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Gram-scale synthesis of (+)- and (-)-trans-10-amino-9-hydroxy-9,10-dihydrophenanthrene by enzymatic hydrolysis.
Irurre, J; Riera, M; Guixá, M.
Afiliação
  • Irurre J; Department of Organic Chemistry, Institut Químic de Sarrià, Barcelona, Spain. jirur@iqs.url.es
Chirality ; 14(6): 490-4, 2002 Jun.
Article em En | MEDLINE | ID: mdl-12112343
The enzymatic resolution of (+/-)-trans-10-azido-9-acetoxy-9,10-dihydrophenanthrene by Candida cylindracea lipase-catalyzed hydrolysis was achieved on the gram-scale with excellent yield and enantiomeric excess. The resulting (+)- and (-)-amino alcohols were derivatized to alpha-hydroxy-N-benzenesulphonamides.
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Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: Chirality Ano de publicação: 2002 Tipo de documento: Article
Buscar no Google
Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: Chirality Ano de publicação: 2002 Tipo de documento: Article