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J Oleo Sci ; 69(3): 271-276, 2020 Mar 01.
Artigo em Inglês | MEDLINE | ID: mdl-32051359

RESUMO

In this study, we investigated the direct detection of DNA, without pretreatment, using a quartz crystal microbalance (QCM) sensor. This sensor is modified by a self-assembled monolayer of a thiol derivative that has an amino group as the terminal functional group. Contact angle values and the attenuated total reflectance Fourier transform infrared (ATR/FT-IR) spectra of the QCM sensors after immersion into an ethanol solution of thiol derivatives clearly showed that self-assembled monolayers of the derivatives were formed on the QCM sensors. Although QCM measurements using unmodified and carboxylic group-modified sensors could not detect DNA-Na salt, the sensor modified with amino groups could detect the DNA. This system can be used for the analysis of the interaction between DNA and DNAbinding proteins.


Assuntos
DNA/análise , Técnicas de Microbalança de Cristal de Quartzo/métodos , Compostos de Sulfidrila/química , Etanol , Psicoterapia Breve , Espectroscopia de Infravermelho com Transformada de Fourier
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