3%), U-type (13.3%), V-type (6.7%), and II-type (6.7%). The results showed that MSCT and three-dimensional reconstruction can be used to visualize the junction pattern and common channel of the pancreatic and biliary ducts, and the structure of the surrounding tissue, in premature infants.