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1.
Appl Radiat Isot ; 204: 111109, 2024 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-38029636

RESUMO

The goal of this study is to provide a benchmark for the use of Monte Carlo simulation when applied to coincidence summing corrections. The examples are based on simple geometries: two types of germanium detectors and four kinds of sources, to mimic eight typical measurement conditions. The coincidence corrective factors are computed for four radionuclides. The exercise input files and calculation results with practical recommendations are made available for new users on a dedicated webpage.

2.
Anal Chim Acta ; 1141: 221-229, 2021 Jan 02.
Artigo em Inglês | MEDLINE | ID: mdl-33248656

RESUMO

Accurate measurement of naturally occurring radionuclides in blast furnace slag, a by-product of the steel industry, is required for compliance with building regulations where it is often used as an ingredient in cement. A matrix reference blast furnace slag material has been developed to support traceability in these measurements. Raw material provided by a commercial producer underwent stability and homogeneity testing, as well as characterisation of matrix constituents, to provide a final candidate reference material. The radionuclide content was then determined during a comparison exercise that included 23 laboratories from 14 countries. Participants determined the activity per unit mass for 226Ra, 232Th and 40K using a range of techniques. The consensus values obtained from the power-moderated mean of the reported participant results were used as indicative activity per unit mass values for the three radionuclides: A0(226Ra) = 106.3 (34) Bq·kg-1, A0(232Th) = 130.0 (48) Bq·kg-1 and A0(40K) = 161 (11) Bq·kg-1 (where the number in parentheses is the numerical value of the combined standard uncertainty referred to the corresponding last digits of the quoted result). This exercise helps to address the current shortage of NORM industry reference materials, putting in place infrastructure for production of further reference materials.

3.
Appl Radiat Isot ; 155: 108920, 2020 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-31622844

RESUMO

The probabilities of locating peaks with a high relative peak-area uncertainty were determined empirically with nine types of peak-location software used in laboratories engaged in gamma-ray spectrometry measurements. It was found that it is not possible to locate peaks with a probability of 0.95, when they have a relative peak-area uncertainty in excess of 50%. Locating peaks at these relatively high peak-area uncertainties with a probability greater than 0.95 is only possible in the library-driven mode, where the peak positions are supposed a-priori. The deficiencies of the library-driven mode and the possibilities to improve the probabilities of locating peaks are briefly discussed.

4.
Appl Radiat Isot ; 154: 108850, 2019 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-31476556

RESUMO

Monte Carlo (MC) simulation is widely used in gamma-ray spectrometry, however, its implementation is not always easy and can provide erroneous results. The present action provides a benchmark for several MC software for selected cases. The examples are based on simple geometries, two types of germanium detectors and four kinds of sources, to mimic eight typical measurement conditions. The action outputs (input files and efficiency calculation results, including practical recommendations for new users) are made available on a dedicated webpage.

5.
Bull Environ Contam Toxicol ; 81(1): 80-4, 2008 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-18431523

RESUMO

The main purpose of this research was to determine the levels of heavy metals in tomato, potato and lettuce, grown in agricultural soils of different soil orders (Alfisols, Endisols and Vertisols), located at Central Greece. Soil samples were analysed for available forms (after extraction with DTPA) and for total concentrations (after digestion with Aqua Regia) of metals. Zn, Cu, Cr and Ni were the common metals detected in the vegetables studied. Pb and Cd concentrations were low and in some cases not detectable. Significant correlations among metals concentrations and soil physicochemical parameters were obtained and discussed. The pH value and the percentage of clay content were found to determine the solubility of metals in the soil and their availability for uptake by plants.


Assuntos
Metais Pesados/análise , Poluentes do Solo/análise , Solo/análise , Verduras/química , Grécia , Concentração de Íons de Hidrogênio , Lactuca/química , Lactuca/metabolismo , Solanum lycopersicum/química , Solanum lycopersicum/metabolismo , Folhas de Planta/química , Raízes de Plantas/química , Dióxido de Silício , Solanum tuberosum/química , Solanum tuberosum/metabolismo
6.
Bull Environ Contam Toxicol ; 80(3): 206-10, 2008 Mar.
Artigo em Inglês | MEDLINE | ID: mdl-18193140

RESUMO

This investigation was performed in order to clarify the degree of heavy metals pollution in forest, agricultural and industrial surface soil samples in relation to pre-anthropogenic soils of Almyros region, in Central Greece. In 2004 and 2005 soil samples were collected and analysed for available (DTPA method) and total (Aqua Regia method) Cd, Cr, Cu, Pb, Zn and Ni concentrations. For each metal the enrichment factor with respect to the levels in pre-anthropogenic soils was calculated. All the types of soils appeared to be less polluted than in other investigations. In agricultural and industrial soils the available Cd concentration was higher than the other metals studied. The enrichment factor of Cu in relation to total concentration has the maximum value of the metals studied.


Assuntos
Metais Pesados/análise , Poluentes do Solo/análise , Solo/análise , Agricultura , Indústrias , Árvores
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