Application of RSM Method for Optimization of Geraniol Transformation Process in the Presence of Garnet.

This paper presents the results of tests obtained for the transformation of geraniol in the presence of garnet as a catalyst by the response surface method (RSM). The method analyzed the influence of the following parameters: a temperature of 50-150 °C, a catalyst concentration (garnet) of 1.0-10.0 wt% and a reaction time of 0.25-24 h. Response functions included the conversion of geraniol (GA), selectivity for conversion to neral (NE) and selectivity for conversion to citronellol (CL). In addition, the influence of all control parameters on each of the response parameters is presented in the form of second-order polynomials. The optimal parameters of the geraniol transformation process were a temperature of 55 °C, a catalyst concentration of 5 wt% and a reaction time of 2 h, for which high values of the GA conversion function and the selectivity of conversion to NE and CL were obtained. For the GA conversion, the optimum was obtained at 94 mol% at 60 °C, a catalyst concentration of 5.0 wt% and a reaction time of 2 h. For NE selectivity, the optimum value was reached at 49 mol% at 60 °C, a catalyst concentration equal to 2.5 (5.0) wt% mole and a reaction time of almost 2 h. For CL selectivity, the optimum value of 49 mol% was obtained for control factors: a temperature equal to 20 °C, a catalyst concentration equal to 5.0 wt% and a response time equal to 2 h. The optimal set of control factors for all power factors is characterized by a temperature of 55 °C, a catalyst concentration of 5 wt% and a reaction time of 2 h.

Enhancing High-Alloy Steel Cutting with Abrasive Water Injection Jet (AWIJ) Technology: An Approach Using the Response Surface Methodology (RSM).

The common machining technologies for difficult-to-machine materials do not remarkably ensure acceptable efficiency and precision in bulk materials cutting. High-energy abrasive water injection jet (AWIJ) treatment can cut diverse materials, even multi-layer composites characterized by divergent properties, accurately cutting complex profiles and carrying them out in special circumstances, such as underwater locations or explosion hazard areas. This work reports research on the AWIJ machining quality performance of X22CrMoV12-1 high-alloy steel. The response surface method (RSM) was utilized in modeling. The most influencing process control parameters on cut kerf surface roughness-abrasive flow rate, pressure, and traverse speed-were tested. The result is a mathematical model of the process in the form of a three-variable polynomial. The key control parameter affecting the cut slot roughness turned out to be the traverse speed. In contrast, pressure has a less significant effect, and the abrasive mass flow rate has the slightest impact on the cut slot roughness. Under the optimal conditions determined as a result of the tests, the roughness of the intersection surface Sq does not exceed 2.3 µm. Based on the ANOVA, we confirmed that the model fits over 96% appropriately with the research outcomes. This method reduces the computations and sharply determines the optimum set of control parameters.

Preliminary Studies into Cutting of a Novel Two Component 3D-Printed Stainless Steel-Polymer Composite Material by Abrasive Water Jet.

Composites are materials with a heterogeneous structure, composed of two or more components with different properties. The properties of composites are never the sum or average of the properties of their components. There is a lot of research and many models on the different property assessments of composite materials. Composites are used as construction materials in key areas of technology, including in civil and mechanical engineering, aviation and space technology, and others. This work presents a modern composite material created with 3D-printing technology using the SLM method, and the possibility of its processing with one of the advanced manufacturing technologies, i.e., the Abrasive Water Jet (AWJ). Tests planned using DoE methods were carried out by changing control parameters such as the pressure, abrasive flow, and traverse speed. As a dependent parameter, the surface roughness parameter Sq (squared mean height) was selected and measured in different places of the cut composite. Based on the S/N ratio, the most favorable control parameters of the cutting process were also determined to achieve the lowest roughness of the cut surface. A clear effect of the controlled cutting process on the surface roughness was observed, as well as roughness variation for the metal and polymer component. In addition, the contact surface of the polymer with the metal in the cut zone was analyzed. Analysis of the contact surfaces on the microscope showed that the gap between the polymer-metal contact surfaces does not exceed 2.5 µm.

Efficiency of Tool Steel Cutting by Water Jet with Recycled Abrasive Materials.

High-pressure water jet machining is characterized by wide possibilities of cutting diverse materials together with multi-layer materials with dissimilar properties, accurate cutting complex profiles, as well as conducting them in uncommon conditions, especially in cases of thick materials. An additional advantage of water jet technology is its environmental friendliness. This paper presents tests of the cutting performance of tool steel with the use of an abrasive water jet (AWJ). The state-of-the-art has shown insufficient scientific evidence in AWJ tool steels cutting using recycled abrasive materials. Therefore, the main motivation for this paper was to carry out research from an environment aspect. The reuse of abrasives and the use of recycled materials have immense potential to reduce processing costs while remaining environmentally friendly. The RSM method was used for modeling and optimization. A response surface design (RSM) is a package of an advanced design-of-experiment (DOE) approaches that support better understanding and optimize response, exploring the relationships between several explanatory variables and one or more response variables. Based on this research, feed rate is the key factor influencing the depth of cut, while the water nozzle diameter has a secondary effect, and the concentration of abrasive has the least influence on the depth of cut. High level of variance (the percentage of variability in the reaction that is interpreted by the formula) confirms that the models fit well to the investigational data.

Research into the Disintegration of Abrasive Materials in the Abrasive Water Jet Machining Process.

The size and distribution of abrasive particles have a significant influence on the effectiveness of the cutting process by the high-speed abrasive water jet (AWJ). This paper deals with the disintegration intensity of abrasive materials in AWJ cutting during the creation of the abrasive jet. An evaluation of the abrasive materials was performed after forming in the cutting head was carried out and grain distribution was evaluated using the geometric and logarithmic Folk and Ward method. The influence of the abrasive concentration of abrasive materials such as alluvial garnet, recycled garnet, corundum, and olivine on grain distribution was studied. A recovery analysis was also carried out and the recycling coefficient was determined for each abrasive material tested.