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1.
Dent Mater ; 2024 Apr 30.
Artigo em Inglês | MEDLINE | ID: mdl-38692997

RESUMO

OBJECTIVE: The current study aimed to evaluate the effects of different combinations of chemical and mechanical challenges on the failure load, failure mode and composition of the resulting fracture surfaces of resin-composite restorations. METHODS: Three resin composites were used to fill dentin disks (2 mm inner diameter, 5 mm outer diameter, and 2 mm thick) made from bovine incisor roots. The model restorations, half of which were preconditioned with a low-pH buffer (48 h under pH 4.5), were subjected to diametral compression with either a monotonically increasing load (fast fracture) or a cyclic load with a continuously increasing amplitude (accelerated fatigue). The load or number of cycles to failure was noted. SEM was performed on the fracture surfaces to determine the proportions of dentin, adhesive, and resin composite. RESULTS: Both cyclic fatigue and acid preconditioning significantly reduced the failure load and increased the proportion of interfacial failure in almost all the cases, with cyclic fatigue having a more pronounced effect. Cyclic fatigue also increased the amount of adhesive/hybrid layer present on the fracture surfaces, but the effect of acid preconditioning on the composition of the fracture surfaces varied among the resin composites. SIGNIFICANCE: The adhesive or hybrid layer was found to be the least resistant against the chemomechanical challenges among the components forming the model restoration. Increasing such resistance of the tooth-restoration interface, or its ability to combat the bacterial actions that lead to secondary caries following interfacial debonding, can enhance the longevity of resin-composite restorations.

2.
J Adhes Dent ; 26(1): 65-78, 2024 Jan 15.
Artigo em Alemão | MEDLINE | ID: mdl-38379400

RESUMO

PURPOSE: Multiple materials are found in the root canal after fiber-post cementation. The layer of a bioceramic-based (BC) sealer may affect the bond strength (σBS) of the fiber post in the root canal. The purpose of this study was to employ multilayer compos-ite-disk models in diametral compression to investigate whether the bond strength between a fiber post and root dentin can be in-creased by the application of a primer on the BC sealer. MATERIALS AND METHODS: The multilayers of materials in the root canal required 3D finite-element (FE) stress analyses (FEA) to pro-vide precise σBS values. First, BC sealer was characterized using x-ray powder diffraction (XRD) to determine when the sealer com-pletely set and the types of crystals formed to select which primer to apply to the sealer. We selected a 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP)-based primer to treat the BC sealer before post cementation. Ultra-highspeed (UHS) imaging was utilized to analyze the crack initiation interface. The obtained failure force was used in FE analysis to calculate σBS. RESULTS: UHS imaging validated the fracture interface at the post-dentin junction as FEA simulations predicted. σBS values of the fiber posts placed with various material combinations in the root canal were 21.1 ± 3.4 (only cement/ post), 22.2 ± 3.4 (BC sealer/cement/post) and 28.6 ± 4.3 MPa (10-MDP primer treated BC sealer/cement/post). The 10-MDP-treated BC sealer exhibited the highest σBS (p < 0.05). CONCLUSION: The multilayer composite disk model proved reliable with diametral compression testing. The presence of BC sealer in the root canal does not reduce σBS of the fiber post. Conditioning the BC sealer layer with 10-MDP primer before fiber-post cemen-tation increases σBS.


Assuntos
Colagem Dentária , Metacrilatos , Materiais Restauradores do Canal Radicular , Materiais Restauradores do Canal Radicular/química , Materiais Restauradores do Canal Radicular/farmacologia , Resinas Epóxi/química , Resinas Epóxi/farmacologia , Cavidade Pulpar , Teste de Materiais , Dentina
3.
Dent Mater ; 39(10): 938-945, 2023 10.
Artigo em Inglês | MEDLINE | ID: mdl-37648562

RESUMO

OBJECTIVE: To investigate the influences of root canal instrumentation on the load capacity and fracture modes of tooth roots under axial compression by performing mechanical tests and finite element analysis (FEA). METHODS: Thirty bovine incisor roots were trimmed into cylinders of 5.0 mm diameter. They were randomly divided into two groups, one with root canals instrumented to ∼2.0 mm in diameter, and one without instrumentation. The specimens were fractured under uniaxial compression at a crosshead speed of 0.2 mm/min, and then micro-CT was used to reveal the fracture patterns in three dimensions. FEA was further performed, using the extended finite element method (XFEM), to compare the compression-induced stress distributions and the initiation and propagation of root fractures in both groups. RESULTS: The mean fracture load of the non-instrumented group (2334 ± 436 N) was statistically significantly higher than that of the instrumented group (1857 ± 377 N) (p < 0.01). Three types of root fractures were identified according to the path and length of the cracks: end-face crack, partial-length crack, and full-length crack. As to the fracture modes, the incidence of partial-length root fracture was the highest in both groups (60% for the non-instrumented group and 53.3% for the instrumented group), followed by that of full-length fracture (26.7% and 40%, respectively) and then end-face fracture (13.3% and 6.7%, respectively). The percentage of full-length fracture was slightly higher in the instrumented group. FEA showed that the compression induced higher Tresca stresses but lower maximum principal stresses in the canal walls of the instrumented group. The XFEM simulations predicted that the fracture of both groups initiated from the outer root surface near an end face and propagated axially to the middle third of the root and radially towards the root canal. These numerical results agreed well with our experimental findings. SIGNIFICANCE: Within the limitation of this study, it was found that root canal instrumentation could significantly decrease the load capacity of tooth roots and potentially increase their susceptibility to full-length root fracture under uniaxial compression.


Assuntos
Tratamento do Canal Radicular , Raiz Dentária , Animais , Bovinos , Análise de Elementos Finitos , Microtomografia por Raio-X
4.
Int Endod J ; 55(10): 1091-1102, 2022 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-35833329

RESUMO

AIM: The use of high-concentration sodium hypochlorite (NaOCl) as an endodontic irrigant remains controversial because of its potential impact on the fracture strength of endodontically treated teeth. This study evaluated the effects of using different NaOCl concentrations, with 2-min-ethylenediaminetetraacetic acid (EDTA) as the final active irrigant, on the biomechanical and structural properties of root dentine. METHODOLOGY: A new test method, which is more clinically relevant, was utilized to calculate the fracture strength of root dentine. Bovine incisors were used to obtain root dentine discs. The root canals were enlarged to mean diameter of 2.90 mm with a taper of 0.06. The resulting discs were divided into five groups (n = 20) and treated with different concentrations of NaOCl (5.25%, 2.5%, and 1.3%) for 30 min plus 17% EDTA for 2 min. The discs were then loaded to fracture by a steel rod with the same taper through the central hole. The fractured specimens were examined by scanning electron microscopy to evaluate changes in the dimensions of the remaining intertubular dentine and the tubular radius. Micro-hardness was also measured with a Knoop diamond indenter along a radius to determine the depth of dentine eroded by the irrigation. Results were analysed by one-way anova and the Tukey test. The level of significance was set at α = 0.05. RESULTS: The damage by NaOCl increased with its concentration. 5.25% NaOCl greatly reduced the fracture strength of root dentine from 172.10 ± 30.13 MPa to 114.58 ± 26.74 MPa. The corresponding reduction in micro-hardness at the root canal wall was 34.1%. The damages reached a depth of up to 400 µm (p < .05). Structural changes involved the degradation of the intratubular wall leading to enlarged dentinal tubules and the loss of intertubular dentine. Changes in the microstructural parameters showed positive linear relationships with the fracture strength. CONCLUSIONS: With the adjunctive use of EDTA, NaOCl caused destruction to the intratubular surface near the root canal and, consequently, reduced the root dentine's mechanical strength. The higher the concentration of NaOCl, the greater the effect. Therefore, endodontists should avoid using overly high concentration of NaOCl for irrigation to prevent potential root fracture in endodontically treated teeth.


Assuntos
Hipoclorito de Sódio , Dente não Vital , Animais , Bovinos , Cavidade Pulpar , Dentina , Ácido Edético/farmacologia , Humanos , Irrigantes do Canal Radicular/farmacologia , Preparo de Canal Radicular , Hipoclorito de Sódio/farmacologia
5.
Dent Mater ; 38(2): 242-250, 2022 02.
Artigo em Inglês | MEDLINE | ID: mdl-34930622

RESUMO

OBJECTIVE: To study the mechanical behavior of endodontically-treated teeth with minimally invasive endodontic access cavities and resin composite restorations under different bonding conditions using finite element analysis (FEA). METHODS: Four Class-II endodontic access cavities including the mesio-occlusal minimally-invasive (MO-MIE), mesio-occlusal conventional (MO-CONV), disto-occlusal minimally-invasive (DO-MIE), and disto-occlusal conventional (DO-CONV) cavities were prepared in 3D-printed maxillary first molars. Each tooth was subjected to root canal preparation and scanned using micro-CT to provide a 3D structural model which was virtually restored with resin composite. An intact 3D-printed molar was used as control. FEA was conducted under a 250-N vertical load. Three different interfacial bonding conditions between dentin/enamel and resin composite were considered, i.e. fully bonded, partially debonded, and fully debonded. The maximum principal stress of dentin and the normal tensile stress at the interfaces were recorded. The risk factor of failure for each component was then calculated. RESULTS: In the fully-bonded tooth, the dentin-composite interface showed significantly higher stress and a higher risk factor than dentin, indicating that debonding at the dentin-composite interface would occur prior to dentin fracture. With the dentin-composite interface debonded, the enamel-composite interface exhibited higher stress and a higher risk factor than dentin, indicating that debonding at the enamel-composite interface would occur next, also prior to dentin fracture. With the resin composite fully debonded from the tooth, stress in dentin increased significantly. Irrespective of the bonding status, the CONV groups exhibited higher median stresses in dentin than the MIE groups. SIGNIFICANCE: Within the limitation of this study, it was shown that debonding of the resin composite restoration increased the stress in dentin and hence the risk of dentin fracture in endodontically-restored teeth. Minimally-invasive access cavities could better safeguard the fracture resistance of interproximally-restored teeth compared to conventional ones.


Assuntos
Fraturas dos Dentes , Dente não Vital , Resinas Compostas/química , Preparo da Cavidade Dentária , Restauração Dentária Permanente , Análise do Estresse Dentário , Análise de Elementos Finitos , Humanos , Dente Molar , Estresse Mecânico
6.
Dent Mater ; 38(1): 204-213, 2022 01.
Artigo em Inglês | MEDLINE | ID: mdl-34949478

RESUMO

OBJECTIVE: To investigate the fatigue behavior of restored teeth, in particular the mechanisms of longitudinal dentinal cracking under cyclic mechanical loading, using finite element analysis (FEA) and the stress-life (S-N) approach. METHODS: Ten root-filled premolars restored with resin composites were subjected to step-stress cyclic loading to produce longitudinal cracks. Fracture loads and number of cycles completed at each load level were recorded. FEA was used to predict the stress amplitude of each component under the global cyclic load. Both intact and debonded conditions were considered for the dentin-composite interface in the FEA. The predicted stress concentrations were compared with the fracture patterns to help elucidate the failure mechanisms. The S-N approach was further used to predict the lifetimes of the different components in the restored teeth. Cumulative fatigue damage was represented by the sum of the fractions of life spent under the different stress amplitudes. RESULTS: Longitudinal cracks were seen in ~50% of the samples with a mean fracture load of 770 ± 45 N and a mean number of cycles to failure of 32,297 ± 12,624. The longitudinal dentinal cracks seemed to start near the line angle of the cavity, and propagated longitudinally towards the root. The sum of fractions of life spent for the dentin-composite interface exceeded 1 after ~7000 cycles when that for dentin was much lower than 1, indicating that interfacial debonding would occur prior to dentin fracture. This was supported by micro-CT images showing widened interfacial space in the cracked samples. In the debonded tooth, FEA showed dentinal stress concentrations at the gingival wall of the cavity, which coincided with the longitudinal cracks found in the cyclic loading test. The sum of fractions of life spent for dentin was close to 1 at ~30,000 cycles, similar to the experimental value. SIGNIFICANCE: Debonding of the dentin-composite interface may occur prior to longitudinal cracking of dentin in root-filled teeth under cyclic loading. The approximate time of occurrence for these events could be estimated using fatigue analysis with stresses provided by FEA. This methodology can therefore be used to evaluate the longevity of restoration designs for root-filled teeth.


Assuntos
Fraturas dos Dentes , Dente Pré-Molar , Resinas Compostas , Restauração Dentária Permanente , Análise do Estresse Dentário , Humanos , Estresse Mecânico
7.
Dent Mater ; 37(5): 796-804, 2021 05.
Artigo em Inglês | MEDLINE | ID: mdl-33653597

RESUMO

OBJECTIVE: To develop a new method to test the fracture strength of endodontically-treated root dentin. METHOD: Bovine tooth roots were transversely cut into 2-mm thick sections and the root canals were enlarged with a taper of 0.06. An outer layer of resin composite was bonded to each section to make the root canal-to-outer radius ratio smaller than 1/3. The resulting discs were treated with irrigants at the inner surface and then fractured by inserting through the center a steel rod of the same taper attached to a universal test system. Fracture strength was calculated by using Lame's equations for thick-walled cylinders. Micro-indentation was performed to evaluate the depth of dentin affected by irrigation. Finite element analysis (FEA) was performed to verify the reasonableness of using resin composite to surround the dentin section as well as the analytical solution. RESULTS: The fracture strength of endodontically-treated root dentin based on the analytical solution for a homogeneous section was 139.69 ± 32.59 MPa. However, FEA that took into account root canal softening caused by the irrigants showed that this was overestimated by about 33.5%. The corrected fracture strength of treated dentin was 114.58 ± 26.74 MPa. By incorporating the layer of affected dentin into the analytical solution, the difference in the fracture-causing stress between the analytical and numerical solutions dropped to around 9.5%. SIGNIFICANCE: A relatively simple but clinically relevant method has been developed for measuring the fracture strength of endodontically-treated root dentin. The method could be applied to root dentin that is treated by conventional canal opening and irrigation.


Assuntos
Colagem Dentária , Dente não Vital , Animais , Bovinos , Resinas Compostas , Cavidade Pulpar , Dentina , Resistência à Flexão , Cimentos de Resina , Preparo de Canal Radicular
8.
Dent Mater ; 37(5): 783-795, 2021 05.
Artigo em Inglês | MEDLINE | ID: mdl-33612308

RESUMO

OBJECTIVE: This paper aimed to derive analytical solutions for the shrinkage stress and cuspal deflection in model Class-II mesial-occlusal-distal (MOD) resin-composite restorations to better understand their dependence on geometrical and material parameters. Based on the stress solutions, it was shown how design curves could be obtained to guide the selection of dimensions and materials for the preparation and restoration of this class of cavities. METHODS: The cavity wall was considered as a cantilevered beam while the resin composite was modeled as Winkler's elastic foundation with closely-spaced linear springs. Further, a mathematical model that took into account the combined effect of material properties, sample geometry and compliance of the surrounding constraint was employed to relate the shrinkage stress at the "tooth-composite" interface to the local compliance of the cavity wall. Exact analytical solutions were obtained for cuspal deflection and shrinkage stress along the cavity wall by solving the resulting differential equation, which had the same form as that for a beam on elastic foundation with a distributed load. To quantify the shrinkage stress at the cavity floor, the resin composite was assumed to be a beam, fixed at both ends and loaded with a uniformly distributed load that approximated the shrinkage stress. The analytical solutions thus obtained were compared with results from finite element analysis (FEA). RESULTS: The analytical solution for cuspal deflection contains a dimensionless parameter, γ, which represents the stiffness of the cavity wall relative to that of the cured resin composite. For the same shrinkage strain, cuspal deflection increases with reducing γ, i.e. reducing stiffness of the cavity wall or increasing stiffness of the composite. For the same γ, cuspal deflection increases proportionally with shrinkage strain. Shrinkage stress along the cavity wall is maximum at the cavity corner and reduces towards the occlusal surface; the maximum value depends only on Young's modulus and the shrinkage strain of the resin composite. For low values of γ, the interfacial stress at the occlusal surface can become compressive. The interfacial stress at the cavity floor can be much higher than that along the cavity wall, increasing exponentially with the resin composite's thickness. The analytical solutions agree well with FEA predictions. SIGNIFICANCE: When validated, the analytical solutions and design curves presented in this study can provide useful guidelines for choosing appropriate dimensions of cavity preparations and resin composite materials with suitable mechanical properties for Class-II MOD restorations to help avoid tooth fracture and interfacial debonding caused by polymerization shrinkage.


Assuntos
Materiais Dentários , Restauração Dentária Permanente , Resinas Compostas , Preparo da Cavidade Dentária , Teste de Materiais , Estresse Mecânico
9.
Dent Mater ; 36(8): 1108-1114, 2020 08.
Artigo em Inglês | MEDLINE | ID: mdl-32505539

RESUMO

OBJECTIVE: This study aims to assess the validity of a recent theory which proposes that (1) the magnitude of the shrinkage stress of resin composites depends on the thickness of the boundary layer under triaxial constraints relative to the total thickness of the specimen and (2) the boundary-layer thickness is proportional to the diameter of the specimen. METHODS: Cylindrical specimens of three commercially available resin composites, three diameters (4, 5 and 6.3mm) and four thicknesses (2, 3, 5 and 6.5mm) were tested. Curing was applied using a LED light for 40s. Microscopic images (32×) of the specimens before and after curing were analyzed to determine the lateral shrinkage profile along the vertical axis. Boundary-layer thickness was determined from the point where lateral shrinkage displacement first reached the maximum value found at mid-thickness. RESULTS: Lateral shrinkage displacement at mid-thickness was close to the theoretical value based on published shrinkage-strain data, with the ratio between experimental and theoretical values being 1.04±0.06. The boundary-layer thickness was found to be proportional to specimen diameter only, independent of material, C-factor, and specimen thickness. The proportionality constant was 0.64±0.07, which was approximately 3 times that of the effective value indicated by shrinkage strain/stress calculations. SIGNIFICANCE: This study validates the assumption made in the shrinkage-stress theory recently proposed and provides a more precise and mechanistic interpretation for the C-factor, i.e. the C-factor, as a measure of a specimen's constraint, is the ratio between the boundary-layer thickness and the total thickness of the specimen.


Assuntos
Resinas Compostas , Teste de Materiais , Estresse Mecânico
10.
Dent Mater ; 36(3): 413-419, 2020 03.
Artigo em Inglês | MEDLINE | ID: mdl-32008749

RESUMO

OBJECTIVE: A method proposed for determining the fracture toughness (FT) of dental materials involves a 'roller' wedging open a V-notch in a cylindrical specimen. There are a number of problems with the design of this test and its mechanical analysis, and thus with the validity of the results obtained, were it to be used. Firstly, friction is ignored in calculating the horizontal wedging force. Secondly, the test specimen does not make use of a pre-crack at the notch tip. The aim of this study was to evaluate the effects of these factors on the FT calculated. METHODS: An analytical solution for the mode-I stress intensity factor (KI) of the compact tension specimen, which bears some similarities, is taken to be applicable. The mechanics of the specimen has been reanalysed, with a finite-element study of the resultant stresses, and compared with the compact-tension test. RESULTS: The assumed analytical solution can provide accurate estimates for KI for the V notched specimen. However, the apparent agreement is due to the fortuitous combination of an overestimated horizontal wedging force and an underestimated stress singularity at the crack tip. In any case, ignoring friction will lead to an overestimate of FT. SIGNIFICANCE: It is concluded that the test as presented is invalid.


Assuntos
Materiais Dentários , Teste de Materiais , Estresse Mecânico
11.
Comput Math Methods Med ; 2019: 7416076, 2019.
Artigo em Inglês | MEDLINE | ID: mdl-31379973

RESUMO

In some cases of proclined maxillary incisors, the proclination can be corrected by a fixed prosthesis. The aim of this study was to investigate the magnitude and distribution of (i) principal stresses in the adjacent alveolar bone and (ii) direct and shear stresses that are normal and parallel, respectively, to the bone-tooth interface of a normal angulated maxillary incisor, a proclined one, and a proclined one corrected with an angled prosthetic crown. 2D finite-element models were constructed, and a static load of 200 N on the palatal surface of the maxillary incisor at different load angles was applied. Load angles (complementary angle to interincisal angle) ranging from 20° to 90° were applied. The results indicate that the load angle could have a more significant impact on the overall stress distributions in the surrounding alveolar bone and along the bone-tooth interface than the proclination of the maxillary incisor. Provided that the resulting interincisal angle is 150° or smaller, the stresses in the surrounding bone and at the bone-tooth interface are similar between a proclined maxillary incisor and the one with prosthodontic correction. Hence, such a correction, when deemed appropriate clinically, can be undertaken with confidence that there is little risk of incurring additional stresses over that already in existence, in the supporting bone and at the tooth-bone interface.


Assuntos
Planejamento de Prótese Dentária , Prótese Dentária/instrumentação , Incisivo/anatomia & histologia , Maxila/anatomia & histologia , Algoritmos , Fenômenos Biomecânicos , Cefalometria , Simulação por Computador , Elasticidade , Análise de Elementos Finitos , Humanos , Incisivo/cirurgia , Modelos Lineares , Teste de Materiais , Maxila/cirurgia , Pressão , Software , Estresse Mecânico , Resistência à Tração
12.
Dent Mater ; 35(5): 818-824, 2019 05.
Artigo em Inglês | MEDLINE | ID: mdl-30885408

RESUMO

OBJECTIVE: To investigate the effect of endodontic instrumentation on fracture susceptibility of root dentin using experiments and stress analysis. METHODS: Root canals of lower premolars were enlarged with different tapers. After, teeth were cut into 2-mm sections. A metal rod of the same taper was pushed through the center of the sections using a universal test system to fracture them. The fracture load was determined from the peak load on the load-displacement curve. To determine fracture-causing stress, an axisymmetric FE model was created. An analytical solution was developed to understand the relationship between fracture load, geometrical and material parameters. RESULTS: For the same taper, increased root canal diameter did not lead to reduced fracture load. Both analytical and FE solutions showed positive linear relationship between fracture load and enlarged root canal diameter. The hoop stress was maximum at inner surface of enlarged root canal and reduced with increasing radial distance from the center. Bending of sections introduced further nonuniform stresses along the depth. Predictions for the fracture load based on the maximum hoop stress were closest to experimental values; however, account must be taken of the variation in fracture stress of dentin along the root length. Significance Our results rejected the hypothesis that fracture load of root dentin sections reduced with endodontic instrumentation size. However, the stress distributions in whole endodontically treated teeth are more complicated. Thus, caution is necessary when using thin root sections to investigate the effect of endodontic instruments on vertical root fracture.


Assuntos
Fraturas dos Dentes , Dente não Vital , Dente Pré-Molar , Cavidade Pulpar , Dentina , Humanos , Preparo de Canal Radicular , Tratamento do Canal Radicular
13.
Dent Mater ; 34(4): 649-656, 2018 04.
Artigo em Inglês | MEDLINE | ID: mdl-29398111

RESUMO

OBJECTIVE: The aim of this paper is to investigate the effects on shrinkage strain/stress development of the lateral constraints at the bonded surfaces of resin composite specimens used in laboratory measurement. METHODS: Using three-dimensional (3D) Hooke's law, a recently developed shrinkage stress theory is extended to 3D to include the additional out-of-plane strain/stress induced by the lateral constraints at the bonded surfaces through the Poisson's ratio effect. The model contains a parameter that defines the relative thickness of the boundary layers, adjacent to the bonded surfaces, that are under such multiaxial stresses. The resulting differential equation is solved for the shrinkage stress under different boundary conditions. The accuracy of the model is assessed by comparing the numerical solutions with a wide range of experimental data, which include those from both shrinkage strain and shrinkage stress measurements. RESULTS: There is good agreement between theory and experiments. The model correctly predicts the different instrument-dependent effects that a specimen's configuration factor (C-factor) has on shrinkage stress. That is, for noncompliant stress-measuring instruments, shrinkage stress increases with the C-factor of the cylindrical specimen; while the opposite is true for compliant instruments. The model also provides a correction factor, which is a function of the C-factor, Poisson's ratio and boundary layer thickness of the specimen, for shrinkage strain measured using the bonded-disc method. For the resin composite examined, the boundary layers have a combined thickness that is ∼11.5% of the specimen's diameter. SIGNIFICANCE: The theory provides a physical and mechanical basis for the C-factor using principles of engineering mechanics. The correction factor it provides allows the linear shrinkage strain of a resin composite to be obtained more accurately from the bonded-disc method.


Assuntos
Resinas Compostas/química , Análise do Estresse Dentário/métodos , Modelos Teóricos , Materiais Dentários/química , Teste de Materiais , Estresse Mecânico , Propriedades de Superfície
14.
Dent Mater ; 33(5): 536-542, 2017 05.
Artigo em Inglês | MEDLINE | ID: mdl-28377042

RESUMO

OBJECTIVE: This paper presents and verifies a simple predictive formula for laboratory shrinkage-stress measurement in dental composites that can account for the combined effect of material properties, sample geometry and instrument compliance. METHODS: A mathematical model for laboratory shrinkage-stress measurement that includes the composite's elastic modulus, shrinkage strain, and their interaction with the sample's dimensions and the instrument's compliance has previously been developed. The model contains a dimensionless parameter, Rc, which represents the compliance of the instrument relative to that of the cured composite sample. A simplified formula, 1/(2+Rc), is proposed here for the normalized shrinkage stress to approximate the original model. The accuracy of the simplified formula is examined by comparing its shrinkage-stress predictions with those given by the exact formula for different cases. These include shrinkage stress measured using instruments with different compliances, samples with different thicknesses and composites with different filler fractions. RESULTS: The simplified formula produces shrinkage-stress predictions that are very similar to those given by the full formula. In addition, it correctly predicts the decrease in shrinkage stress with an increasing configuration factor for compliant instruments. It also correctly predicts the value of the so-called flow factor of composites despite the fact that creep is not considered in the model. SIGNIFICANCE: The new simple formula significantly simplifies the prediction of shrinkage stress for disc specimens used in laboratory experiments without much loss in precision. Its explicit analytical form shows clearly all the important parameters that control the level of shrinkage stress in such measurements. It also helps to resolve much of the confusion caused by the seemingly contradictory results reported in the literature. Further, the formula can be used as a guide for the design of dental composite materials or restorations to minimize their shrinkage stress.


Assuntos
Resinas Compostas , Materiais Dentários , Modelos Teóricos , Análise do Estresse Dentário , Módulo de Elasticidade , Humanos , Teste de Materiais , Estresse Mecânico
15.
J Vis Exp ; (89)2014 Jul 21.
Artigo em Inglês | MEDLINE | ID: mdl-25079865

RESUMO

Polymerization shrinkage of dental resin composites can lead to restoration debonding or cracked tooth tissues in composite-restored teeth. In order to understand where and how shrinkage strain and stress develop in such restored teeth, Digital Image Correlation (DIC) was used to provide a comprehensive view of the displacement and strain distributions within model restorations that had undergone polymerization shrinkage. Specimens with model cavities were made of cylindrical glass rods with both diameter and length being 10 mm. The dimensions of the mesial-occlusal-distal (MOD) cavity prepared in each specimen measured 3 mm and 2 mm in width and depth, respectively. After filling the cavity with resin composite, the surface under observation was sprayed with first a thin layer of white paint and then fine black charcoal powder to create high-contrast speckles. Pictures of that surface were then taken before curing and 5 min after. Finally, the two pictures were correlated using DIC software to calculate the displacement and strain distributions. The resin composite shrunk vertically towards the bottom of the cavity, with the top center portion of the restoration having the largest downward displacement. At the same time, it shrunk horizontally towards its vertical midline. Shrinkage of the composite stretched the material in the vicinity of the "tooth-restoration" interface, resulting in cuspal deflections and high tensile strains around the restoration. Material close to the cavity walls or floor had direct strains mostly in the directions perpendicular to the interfaces. Summation of the two direct strain components showed a relatively uniform distribution around the restoration and its magnitude equaled approximately to the volumetric shrinkage strain of the material.


Assuntos
Materiais Dentários/química , Prótese Dentária , Interpretação de Imagem Assistida por Computador/métodos , Teste de Materiais/métodos , Cerâmica/química , Resinas Compostas/química , Humanos , Cura Luminosa de Adesivos Dentários/métodos , Resinas Sintéticas/química
16.
J Prosthet Dent ; 112(2): 276-84, 2014 Aug.
Artigo em Inglês | MEDLINE | ID: mdl-24461947

RESUMO

STATEMENT OF PROBLEM: Whether splinting or not splinting adjacent implants together can optimize the stress/strain transfer to the supporting structures remains controversial. PURPOSE: The purpose of this study was to compare the photoelasticity and digital image correlation (DIC) in analyzing the stresses/strains transferred by an implant-supported prosthesis. MATERIAL AND METHODS: A polymethylmethacrylate model was made with a combination of acrylic resin replicas of a mandibular first premolar and second molar and threaded implants replacing the second premolar and first molar. Splinted (G1/G3) and nonsplinted (G2/G4) metal-ceramic screw-retained crowns were loaded with (G1/G2) and without (G3/G4) the presence of the second molar. Vertical static loads were applied to the first molar implant-supported crown (50 N-photoelasticity; 250 N-DIC). The resulting isochromatic fringes in the photoelastic models were photographed, and a single-camera 2-dimensional DIC system recorded the deformation at the surface of the resin models. RESULTS: Residual stresses were present in the photoelastic model after screw fixation of the crowns. The following average photoelastic stress results (MPa) were found around the loaded implant: G1 (20.06), G2 (23.49), G3 (30.86), G4 (37.64). Horizontal strains (εxx, %) between the molars averaged over the length of the loaded implant were found by DIC: G1 (0.08 ± 0.09), G2 (0.13 ± 0.10), G3 (0.13 ± 0.11), G4 (0.16 ± 0.11). Splinted crowns transferred lower stresses to the supporting bone when the second molar was absent. The second molar optimized the stress distribution between the supporting structures even for nonsplinted restorations. CONCLUSIONS: Both methods presented similar results and seemed capable of indicating where issues associated with stress/strain concentrations might arise. However, DIC, while apparently less sensitive than photoelasticity, is not restricted to the use of light-polarizing materials.


Assuntos
Implantes Dentários , Planejamento de Prótese Dentária , Prótese Dentária Fixada por Implante , Apatitas/química , Fenômenos Biomecânicos , Ligas de Cromo/química , Coroas , Análise do Estresse Dentário , Resinas Epóxi/química , Humanos , Processamento de Imagem Assistida por Computador/métodos , Mandíbula/anatomia & histologia , Ligas Metalo-Cerâmicas/química , Modelos Anatômicos , Níquel/química , Fotografação/métodos , Polimetil Metacrilato/química , Estresse Mecânico , Titânio/química
17.
Dent Mater ; 29(11): 1108-15, 2013 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-24029101

RESUMO

OBJECTIVES: The aim of this paper is to develop a comprehensive mathematical model for shrinkage stress development in dental composites that can account for the combined effect of material properties, specimen geometry and external constraints. METHODS: A viscoelastic model that includes the composite's elastic, creep and shrinkage strains, and their interaction with the sample's dimensions and the external constraint is developed. The model contains two dimensionless parameters. The first one represents the compliance of the external constraint relative to that of the composite sample, and the second controls the rate of shrinkage stress decay through creep. The resulting differential equation is solved for two special cases: zero compliance and zero creep. Predictions for shrinkage stress measurements are then made using the analytical solutions for instruments with different compliances, samples with different thicknesses and composites with different filler fractions. RESULTS: The model correctly predicts how shrinkage stress increases with time, its dependence on the interaction between the entire system's compliance and the material properties, and the effect of the filler fraction on its maximum value. Comparisons with reported shrinkage stress measurements have provided very good agreement between theory and experiments. SIGNIFICANCE: The results provided by the model can help to resolve most, if not all, of the seemingly conflicting experimental observations reported in the literature. They can also provide some useful guidelines for optimizing the mechanical performance of dental composite restorations. The compliance ratio, a new parameter derived from the model, represents a fuller description of the constraints of the system.


Assuntos
Materiais Dentários , Estresse Mecânico , Cárie Dentária , Humanos , Modelos Teóricos
18.
Dent Mater ; 29(7): 788-96, 2013 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-23694844

RESUMO

OBJECTIVES: A validated numerical model for stress/strain predictions is essential in understanding the biomechanical behavior of implant-supported dental prostheses. The digital image correlation (DIC) method for full-field strain measurement was compared with finite element analysis (FEA) in assessing bone strain induced by implants. METHODS: An epoxy resin model simulating the lower arch was made for the experimental test with acrylic resin replicas of the first premolar and second molar and threaded implants replacing the second premolar and first molar. Splinted (G1/G3) and non-splinted (G2/G4) metal-ceramic screw-retained crowns were fabricated and loaded with (G1/G2) or without (G3/G4) the second molar that provided proximal contact. A single-camera, two-dimensional DIC system was used to record deformation of the resin model surface under a load of 250N. Three-dimensional finite element (FE) models were constructed for the physical models using computer-aided design (CAD) software. Surface strains were used for comparison between the two methods, while internal strains at the implant/resin block interface were calculated using FEA. RESULTS: Both methods found similar strain distributions over the simulant bone block surface, which indicated possible benefits of having splinted crowns and proximal contact in reducing bone strains. Internal strains predicted by FEA at the implant-resin interface were 8 times higher than those on the surface of the model, and they confirmed the results deduced from the surface strains. FEA gave higher strain values than experiments, probably due to incorrect material properties being used. SIGNIFICANCE: DIC is a useful tool for validating FE models used for the biomechanical analysis of dental prosthesis.


Assuntos
Prótese Dentária Fixada por Implante , Análise do Estresse Dentário/métodos , Análise de Elementos Finitos , Processamento de Imagem Assistida por Computador , Imageamento Tridimensional , Análise Numérica Assistida por Computador , Análise de Variância , Fenômenos Biomecânicos , Força Compressiva , Implantes Dentários , Módulo de Elasticidade , Humanos , Estatísticas não Paramétricas
19.
Dent Mater ; 28(10): 1098-104, 2012 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-22857877

RESUMO

OBJECTIVE: A novel technique using a composite disk under diametral compression was presented in a previous study for measuring the bond strength between intracanal posts and dentin. This study deals with the stress distribution within the composite disk to allow the bond strength to be calculated accurately. The effects of changing geometrical and material parameters on the post-dentin interfacial stress are also evaluated. METHODS: The finite element method with 3D models is used to analyze the stress distribution and to carry out the sensitivity analysis. Progressive post-dentin interfacial debonding is also simulated to better understand the failure process observed in experiments. RESULTS: Material mismatch causes stress concentrations at the interfaces. The results are presented as correction factors to be used in conjunction with the analytical solution for a homogeneous disk. Comparison between the stresses at the post-dentin interface and those in dentin confirms that interfacial debonding will take place prior to fracture in the dentin. SIGNIFICANCE: The numerical solutions presented here will facilitate the adoption of the composite disk in diametral compression for bond strength measurement.


Assuntos
Resinas Compostas/química , Análise do Estresse Dentário/métodos , Adesivos Dentinários/química , Dentina/química , Análise de Elementos Finitos , Teste de Materiais , Modelos Dentários , Propriedades de Superfície , Resistência à Tração
20.
Dent Mater ; 28(9): 996-1003, 2012 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-22727356

RESUMO

OBJECTIVES: The aim of this study was to numerically evaluate the effects of filler contents and resin properties on the material properties of dental composites utilizing realistic 3D micromechanical finite element models. METHODS: 3D micromechanical finite element models of dental composites containing irregular fillers with non-uniform sizes were created based on a large-scale, surrogate mixture fabricated from irregularly shaped stones and casting resin. The surrogate mixture was first scanned with a micro-CT scanner, and the images reassembled to produce a 3D finite element model. Different filler fractions were achieved by adjusting the matrix volume while keeping the fillers unchanged. Polymerization shrinkage, Young's modulus, Poisson's ratio and viscosity of the model composites were predicted using the finite element models, and their dependence on the filler fraction and material properties of the resin matrix were considered. Comparison of the numerical predictions with available experimental data and analytical models from the literature was performed. RESULTS: Increased filler fraction resulted in lower material shrinkage, higher Young's modulus, lower Poisson's ratio and higher viscosity in the composite. Predicted shrinkage and Young's modulus agreed well with the experimental data and analytical predictions. The McGee-McCullough model best fit the shrinkage and Young's modulus predicted by the finite element method. However, a new parameter, used as the exponent of the filler fraction, had to be introduced to the McGee-McCullough model to better match the predicted viscosity and Poisson's ratio with those from the finite element analysis. SIGNIFICANCE: Realistic micro-structural finite element models were successfully applied to study the effects of filler fraction and matrix properties on a wide range of mechanical properties of dental composites with irregular fillers. The results can be used to direct the design of such materials to achieve the desired mechanical properties.


Assuntos
Resinas Compostas/química , Materiais Dentários/química , Análise de Elementos Finitos , Polímeros/química , Módulo de Elasticidade , Modelos Teóricos , Distribuição de Poisson , Propriedades de Superfície , Viscosidade
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