Unveiling Extreme Anisotropy in Elastic Structured Media.

Periodic structures can be engineered to exhibit unique properties observed at symmetry points, such as zero group velocity, Dirac cones, and saddle points; identifying these and the nature of the associated modes from a direct reading of the dispersion surfaces is not straightforward, especially in three dimensions or at high frequencies when several dispersion surfaces fold back in the Brillouin zone. A recently proposed asymptotic high-frequency homogenization theory is applied to a challenging time-domain experiment with elastic waves in a pinned metallic plate. The prediction of a narrow high-frequency spectral region where the effective medium tensor dramatically switches from positive definite to indefinite is confirmed experimentally; a small frequency shift of the pulse carrier results in two distinct types of highly anisotropic modes. The underlying effective equation mirrors this behavior with a change in form from elliptic to hyperbolic exemplifying the high degree of wave control available and the importance of a simple and effective predictive model.

Time-driven superoscillations with negative refraction.

The flat-lens concept based on negative refraction proposed by Veselago in 1968 has been mostly investigated in the monochromatic regime. It was recently recognized that time development of the superlensing effect discovered in 2000 by Pendry is yet to be assessed and may spring surprises: Time-dependent illumination could improve the spatial resolution of the focusing. We investigate dynamics of flexural wave focusing by a 45°-tilted square lattice of circular holes drilled in a duralumin plate. Time-resolved experiments reveal that the focused image shrinks with time below the diffraction limit, with a lateral resolution increasing from 0.8λ to 0.35λ, whereas focusing under harmonic excitation remains diffraction limited. Modal analysis reveals the role in pulse reconstruction of radiating lens resonances, which repeatedly self-synchronize at the focal spot to shape a superoscillating field.

Experiments on seismic metamaterials: molding surface waves.

Materials engineered at the micro- and nanometer scales have had a tremendous and lasting impact in photonics and phononics. At much larger scales, natural soils civil engineered at decimeter to meter scales may interact with seismic waves when the global properties of the medium are modified, or alternatively thanks to a seismic metamaterial constituted of a mesh of vertical empty inclusions bored in the initial soil. Here, we show the experimental results of a seismic test carried out using seismic waves generated by a monochromatic vibrocompaction probe. Measurements of the particles' velocities show a modification of the seismic energy distribution in the presence of the metamaterial in agreement with numerical simulations using an approximate plate model. For complex natural materials such as soils, this large-scale experiment was needed to show the practical feasibility of seismic metamaterials and to stress their importance for applications in civil engineering. We anticipate this experiment to be a starting point for smart devices for anthropic and natural vibrations.

Achieving invisibility over a finite range of frequencies.

We analyze cloaking of transverse electric (TE) fields through homogenization of radially symmetric metallic structures. The two-dimensional circular cloak consists of concentric layers cut into a large number of small infinitely conducting sectors which is equivalent to a highly anisotropic permittivity. We find that a wave radiated by a magnetic line current source located a couple of wavelengths away from the cloak is almost unperturbed in magnitude but not in phase. Our structured cloak is shown to work for different wavelengths provided they are ten times larger than the outermost sectors.

Analytical and numerical analysis of lensing effect for linear surface water waves through a square array of nearly touching rigid square cylinders.

This paper describes transport properties of linear water waves propagating within a square array of fixed square cylinders. The main focus is on achieving the conditions for all-angle-negative-refraction (AANR) thanks to anomalous dispersion in fluid-filled periodic structures. Of particular interest are two limit cases when either the edges or the vertices of the cylinders come close to touching. In the former case, the array can be approximated by a lattice of thin water channels (for which dispersion curves are given in closed form and thus frequencies at which AANR occurs) whereas in the latter case, the array behaves as a checkerboard with cells consisting either of water tanks or rigid cylinders (for which standing modes are given in closed form). The tools of choice for the present analysis are, on the one hand, the finite element method which solves numerically spectral problems in periodic media, and on the other hand, a two-scale asymptotic method which provides estimates of dispersion curves and associated eigenfields through a lattice approximation (namely thin water channels between rigid cylinders). Simple duality correspondences are found based on fourfold symmetry of square water checkerboards that allow us to get some insight into their spectra. Last, some numerical evidence is provided for water waves focusing with no astigmatism through such arrays, when they are of finite extent.

Tailoring drug release rates in hydrogel-based therapeutic delivery applications using graphene oxide.

Graphene oxide (GO) is increasingly used for controlling mass diffusion in hydrogel-based drug delivery applications. On the macro-scale, the density of GO in the hydrogel is a critical parameter for modulating drug release. Here, we investigate the diffusion of a peptide drug through a network of GO membranes and GO-embedded hydrogels, modelled as porous matrices resembling both laminated and 'house of cards' structures. Our experiments use a therapeutic peptide and show a tunable nonlinear dependence of the peptide concentration upon time. We establish models using numerical simulations with a diffusion equation accounting for the photo-thermal degradation of fluorophores and an effective percolation model to simulate the experimental data. The modelling yields an interpretation of the control of drug diffusion through GO membranes, which is extended to the diffusion of the peptide in GO-embedded agarose hydrogels. Varying the density of micron-sized GO flakes allows for fine control of the drug diffusion. We further show that both GO density and size influence the drug release rate. The ability to tune the density of hydrogel-like GO membranes to control drug release rates has exciting implications to offer guidelines for tailoring drug release rates in hydrogel-based therapeutic delivery applications.

Finite checkerboards of dissipative negative refractive index.

The electromagnetic properties of finite checkerboards consisting of alternating rectangular cells of positive refractive index (epsilon= +1, micro= +1) and negative refractive index (epsilon= -1, micro= -1) have been investigated numerically. We show that the numerical calculations have to be carried out with very fine discretization to accurately model the highly singular behaviour of these checkerboards. Our solutions show that, within the accuracy of the numerical calculations, the focusing properties of these checkerboards are reasonably robust in the presence of moderate levels of dissipation. We also show that even small systems of checkerboards can display focussing effects to some extent.

Cloaking through cancellation of diffusive wave scattering.

A new cloaking mechanism, which makes enclosed objects invisible to diffusive photon density waves, is proposed. First, diffusive scattering from a basic core-shell geometry, which represents the cloaked structure, is studied. The conditions of scattering cancellation in a quasi-static scattering regime are derived. These allow for tailoring the diffusivity constant of the shell enclosing the object so that the fields scattered from the shell and the object cancel each other. This means that the photon flow outside the cloak behaves as if the cloaked object were not present. Diffusive light invisibility may have potential applications in hiding hot spots in infrared thermography or tissue imaging.

Wavelength-scale light concentrator made by direct 3D laser writing of polymer metamaterials.

We report on the realization of functional infrared light concentrators based on a thick layer of air-polymer metamaterial with controlled pore size gradients. The design features an optimum gradient index profile leading to light focusing in the Fresnel zone of the structures for two selected operating wavelength domains near 5.6 and 10.4 µm. The metamaterial which consists in a thick polymer containing air holes with diameters ranging from λ/20 to λ/8 is made using a 3D lithography technique based on the two-photon polymerization of a homemade photopolymer. Infrared imaging of the structures reveals a tight focusing for both structures with a maximum local intensity increase by a factor of 2.5 for a concentrator volume of 1.5 λ3, slightly limited by the residual absorption of the selected polymer. Such porous and flat metamaterial structures offer interesting perspectives to increase infrared detector performance at the pixel level for imaging or sensing applications.

Rayleigh-Bloch waves along elastic diffraction gratings.

Rayleigh-Bloch (RB) waves in elasticity, in contrast to those in scalar wave systems, appear to have had little attention. Despite the importance of RB waves in applications, their connections to trapped modes and the ubiquitous nature of diffraction gratings, there has been no investigation of whether such waves occur within elastic diffraction gratings for the in-plane vector elastic system. We identify boundary conditions that support such waves and numerical simulations confirm their presence. An asymptotic technique is also developed to generate effective medium homogenized equations for the grating that allows us to replace the detailed microstructure by a continuum representation. Further numerical simulations confirm that the asymptotic scheme captures the essential features of these waves.

Thermal invisibility based on scattering cancellation and mantle cloaking.

We theoretically and numerically analyze thermal invisibility based on the concept of scattering cancellation and mantle cloaking. We show that a small object can be made completely invisible to heat diffusion waves, by tailoring the heat conductivity of the spherical shell enclosing the object. This means that the thermal scattering from the object is suppressed, and the heat flow outside the object and the cloak made of these spherical shells behaves as if the object is not present. Thermal invisibility may open new vistas in hiding hot spots in infrared thermography, military furtivity, and electronics heating reduction.

Analogies between optical propagation and heat diffusion: applications to microcavities, gratings and cloaks.

A new analogy between optical propagation and heat diffusion in heterogeneous anisotropic media has been proposed recently by three of the present authors. A detailed derivation of this unconventional correspondence is presented and developed. In time harmonic regime, all thermal parameters are related to optical ones in artificial metallic media, thus making possible to use numerical codes developed for optics. Then, the optical admittance formalism is extended to heat conduction in multilayered structures. The concepts of planar microcavities, diffraction gratings and planar transformation optics for heat conduction are addressed. Results and limitations of the analogy are emphasized.

Sonic band gaps in PCF preforms: enhancing the interaction of sound and light.

We study the localisation and control of high frequency sound in a dual-core square-lattice photonic crystal fibre preform. The coupled states of two neighboring acoustic resonances are probed using an interferometric set up, and experimental evidence is obtained for odd and even symmetry trapped states. Full numerical solutions of the acoustic wave equation show the existence of a two-dimensional sonic band gap, and numerical modelling of the strain field at the defects gives results that agree well with the experimental observations. The results suggest that sonic band gaps can be used to manipulate sound with great precision and enhance its interaction with light.

Duality relation for the Maxwell system.

This paper is intended to establish a link between the vector Maxwell system for three-dimensional (3D) and 2D finite photonic crystals in the low-frequency limit. For this, we generalize the classical results of Keller and Dykhne (chessboard problem) to periodic media described by piecewise continuous permittivity profiles: our theorem enlights the result of Mendelson (polycrystalline and multiphase media) in the framework of homogenization theory of elliptic operators. In fine, we give illustrative examples by using both integral equation and variational approaches via the so-called method of fictitious charges and finite-element method.

An asymptotic theory for waves guided by diffraction gratings or along microstructured surfaces.

An effective surface equation, that encapsulates the detail of a microstructure, is developed to model microstructured surfaces. The equations deduced accurately reproduce a key feature of surface wave phenomena, created by periodic geometry, that are commonly called Rayleigh-Bloch waves, but which also go under other names, for example, spoof surface plasmon polaritons in photonics. Several illustrative examples are considered and it is shown that the theory extends to similar waves that propagate along gratings. Line source excitation is considered, and an implicit long-scale wavelength is identified and compared with full numerical simulations. We also investigate non-periodic situations where a long-scale geometrical variation in the structure is introduced and show that localized defect states emerge which the asymptotic theory explains.

Platonic scattering cancellation for bending waves in a thin plate.

We propose an ultra-thin elastic cloak to control the scattering of bending waves in isotropic heterogeneous thin plates. The cloak design makes use of the scattering cancellation technique applied, for the first time, to the biharmonic operator describing the propagation of bending waves in thin plates. We first analyze scattering from hard and soft cylindrical objects in the quasistatic limit, then we prove that the scattering of bending waves from an object in the near and far-field regions can be suppressed significantly by covering it with a suitably designed coating. Beyond camouflaging, these findings may have potential applications in protection of buildings from earthquakes and isolating structures from vibrations in the motor vehicle industry.

Fick's second law transformed: one path to cloaking in mass diffusion.

Here, we adapt the concept of transformational thermodynamics, whereby the flux of temperature is controlled via anisotropic heterogeneous diffusivity, for the diffusion and transport of mass concentration. The n-dimensional, time-dependent, anisotropic heterogeneous Fick's equation is considered, which is a parabolic partial differential equation also applicable to heat diffusion, when convection occurs, for example, in fluids. This theory is illustrated with finite-element computations for a liposome particle surrounded by a cylindrical multi-layered cloak in a water-based environment, and for a spherical multi-layered cloak consisting of layers of fluid with an isotropic homogeneous diffusivity, deduced from an effective medium approach. Initial potential applications could be sought in bioengineering.

Asymptotics for metamaterials and photonic crystals.

Metamaterial and photonic crystal structures are central to modern optics and are typically created from multiple elementary repeating cells. We demonstrate how one replaces such structures asymptotically by a continuum, and therefore by a set of equations, that captures the behaviour of potentially high-frequency waves propagating through a periodic medium. The high-frequency homogenization that we use recovers the classical homogenization coefficients in the low-frequency long-wavelength limit. The theory is specifically developed in electromagnetics for two-dimensional square lattices where every cell contains an arbitrary hole with Neumann boundary conditions at its surface and implemented numerically for cylinders and split-ring resonators. Illustrative numerical examples include lensing via all-angle negative refraction, as well as omni-directive antenna, endoscope and cloaking effects. We also highlight the importance of choosing the correct Brillouin zone and the potential of missing interesting physical effects depending upon the path chosen.

Negative refraction, surface modes, and superlensing effect via homogenization near resonances for a finite array of split-ring resonators.

We present a theoretical and numerical analysis of liquid surface waves (LSWs) localized at the boundary of a phononic crystal consisting of split-ring resonators (SRRs). We first derive the homogenized parameters of the fluid-filled structure using a three-scale asymptotic expansion in the linearized Navier-Stokes equations. In the limit when the wavelength of the LSW is much larger than the typical heterogeneity size of the phononic crystal, we show that it behaves as an artificial fluid with an anisotropic effective shear modulus and a dispersive effective-mass density. We then analyze dispersion diagrams associated with LSW propagating within an infinite array of SRR, for which eigensolutions are sought in the form of Floquet-Bloch waves. The main emphasis is given to the study of localized modes within such a periodic fluid-filled structure and to the control of low-frequency stop bands associated with resonances of SRRs. Considering a macrocell, we are able to compute the dispersion of LSW supported by a semi-infinite phononic crystal of SRRs. We find that the dispersion of this evanescent mode nearly sits within the first stop band of the doubly periodic structure. We further discover that it is linked to the frequency at which the effective-mass density of the homogenized phononic crystal becomes negative. We demonstrate that this surface mode displays the hallmarks of all-angle negative refraction and it leads to a superlensing effect. Last, we note that our homogenization results for the velocity potential can be applied mutatis mutandis to designs of electromagnetic and acoustic superlenses for transverse electric waves propagating in arrays of infinite conducting SRRs and antiplane shear waves in arrays of cracks shaped as SRRs.