RESUMO
Nine laboratories participated in an intercomparison exercise organised by the European Radiation Dosimetry Group (EURADOS) for emergency radiobioassay involving four high-risk radionuclides ((239)Pu, (241)Am, (90)Sr and (226)Ra). Diverse methods of analysis were used by the participating laboratories for the in vitro determination of each of the four radionuclides in urine samples. Almost all the methods used are sensitive enough to meet the requirements for emergency radiobioassay derived for this project in reference to the Clinical Decision Guide introduced by the NCRP. Results from most of the methods meet the requirements of ISO 28218 on accuracy in terms of relative bias and relative precision. However, some technical gaps have been identified. For example, some laboratories do not have the ability to assay samples containing (226)Ra, and sample turnaround time would be expected to be much shorter than that reported by many laboratories, as timely results for internal contamination and early decisions on medical intervention are highly desired. Participating laboratories are expected to learn from each other on the methods used to improve the interoperability among these laboratories.
Assuntos
Bioensaio/métodos , Medicina de Emergência/métodos , Laboratórios/normas , Monitoramento de Radiação/métodos , Poluentes Radioativos/urina , Radioquímica/métodos , Urinálise/métodos , Humanos , Radiometria , Padrões de Referência , Avaliação da Tecnologia Biomédica , Urina/químicaRESUMO
Exposure to indoor radon is of great concern because it is an environmental hazard for developing lung cancer. 210Pb, a radon decay product, was measured in home dust samples from the city of Ottawa, Canada. The 210Pb level in dust ranged from 33 to 352 Bq kg(-1), with the geometric mean and median values of 105 and 110 Bq kg(-1), respectively. Despite the complexity of the formation of 210Pb in the indoor environment, an encouraging correlation between 210Pb concentrations in home dust and radon levels in indoor air was observed when the measurement data were grouped according to four geographic regions of the city. This observation could lead to the development of 210Pb in home dust as a potential marker for indoor radon exposure.
Assuntos
Poluentes Radioativos do Ar/análise , Poeira/análise , Monitoramento Ambiental/métodos , Radioisótopos de Chumbo/análise , Radônio/análise , Biomarcadores/análise , Canadá , Cidades , GeografiaRESUMO
This work investigated the application of diffusive gradients in thin films technique (DGT) to uranium speciation measurements in natural water. Two binding phases were examined, a commercially available affinity membrane, Whatman DE 81 (DE 81), with amino binding functional groups and the conventionally used Chelex 100 beads imbedded polyacrylamide hydrogel (Chelex) with iminodiacetate functional groups. The DGT devices assembled with the binding phases of DE 81 (DE 81 DGT) and Chelex gel (Chelex DGT) were tested both in synthetic river water solutions and in local river water. DE 81 DGT and Chelex DGT measured 80% and 75% of the total uranium in synthetic river water solution, respectively, and measured 73% and 60% of the total uranium in St. Lawrence River, Canada, respectively. The binding properties of the DE 81 membrane and Chelex gel for uranium, and the diffusion of uranyl complexes in the polyacrylamide gel (PAM) were also studied.