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Triacetonide of Glucoheptonic Acid in the Scalable Syntheses of d-Gulose, 6-Deoxy-d-gulose, l-Glucose, 6-Deoxy-l-glucose, and Related Sugars.
Liu, Zilei; Yoshihara, Akihide; Jenkinson, Sarah F; Wormald, Mark R; Estévez, Ramón J; Fleet, George W J; Izumori, Ken.
Afiliação
  • Liu Z; Chemistry Research Laboratory, Department of Chemistry, University of Oxford , Oxford OX1 3TA, U.K.
  • Yoshihara A; Oxford Glycobiology Institute, Department of Biochemistry, University of Oxford , Oxford OX1 3QU, U.K.
  • Jenkinson SF; International Institute of Rare Sugar Research and Education, Kagawa University , Miki, Kagawa 761-0795, Japan.
  • Wormald MR; Chemistry Research Laboratory, Department of Chemistry, University of Oxford , Oxford OX1 3TA, U.K.
  • Estévez RJ; Oxford Glycobiology Institute, Department of Biochemistry, University of Oxford , Oxford OX1 3QU, U.K.
  • Fleet GW; Departamento de Química Orgánica and Centro Singular de Investigación en Química Biolóxica e Materiais Moleculares, Universidade de Santiago de Compostela , 15782 Santiago de Compostela, Spain.
  • Izumori K; Chemistry Research Laboratory, Department of Chemistry, University of Oxford , Oxford OX1 3TA, U.K.
Org Lett ; 18(16): 4112-5, 2016 08 19.
Article em En | MEDLINE | ID: mdl-27487167
ABSTRACT
Ease of separation of petrol-soluble acetonides derived from the triacetonide of methyl glucoheptonate allows scalable syntheses of rare sugars containing the l-gluco or d-gulo structural motif with any oxidation level at the C6 or C1 position of the hexose, usually without chromatography meso-d-glycero-d-guloheptitol available in two steps is an ideal entry point for the study of the biotechnological production of heptoses.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Açúcares Ácidos / Açúcares / Hexoses Idioma: En Revista: Org Lett Ano de publicação: 2016 Tipo de documento: Article
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Açúcares Ácidos / Açúcares / Hexoses Idioma: En Revista: Org Lett Ano de publicação: 2016 Tipo de documento: Article