Your browser doesn't support javascript.
loading
Mostrar: 20 | 50 | 100
Resultados 1 - 1 de 1
Filtrar
Mais filtros








Base de dados
Intervalo de ano de publicação
1.
Int J Mol Sci ; 12(12): 8575-80, 2011.
Artigo em Inglês | MEDLINE | ID: mdl-22272092

RESUMO

In this work, the results of a study comparing the use of irradiation from different regions of the infrared spectrum for the promotion of several organic reactions, are presented and discussed. This use of eco-conditions provides a green approach to chemical synthesis. A set of ten different organic reactions were evaluated, including the Knoevenagel, Hantzsch, Biginelli and Meldrum reactions. It is important to highlight the use of a commercial device that produces infrared irradiation in the near infrared region and its distribution by convection providing heating uniformity, significantly reducing reaction times, achieving good yields and proceeding in the absence of solvent. It is also worth noting that a variety of different reactions may be performed at the same time. Finally, the products obtained were identified using TLC, together with corresponding MS-data, complementarily in comparison of NMR (1)H and (13)C data with literature information.


Assuntos
Química Verde/métodos , Raios Infravermelhos , Benzaldeídos/química , Espectroscopia de Ressonância Magnética Nuclear de Carbono-13/métodos , Química Verde/instrumentação , Espectrometria de Massas/métodos , Espectroscopia de Prótons por Ressonância Magnética/métodos , Solventes/química
SELEÇÃO DE REFERÊNCIAS
DETALHE DA PESQUISA