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J Biomed Mater Res A ; 70(2): 303-8, 2004 Aug 01.
Artigo em Inglês | MEDLINE | ID: mdl-15227675

RESUMO

Development of a new calcium phosphate cement (CPC) system as an alternative to that commonly used, basically consisting of tetracalcium phosphate and dicalcium phosphate self-setting mixtures, could be of interest in achieving special properties of the product. Powder mixtures of Ca(OH)(2) and KH(2)PO(4) were studied to assess their potential for the precipitation of apatite-like phase with the use of potassium phosphate salt solution as the cement liquid. X-ray diffraction and infrared (IR) spectroscopy studies and pH and setting time measurements were performed. The set cement was revealed to consist of a low crystalline carbonate-substituted apatite-like phase. The setting time of the cement was about 5 min. Its dissolution in distilled water led to an increase in solution pH to about 11.5, the pH slowly decreasing to 10.2 at day 10. The results showed the cement to be of an increased carbonate substitution ability compared to the tetracalcium phosphate-dicalcium phosphate anhydrous cement.


Assuntos
Apatitas/isolamento & purificação , Materiais Biocompatíveis/isolamento & purificação , Cimentos Ósseos/isolamento & purificação , Substitutos Ósseos/isolamento & purificação , Hidróxido de Cálcio , Fosfatos de Cálcio/isolamento & purificação , Teste de Materiais , Microscopia Eletrônica de Varredura , Fosfatos , Compostos de Potássio , Espectrofotometria Infravermelho , Difração de Raios X
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