Influence of Process Parameters on Selected Properties of Ti6Al4V Manufacturing via L-PBF Process.

This study investigates the microstructural effects of process parameters on Ti6Al4V alloy produced via powder bed fusion (PBF) using laser beam melting (LB/M) technology. The research focuses on how variations in laser power, exposure velocity, and hatching distance influence the final material's porosity, microhardness, and microstructure. To better understand the relationships between process parameters, energy density, and porosity, a simple mathematical model was developed. The microstructure of the alloy was analyzed in the YZ plane using a confocal microscope. The study identified optimal parameters-302.5 W laser power, 990 mm/s exposure velocity, and 0.14 mm hatching distance-yielding the lowest porosity index of 0.005%. The material's average hardness was measured at 434 ± 18 HV0.5. These findings offer valuable insights for optimizing printing parameters to produce high-quality Ti6Al4V components using PBF-LB/M technology, shedding light on the critical relationship between process parameters and the resulting microstructure.

The Structural and Mechanical Properties of Al2O3-Ni Composites Obtained by Magnetic Field-Assisted Centrifugal Slip Casting.

This study investigates the influence of a magnetic field on the microstructure and properties of Al2O3-Ni composites fabricated via centrifugal slip casting at 1500 rpm. Al2O3 and Ni powders were combined with water and deflocculants, homogenized, and then cast into a porous plaster mold surrounded by Nd-Fe-B magnets. The resulting composites, sintered in a reducing atmosphere, exhibited a three-zone structure with varying Ni content due to the combined effects of the magnetic field and centrifugal force. SEM, EDX, and XRD analyses confirmed the distribution and composition of the phases. Hardness tests revealed the highest values at the outermost zone, with a gradual decrease toward the inner zones. Compression tests employing digital image correlation revealed high internal stresses and a significant improvement in compressive strength compared to non-magnetic field methods. This study confirms that magnetic field-assisted centrifugal slip casting significantly enhances the structural, hardness, and compressive strength properties of Al2O3-Ni composites, indicating promising potential for advanced applications.

Strength and Electrostatic Discharge Resistance Analysis of Additively Manufactured Polyethylene Terephthalate Glycol (PET-G) Parts for Potential Electronic Application.

Optoelectronic components are crucial across various industries. They benefit greatly from advancements in 3D printing techniques that enable the fabrication of intricate parts. Among these techniques, Material Extrusion (MEX) stands out for its simplicity and cost-effectiveness. Integrating 3D printing into production processes offers the potential to create components with enhanced electrostatic discharge (ESD) resistance, a critical factor for ensuring the reliability and safety of optoelectronic devices. Polyethylene terephthalate glycol-modified (PET-G) is an amorphous copolymer renowned for its high transparency, excellent mechanical properties, and chemical resistance, which make it particularly suitable for 3D printing applications. This study focuses on analyzing the mechanical, structural, and electrostatic properties of pure PET-G as well as PET-G doped with additives to evaluate the effects of doping on its final properties. The findings highlight that pure PET-G exhibits superior mechanical strength compared to doped variants. Conversely, doped PET-G demonstrates enhanced resistance to electrostatic discharge, which is advantageous for applications requiring ESD mitigation. This research underscores the importance of material selection and optimization in 3D printing processes to achieve desired mechanical and electrical properties in optoelectronic components. By leveraging 3D printing technologies like MEX and exploring material modifications, industries can further innovate and enhance the production of optoelectronic devices, fostering their widespread adoption in specialized fields.

17-4 PH Steel Parts Obtained through MEX and PBF-LB/M Technologies: Comparison of the Structural Properties.

The material extrusion (MEX) method utilizing highly filled metal filament presents an alternative to advanced additive metal manufacturing technologies. This process enables the production of metal objects through deposition and sintering, which is particularly attractive compared to powder bed fusion (PBF) technologies employing lasers or high-power electron beams. PBF requires costly maintenance, skilled operators, and controlled process conditions, whereas MEX does not impose such requirements. This study compares research on 17-4 PH steel manufactured using two different commercially available techniques: MEX and powder bed fusion with laser beam melting (PBF-LB/M). This research included assessing the density of printed samples, analyzing surface roughness in two printing planes, examining microstructure including porosity and density determination, and measuring hardness. The conducted research aimed to determine the durability and quality of the obtained samples and to evaluate their strength. The research results indicated that samples produced using the PBF-LB/M technology exhibited better density and a more homogeneous structure. However, MEX samples exhibited better strength properties (hardness).

Bending Strength of Continuous Fiber-Reinforced (CFR) Polyamide-Based Composite Additively Manufactured through Material Extrusion.

This paper shows the three-point bending strength analysis of a composite material consisting of polyamide doped with chopped carbon fiber and reinforced with continuous carbon fiber produced by means of the material extrusion (MEX) additive manufacturing technique. For a comparison, two types of specimens were produced: unreinforced and continuous fiber-reinforced (CFR) with the use of carbon fiber. The specimens were fabricated in two orientations that assure the highest strength properties. Strength analysis was supplemented by additional digital image correlation (DIC) analysis that allowed for the identification of regions with maximum strain within the specimens. The utilization of an optical microscope enabled a fractographic examination of the fracture surfaces of the specimens. The results of this study demonstrated a beneficial effect of continuous carbon fiber reinforcement on both the stiffness and strength of the material, with an increase in flexural strength from 77.34 MPa for the unreinforced composite to 147.03 MPa for the composite reinforced with continuous carbon fiber.

Mechanical Properties of the AlCu4Mg1 Alloy Joint Manufactured by Underwater Friction Stir Welding.

The manuscript presents the results of butt joining of 3-millimeter-thick AlCu4Mg1 alloy sheets using the FSW (friction stir welding) and UWFSW (underwater friction stir welding) methods. The aim of the research is to verify the influence of the water environment on the FSW friction welding process. The article checked three sets of joint parameters. The parameters differed in tool rotation speed and feed rate. The same sets of parameters were used for the FSW and UWFSW fusion techniques. With the supplied devices, metallographic sections are cross-sectioned, and the power supplies are subjected to a light microscope. Microhardness tests and the influence of the heat-affected zone were carried out. A monotonic test was performed. A monotonic test is available, extended with a visual correlation test. The obtained cracked fracture surfaces were examined using a scanning microscope. An analysis of the microfractographic cracking process was carried out. The obtained results did not show any improvement in the strength properties of the obtained joints made using the UWFSW technique when using a scanning microscope.

An Eco-Friendly and Innovative Approach in Building Engineering: The Production of Cement-Glass Composite Bricks with Recycled Polymeric Reinforcements.

Cementitious-glass composite bricks (CGCBs) with 3D-printed reinforcement structures made of PET-G could be an innovative production method that relies on recycling glass waste (78%) and PET-G (8%). These bricks offer a promising solution for the construction industry, which has a significant impact on climate change due to its greenhouse gas emissions and extensive use of natural aggregates. The approach presented in this article serves as an alternative to using conventional building materials that are not only costlier but also less environmentally friendly. The conducted research included mechanical tests using digital image correlation (DIC), utilized for measuring deformations in specimens subjected to three-point bending and compression tests, as well as thermal investigations covering measurements of their thermal conductivity, thermal diffusivity, and specific heat. The results highlighted the superior thermal properties of the CGCBs with PET-G reinforcements compared to traditional cementitious-glass mortar (CGM). The CGCBs exhibited a 12% lower thermal conductivity and a 17% lower specific heat. Additionally, the use of specially designed reinforcement substantially enhanced the mechanical properties of the bricks. There was a remarkable 72% increase in flexural strength in the vertical direction and a 32% increase in the horizontal direction.

A Comparative Investigation of Properties of Metallic Parts Additively Manufactured through MEX and PBF-LB/M Technologies.

In this study, the research on 316L steel manufactured additively using two commercially available techniques, Material Extrusion (MEX) and Laser Powder Bed Fusion of Metals (PBF-LB/M), were compared. The additive manufacturing (AM) process based on powder bed synthesis is of great interest in the production of metal parts. One of the most interesting alternatives to PBF-LB/M, are techniques based on material extrusion due to the significant initial cost reduction. Therefore, the paper compares these two different methods of AM technologies for metals. The investigations involved determining the density of the printed samples, assessing their surface roughness in two printing planes, examining their microstructures including determining their porosity and density, and measuring their hardness. The tests carried out make it possible to determine the durability, and quality of the obtained sample parts, as well as to assess their strength. The conducted research revealed that samples fabricated using the PBF-LB/M technology exhibited approximately 3% lower porosity compared to those produced using the MEX technology. Additionally, it was observed that the hardness of PBF-LB/M samples was more than twice as high as that of the samples manufactured using the MEX technology.

Regeneration of the Damaged Parts with the Use of Metal Additive Manufacturing-Case Study.

The paper shows the results related to regeneration possibilities analysis of a damaged slider removed from a hydraulic splitter that was repaired using additive manufacturing (AM), laser-based powder bed fusion of metals (PBF-LB/M) technology. The results demonstrate the high quality of the connection zone between the original part and the regenerated zone. The hardness measurement conducted at the interface between the two materials indicated a significant increase equal to 35% by using the M300 maraging steel, as a material for regeneration. Additionally, the use of digital image correlation (DIC) technology enabled the identification of the area where the largest deformation occurred during the tensile test, which was out of the connection zone between the two materials.

Process Parameter Investigation and Torsional Strength Analysis of the Additively Manufactured 3D Structures Made of 20MnCr5 Steel.

An ongoing growth of the available materials dedicated to additive manufacturing (AM) significantly extends the possibilities of their usage in many applications. A very good example is 20MnCr5 steel which is very popular in conventional manufacturing technologies and shows good processability in AM processes. This research takes into account the process parameter selection and torsional strength analysis of AM cellular structures. The conducted research revealed a significant tendency for between-layer cracking which is strictly dependent on the layered structure of the material. Additionally, the highest torsional strength was registered for specimens with a honeycomb structure. To determine the best-obtained properties, in the case of the samples with cellular structures, a torque-to-mass coefficient was introduced. It indicated the best properties of honeycomb structures, which have about 10% smaller torque-to-mass coefficient values than monolithic structures (PM samples).

Performance Properties of Cement-Glass Composite Bricks (CGCB) with Additively Manufactured (AM) Polymeric Scaffolding.

This study provides an alternative to traditional masonry materials: a cement-glass composite brick (CGCB), with a printed polyethylene terephthalate glycol (PET-G) internal scaffolding (gyroidal structure). This newly designed building material consists of 86% waste (78% glass waste, and 8% recycled PET-G). It can respond to the construction market's needs and provide a cheaper alternative to traditional materials. Performed tests showed an improvement in thermal properties after the use of an internal grate in the brick matrix, i.e., an increase in thermal conductivity (5%), and a decrease in thermal diffusivity (8%) and specific heat (10%). The obtained anisotropy of the CGCB's mechanical properties was much lower than the non-scaffolded parts, indicating a very positive effect of using this type of scaffolding in CGCB bricks.

Research on Explosive Hardening of Titanium Grade 2.

In this investigation, three different explosive materials have been used to improve the properties of titanium grade 2: ammonal, emulsion explosives, and plastic-bonded explosives. In order to establish the influence of explosive hardening on the properties of the treated alloys, tests were conducted, including microhardness testing, microstructure analysis, and tensile and corrosion tests. It has been found that it is possible to achieve a 40% increase in tensile strength using a plastic explosive (PBX) as an explosive material. On the other hand, the impact of the shock wave slightly decreased the corrosion resistance of titanium grade 2. The change in corrosion rate is less than 0.1µm/year, which does not significantly affect the overall corrosion resistance of the material. The reduction in corrosion resistance is probably due to the surface geometry changes as a result of explosive treatment.

Processability of 21NiCrMo2 Steel Using the Laser Powder Bed Fusion: Selection of Process Parameters and Resulting Mechanical Properties.

With the development and popularization of additive manufacturing, attempts have been made to implement this technology into the production processes of machine parts, including gears. In the case of the additive manufacturing of gears, the availability of dedicated materials for this type of application is low. This paper summarizes the results of research on the implementation of 21NiCrMo2 low-alloy steel, which is conventionally used to produce gears as a feedstock in the PBF-LB/M process. The work presents research on the selection of process parameters based on porosity measurements, static tensile tests, and hardness measurements. In addition, the article includes a mathematical model based on the quadratic regression model, which allows the estimation of the percentage of voids in the material depending on the assumed values of independent variables (laser power, scanning velocity, and hatch distance). The paper includes a range of process parameters that enable the production of elements made of 21NiCrMo2 steel with a density of over 99.7%. Additionally, comparative tests were carried out on PBF-LB/M-manufactured steel (in the state after printing and the state after heat treatment) and conventionally manufactured steel in terms of its mechanical and microstructural properties. The results showed that the steel exhibited similar mechanical properties to other carburizing steels (20MnCr5 and 16MnCr5) that have been used to date in PBF-LB/M processes and it can be used as an alternative to these materials.

A Comparative Study on Laser Powder Bed Fusion of Differently Atomized 316L Stainless Steel.

The significant growth of Additive Manufacturing (AM), visible over the last ten years, has driven an increase in demand for small gradation metallic powders of a size lower than 100 µm. Until now, most affordable powders for AM have been produced using gas atomization. Recently, a new, alternative method of powder production based on ultrasonic atomization with melting by electric arc has appeared. This paper summarizes the preliminary research results of AM samples made of two AISI 316L steel powder batches, one of which was obtained during Ultrasonic Atomization (UA) and the other during Plasma Arc Gas Atomization (PAGA). The comparison starts from powder particle statistical distribution, chemical composition analysis, density, and flowability measurements. After powder analysis, test samples were produced using AM to observe the differences in microstructure, porosity, and hardness. Finally, the test campaign covered an analysis of mechanical properties, including tensile testing with Digital Image Correlation (DIC) and Charpy's impact tests. A comparative study of parts made of ultrasonic and gas atomization powders confirms the likelihood that both methods can deliver material of similar properties.

Bending Strength of Polyamide-Based Composites Obtained during the Fused Filament Fabrication (FFF) Process.

The research shows the comparison between two types of polyamide-based (PA) composites and pure, base material. The conducted analysis describes how the additions of carbon fibers and glass microbeads affect the material's properties and its behavior during the bending tests. All samples have been tested in the three main directions available during the FFF process. To extend the scope of the research, additional digital-image-correlation tests and fracture analyses were made. The obtained results indicated a positive influence of the addition of carbon fibers into the material's volume (from 81.39 MPa in the case of pure PA to 243.62 MPa in the case of the PA reinforced by carbon fibers).

Mechanical Properties Analysis of Explosive Welded Sheet of AA2519-Ti6Al4V with Interlayer of AA1050 Subjected to Heat-Treatment.

The paper presents results of investigations of welding sheets of AA2519-Ti6Al4V, a difficult-to-joint components materials, produced by explosive welding with a thin technological interlayer of AA1050. The joining process leads to the formation of intermetalics in the vicinity of joint and generates significant residual stresses. In the next step the laminate was subjected to a heat treatment process in order to improve the mechanical properties by precipitation hardening. This treatment should not be carried out before welding because of negative influence on a ductility of the aluminum alloy. Material in this state was subjected to the tests of chemical composition, microstructure, and microhardness. A tensile test was carried out with accompanying strain analysis by the digital image correlation (DIC) method. Moreover, the residual stresses were determined which were measured by using two methods, the X-ray diffraction and the hole drilling. This approach made it possible to measure the residual stresses both in the plane parallel to the surface and in the cross section of the laminate.

Microstructure and Mechanical Properties of Dissimilar Friction Stir Welded Joint AA7020/AA5083 with Different Joining Parameters.

The present paper aims to analyze the influence of process parameters (tool traverse speed and tool rotational speed) on the macrostructure, microhardness, and mechanical properties of dissimilar friction stir welded (FSW) butt joints. Nine combinations of FSW parameters welded joints of aluminum alloys 7020-T651 and 5083-H111 were characterized. Plates in 5 mm thickness were welded using the FSW method as dissimilar joints with three values of tool rotation parameters (400, 800, and 1200 rpm) and three welding speeds (100, 200, 300 mm/min). The macroscopic observations revealed various shapes of the stir zone and defects resulting from excess and insufficient heat input. Microfractographic analysis and tensile test results showed that the samples made with the FSW parameters of 800 rpm and 200 mm/min had the best strength properties: UTS = 303 MPa, YS = 157 MPa, and A = 11.6 %. Moreover, for all welds at welding speed 100 mm/min, the joint efficiency reached 95%.

Additive Manufacturing of Plastics Used for Protection against COVID19-The Influence of Chemical Disinfection by Alcohol on the Properties of ABS and PETG Polymers.

In this paper, the influence of disinfection on structural and mechanical properties of additive manufactured (AM) parts was analyzed. All AM parts used for a fight against COVID19 were disinfected using available methods-including usage of alcohols, high temperature, ozonation, etc.-which influence on AM parts properties has not been sufficiently analyzed. During this research, three types of materials dedicated for were tested in four different disinfection times and two disinfection liquid concentrations. It has been registered that disinfection liquid penetrated void into material's volume, which caused an almost 20% decrease in tensile properties in parts manufactured using a glycol-modified version of polyethylene terephthalate (PETG).

Selective Laser Melted M300 Maraging Steel-Material Behaviour during Ballistic Testing.

Significant growth in knowledge about metal additive manufacturing (AM) affects the increase of interest in military solutions, where there is always a need for unique technologies and materials. An important section of materials in the military are those dedicated to armour production. An AM material is characterised by different behaviour than those conventionally made, especially during more dynamic loading such as ballistics testing. In this paper, M300 maraging steel behavior was analysed under the condition of ballistic testing. The material was tested before and after solution annealing and ageing. This manuscript also contains some data based on structural analysis and tensile testing with digital image correlation. Based on the conducted research, M300 maraging steel was found to be a helpful material for some armour solutions after pre- or post-processing activities. Conducted solution annealing and ageing increased the ballistic properties by 87% in comparison to build samples. At the same time, the material's brittleness increased, which affected a significant growth in fragmentation of the perforated plate. According to such phenomena, a detailed fracture analysis was made.

The Influence of Heat Treatment on Low Cycle Fatigue Properties of Selectively Laser Melted 316L Steel.

The paper is a project continuation of the examination of the additive-manufactured 316L steel obtained using different process parameters and subjected to different types of heat treatment. This work contains a significant part of the research results connected with material analysis after low-cycle fatigue testing, including fatigue calculations for plastic metals based on the Morrow equation and fractures analysis. The main aim of this research was to point out the main differences in material fracture directly after the process and analyze how heat treatment affects material behavior during low-cycle fatigue testing. The mentioned tests were run under conditions of constant total strain amplitudes equal to 0.30%, 0.35%, 0.40%, 0.45%, and 0.50%. The conducted research showed different material behaviors after heat treatment (more similar to conventionally made material) and a negative influence of precipitation heat treatment of more porous additive manufactured materials during low-cycle fatigue testing.