Visualization of the interaction of guided acoustic waves with water by light refractive vibrometry.

Guided acoustic waves, such as Lamb waves, are widely applied for material characterization, sensing of liquids and the generation of streaming in liquids. There are numerical simulation tools for the prediction of their propagation near a solid-liquid boundary but a demand for complementary measurement techniques for the validation of the simulation results remains. In this contribution it is demonstrated that light refractive vibrometry is a suitable approach for the visualization of the interaction of guided acoustic waves with liquids. For this purpose Lamb waves were excited by piezoelectric transducers on copper plates partially immersed in water. There the fundamental symmetric and antisymmetric modes are converted to compressional waves and quasi-Scholte plate waves below a frequency-thickness product of 1 MHz mm. From the vibrometry scans the wavelengths, radiation angles and pressure amplitudes of the involved modes could be determined and thus theoretical predictions of the attenuation of the Lamb modes and the energy distribution of quasi-Scholte plate waves between the solid substrate and the liquid environment could be confirmed.

Monitoring of Soft Deposition Layers in Liquid-Filled Tubes with Guided Acoustic Waves Excited by Clamp-on Transducers.

The monitoring of liquid-filled tubes with respect to the formation of soft deposition layers such as biofilms on the inner walls calls for non-invasive and long-term stable sensors, which can be attached to existing pipe structures. For this task a method is developed, which uses an ultrasonic clamp-on device. This method is based on the impact of such deposition layers on the propagation of circumferential guided waves on the pipe wall. Such waves are partly converted into longitudinal compressional waves in the liquid, which are back-converted to guided waves in a circular cross section of the pipe. Validating this approach, laboratory experiments with gelatin deposition layers on steel tubes exhibited a distinguishable sensitivity of both wave branches with respect to the thickness of such layers. This allows the monitoring of the layer growth.

Pearls in running drops on an inclined glass substrate excited by Lamb waves.

We demonstrate that pearling droplets will be released from droplets as they sliding down a partially wetting glass plate excited by Lamb waves. During the movement, we find that the transitions at generating pearling are independent of the drop size and depend only on a critical capillary number Ca. Further up, the position of the pearls must be at or around the droplet's advancing or receding end of the initial state.

Optimized procedures for manganese-52: Production, separation and radiolabeling.

Pressed chromium-powder cyclotron targets were irradiated with 16MeV protons, producing 52Mn with average yields of 6.2±0.8MBq/µAh. Separation by solid-phase anion exchange from ethanol-HCl mixtures recovered 94.3±1.7% of 52Mn and reduced the chromium content by a factor of 2.2±0.4×105. An additional AG 1-X8 column was used to remove copper, iron, cobalt and zinc impurities from the prepared 52Mn in 8M HCl. The macrocyclic chelator DOTA was rapidly radiolabeled with 52Mn in aq. ammonium acetate (pH 7.5R.T.) with a radiochemical yield >99% within 1min and was stable for >2 days in bovine serum. The improved separation and purification methodology facilitates the use of 52Mn in basic science and preclinical investigations.