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1.
Polymers (Basel) ; 13(5)2021 Mar 09.
Artigo em Inglês | MEDLINE | ID: mdl-33803474

RESUMO

This study seeks to render residues from banana plants into a useful byproduct with possible applications in wound dressings and food packaging. Films based on cellulose extracted from banana plant pseudostem and doped with phenolic compounds extracted from banana plant leaves were developed. The phenolic compounds were extracted using batch solid-liquid and Soxhlet methods, with different drying temperatures and periods of time. The total phenolic content and antioxidant activity were quantified. The optimum values were obtained using a three-day period batch-solid extraction at 40 °C (791.74 ± 43.75 mg/L). SEM analysis indicates that the pseudostem (PS) films have a porous structure, as opposed to hydroxyethyl cellulose (HEC) films which presented a homogeneous and dense surface. Mechanical properties confirmed the poor robustness of PS films. By contrast HEC films manifested improved tensile strength at low levels of water activity. FTIR spectroscopy reinforced the need to improve the cellulose extraction process, the success of lignin and hemicellulose removal, and the presence of phenolic compounds. XRD, TGA and contact angle analysis showed similar results for both films, with an amorphous structure, thermal stability and hydrophilic behavior.

2.
J Food Sci ; 79(6): E1142-9, 2014 Jun.
Artigo em Inglês | MEDLINE | ID: mdl-24891032

RESUMO

UNLABELLED: Natural extracts obtained from grape pomace are particularly interesting, due to the substantial variety of valuable compounds present with health benefits, specifically phenolic compounds such as anthocyanins, trans-resveratrol, quercetin, and proanthocyanidins. The production of such extracts has been recognized as a profitable way to valorize grape byproducts, which are low-value and most abundant. First, the effect of the solvent on the extraction of bioactive compounds from grape pomace is studied. The selected solvents are water and ethanol, biocompatible and available in wineries and distilleries. Then, different types of grape pomace obtained along the various stages of current industrial winemaking and distillation processes are analyzed. As a result, the best stage of the winemaking and distillation processes for pomace valorization is identified, corresponding to the grape byproduct with the highest potential as source of bioactive compounds. These studies were performed with Vitis vinifera variety of Tempranillo grapes (same year, same vineyard). PRACTICAL APPLICATION: This work optimizes the production of natural extracts from (byproduct) grape pomace with recognized health benefits, to be used as high value nutraceuticals ingredients. The process proposed uses renewable and low-cost resources existent in wineries and distilleries. The select solvent extracting is a mixture of the biocompatible water and ethanol. The selected fermented grape pomace was chosen from different and comparable types of grape pomace obtained at current winemaking and distillation processes, to be used in extraction without any pretreatment.


Assuntos
Flavonoides/análise , Frutas/química , Fenóis/análise , Vitis/química , Vinho/análise , Dieta , Humanos , Solventes
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