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Rev Sci Instrum ; 78(7): 076103, 2007 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-17672802

RESUMO

An on-board sample cleaver has been developed in order to cleave small and hard-to-cleave samples. To acquire good cleaves from rigid samples the alignment of the cleaving blade with respect to the internal crystallographic planes is crucial. To have the opportunity to mount the sample and align it to the blade ex situ has many advantages. The design presented has allowed us to cleave very tiny and rigid samples, e.g., the high-temperature superconductor La((2-x))Sr(x)CuO(4). Further, in this design the sample and the cleaver will have the same temperature, allowing us to cleave and keep the sample at low temperature. This is a big advantage over prior cleaver systems. As a result, better surfaces and alignments can be realized, which considerably simplifies and improves the experiments.


Assuntos
Teste de Materiais/instrumentação , Microtomia/instrumentação , Manejo de Espécimes/instrumentação , Desenho de Equipamento , Análise de Falha de Equipamento , Teste de Materiais/métodos , Microtomia/métodos , Miniaturização , Reprodutibilidade dos Testes , Sensibilidade e Especificidade , Manejo de Espécimes/métodos , Integração de Sistemas
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