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1.
Molecules ; 29(18)2024 Sep 15.
Artículo en Inglés | MEDLINE | ID: mdl-39339387

RESUMEN

The current study proceeded to reduce the environmental hazards spreading worldwide due to synthetic dyes. To overcome these problems, eco-friendly natural dyes are introduced as alternative sources of synthetic dyes. The present study was focused on exploring the bio-colorant of the aqueous and acidic extract of the bark of Melia azedarach L. for the dyeing of both silk and cotton samples. The results of the extraction medium specified that the aqueous extract gave maximum colorant solubility and upon fabric dyeing produced higher color strength in contrast to the acidic medium. The optimization experimentation data showed that excellent color strength of silk fabric was found at 45 min dyeing time duration, in 35:1 mL dye extract, and using 2% salt (NaCl) as an exhausting agent, whereas cotton fabric showed the maximum K/S value at 60 min dyeing time, in a 45:1 mL liquor ratio, and with the use of 2% salt. Bio-mordants produce different shades on both fabrics. Bio-mordanting experiments on silk revealed that pre-mordanting with 2% turmeric and 3% pomegranate, and post-mordanting using 3% turmeric and 2% pomegranate produced a darker shade. In the case of cotton, the pre-mordanted samples with 2% turmeric and 3% pomegranate and the post-mordanted samples with 4% turmeric and 4% pomegranate gave the highest color strengths. All the mordanted samples gave excellent fastness ratings. Overall, it has been found that Bakain bark proved to be an excellent source of tannin. The result of this study showed that it could be a cost-effective and eco-friendly dye source for textile progress.


Asunto(s)
Colorantes , Corteza de la Planta , Extractos Vegetales , Textiles , Colorantes/química , Corteza de la Planta/química , Extractos Vegetales/química , Textiles/análisis , Celulosa/química , Color , Fibra de Algodón/análisis
2.
Sci Prog ; 107(3): 368504241271737, 2024.
Artículo en Inglés | MEDLINE | ID: mdl-39109939

RESUMEN

In the industrial sector, vegetable residual materials have received attention in the production of bio-colorant for textile dyeing. The current research endeavor is centered on investigating the possibility of using sugar beet leaves as a natural source of dye for the purpose of dyeing cotton fabrics. Different extraction methods were utilized to isolate the bio-colorant present in sugar beet residual material, and the most favorable colorant yield was obtained using a 5% methanolic KOH solution. For optimal dyeing results, the cotton fabric performed dyeing for a duration of 45 min at a temperature of 60 °C, using a salt solution concentration of 6 g/100 mL and 50 mL of the extracted dye solution. Characterization of dye using Fourier transform infrared spectroscopy analysis confirmed the presence of quercetin in the leaf extract. For the creation of a range of color variations, mordants that were chemical in nature, such as tannic acid, iron sulfate, potassium dichromate, and copper sulfate, as well as mordants that were bio-based, such as onion peel, pomegranate peel, henna, golden shower bark, and turmeric, were employed in harmony. In comparison, the utilization of bio-mordants resulted in darker shades that exhibited enhanced color intensity and superior color fastness properties with the value of 4-5 for wash, 4 for wet rubbing, 4-5 for dry rubbing, and 4-5 for light. The findings of this study hold significant value in terms of ecofriendly waste management and contribute to advancements in the industrial sector by utilizing waste residual materials as a natural source of colorants.


Asunto(s)
Beta vulgaris , Colorantes , Hojas de la Planta , Beta vulgaris/química , Hojas de la Planta/química , Colorantes/química , Extractos Vegetales/química , Espectroscopía Infrarroja por Transformada de Fourier , Fibra de Algodón/análisis , Color , Industria Textil
3.
Sci Rep ; 14(1): 13032, 2024 06 06.
Artículo en Inglés | MEDLINE | ID: mdl-38844676

RESUMEN

Green products such as plant tints are becoming more and more well-known worldwide due to their superior biological and ayurvedic properties. In this work, colorant from Amba Haldi (Curcuma aromatica) was isolated using microwave (MW), and bio-mordants were added to produce colorfast shades. Response surface methodology was used to develop a central composite design (CCD), which maximizes coloring variables statistically. The findings from 32 series of experiments show that excellent color depth (K/S = 12.595) was established onto MW-treated silk fabric (RS = 4 min) by employing 65 mL of radiated aqueous extract (RE = 4 min) of 5 pH cutting-edge the existence of 1.5 g/100 mL used sodium chloride at 75 °C for 45 min. It was discovered that acacia (keekar) extract (1%), pomegranate extract (2%), and pistachio extract (1.5%) were present before coloring by the use of bio-mordants. On the other hand, upon dyeing, acacia extract (1.5%), pomegranate extract (1.5%), and pistachio extract (2%) have all shown extremely strong colorfast colors. Comparatively, before dyeing, salts of Al3+ (1.5%), Fe2+ (2%), and TA (1.5%) gave good results; after dyeing, salts of Al3+ (1%) and Fe2+ (1.5%) and TA (2%) gave good results. When applied to silk fabric, MW radiation has increased the production of dyes recovered from rhizomes. Additionally, the right amount of chemical and biological mordants have been added, resulting in color fastness ratings ranging from outstanding to good. Therefore, the natural color extracted from Amba Haldi can be a sustainable option for the dyeing of silk fabric in the textile dyeing and finishing industries.


Asunto(s)
Colorantes , Curcuma , Extractos Vegetales , Rizoma , Seda , Curcuma/química , Rizoma/química , Colorantes/química , Extractos Vegetales/química , Seda/química , Microondas , Color , Tecnología Química Verde/métodos
4.
Sci Prog ; 107(2): 368504241242282, 2024.
Artículo en Inglés | MEDLINE | ID: mdl-38614468

RESUMEN

This research aims to optimize the silk and wool dyeing process using natural dyes from Bixa orellana (annatto) through response surface methodology. Central composite design experiments highlight the significant enhancement of color outcomes achieved through microwave treatment. For silk, the optimal conditions (80 °C for 40 min) with annatto extract yield a color strength (K/S) of 17.8588, while wool achieves a K/S of 7.5329. Introducing eco-friendly bio-mordants, such as pomegranate peel and red sumac tannins, enhances color strength. Pre-dyeing treatments with 2% red sumac, 1.5% pomegranate peel, and weld flower extracts for silk produce high color strength, with K/S values of 16.4063, 16.3784, and 12.1658, respectively. Post-dyeing, the K/S values increase to 40.1178, 17.4779, and 21.6494. Wool yarn exhibits similar improvements, with pre-dyeing K/S values of 13.1353, 13.5060, and 16.3232, escalating to 10.5892, 15.3141, and 23.4850 post-dyeing. Furthermore, this research underscores improved colorfastness properties, including notable enhancements in light, wash, and rubbing fastness for both silk fabric and wool yarn. These findings underscore the efficacy of the proposed sustainable dyeing methods, offering valuable insights for eco-friendly textile production.


Asunto(s)
Carotenoides , Árboles , Lana , Animales , Bixaceae , Textiles , Semillas , Seda
5.
Environ Sci Pollut Res Int ; 30(52): 112825-112835, 2023 Nov.
Artículo en Inglés | MEDLINE | ID: mdl-37840083

RESUMEN

This study investigates the absorption behavior of natural dyes on silk fabric: madder roots (red dye) and amaltas (brown dye). The dyes were extracted under optimized conditions in an acidic medium. Binary mixtures of these dyes in different proportions were employed to develop various shades. This research work has explored the impact of single as well as binary mixture of chemical mordants on the dyeing behavior of natural dyes on silk. Al (Alum), iron (Fe), and tannic acid (T.A.) were used as pre- and post-mordants. Different concentrations of the dye mixtures were used to achieve different shades. The absorption behavior of the binary mixture of natural dyes was assessed using a spectra photometer Colori-spectra SF600. The study found that the highest color strength was achieved when an acidic extract with a table salt concentration of 2 g/100 mL was applied to silk fabric at 65 °C for 55 min and subjected to microwave treatment for 6 min. The study revealed excellent results for the selected binary mixtures of chemical mordants, such as (Al + Fe), (Al + T.A.), and (Fe + T.A.), in comparison by employing single mordants such as (Al, Fe, and T.A.).


Asunto(s)
Colorantes , Seda , Textiles , Plantas , Taninos
6.
Environ Sci Pollut Res Int ; 30(58): 122262-122273, 2023 Dec.
Artículo en Inglés | MEDLINE | ID: mdl-37968482

RESUMEN

Agricultural waste is an unwanted material that is not only unmarketable, but also has secondary costs such as environmental pollution. Oleaster, also known as olive Russian fruit, has various uses, but it also produces waste such as seeds and peels. Oleaster fruit and all its parts are tannin rich, which can be utilized as natural mordant. Improvement of fastness and color properties of natural dyed fibers is obtained by using mordant. The employing of this mordant is effective in reducing agricultural waste and the production of dyeing chemical waste. Reseda extract was utilized as natural dye to investigate the color characteristics. The study of the phenolic percentage of different components of the Oleaster fruit, including peel, seed, and flesh, showed that each of these materials can be used as natural mordant. The formation of physical bonds in the presence of all kinds of mordant was investigated using the FTIR method, and the results showed that their performance is similar and they are effective in surface treatment of wool. Investigation of color characteristics of the yarns showed that the color strength increases in the presence of mordant. Studying the fastness of yarns dyed with ISO methods showed that the samples have high washing fastness.


Asunto(s)
Colorantes , Elaeagnaceae , Lana , Animales , Colorantes/química , Contaminación Ambiental , Semillas , Taninos/análisis , Lana/química , Elaeagnaceae/química
7.
Cureus ; 15(3): e36975, 2023 Mar.
Artículo en Inglés | MEDLINE | ID: mdl-37131567

RESUMEN

Background Appendicitis is a common clinical problem that has multifactorial etiologies. Accounting for almost 1 million hospital days per year, it poses serious health hazards. If not treated on time, it may burst. Surgical intervention is the best option in such cases. Prophylactic use of antibiotics has been shown to reduce post-operative infections. Methodology This prospective observational study aimed to evaluate the adherence to the antibiotic prophylaxis guidelines for appendectomy in patients admitted to the surgical department at Salmanyia Medical Complex in Bahrain from January to August 2020. From the electronic records of these patients, information was extracted and evaluated regarding demographic data, the type of antibiotics given for prophylaxis, the timing of the administration of the antibiotics, and any alternative antibiotic given based on local hospital guidelines. Results The current study revealed that the majority of the patients (98%, N=273) admitted to the Salmanyia Medical Complex, Bahrain, were not administered the antibiotics within the prescribed time (30-60 minutes) as per hospital guidelines. Also, the antibiotics administered for prophylaxis prior to the appendectomy procedure were not according to the guidelines, i.e., Cefazolin 1g with Metronidazole 500 mg. Out of a total of 278 patients included in the study, none were administered the right choice as provided by the local guidelines. Second, 1.8% of patients (5 out of 278) were not administered any antibiotics for prophylaxis prior to the surgical procedure for appendicitis. Conclusion The study concluded that most patients were not administered antibiotics according to the local guidelines of the hospital.

8.
J Surg Case Rep ; 2023(9): rjad521, 2023 Sep.
Artículo en Inglés | MEDLINE | ID: mdl-37724066

RESUMEN

Awake craniotomy (AC) is a neurosurgical technique that enables the precise localization of functional neural networks through intraoperative brain mapping and real-time monitoring. This operative method has been popularized in recent years due to decreased postoperative morbidities. We present a case of 31-year-old female who was presented with episodes of generalized tonic colonic seizures. She had a history of recurring seizures. Upon further investigations, she was diagnosed with brain space-occupying lesions initially suspected as low-grade glioma. Considering the lesion site, the patient was deemed a suitable candidate for an AC. To achieve conscious sedation, the patient received infusions of remifentanil and propofol at varying rates. During the procedure, the patient was under sedation and was regularly tested for response to predetermined commands. The tumor was successfully excised by using a combination of local anesthesia on the scalp and by the administration of propofol and boluses through a systemic infusion.

9.
Cureus ; 15(9): e46250, 2023 Sep.
Artículo en Inglés | MEDLINE | ID: mdl-37908946

RESUMEN

The preoperative assessment of patients undergoing surgery, often conducted in pre-anesthesia clinics, plays an important role in ensuring patient safety and optimizing perioperative outcomes. This assessment aids in identifying underlying medical conditions that might otherwise remain asymptomatic until they manifest as complications during or after surgery. Through these two case reports, the importance of pre-anesthesia assessment is highlighted. The first case involves a 67-year-old male whose surgery for lymph node excision was planned. However, during the preoperative assessment, atrial fibrillation and pulmonary hypertension were identified, necessitating further intervention and treatment adjustments before surgery. In the second case, an eight-year-old child with a history of vomiting and abdominal pain planned for tonsillectomy was discovered to have congenital hypothyroidism through a vigilant preoperative evaluation. Timely intervention and consultation with an endocrinologist ensured a safe surgery without complications. These cases emphasize the role of preoperative cardiovascular assessment, the utility of electrocardiograms (ECGs), and the relevance of routine laboratory tests in reducing perioperative mortality. Hence, pre-anesthesia assessments are not mere routine steps; they are essential components of patient care that significantly impact perioperative results.

10.
Nat Prod Res ; : 1-7, 2023 Nov 11.
Artículo en Inglés | MEDLINE | ID: mdl-37950664

RESUMEN

Natural products have become the main focus of mankind due to increasing environmental pollution. The current study was concerned with brinjal plant residues as a source of bio colourant for cotton dyeing. Various media have been employed for the extraction of colourant. Present studies illustrated that excellent colourant yield was obtained in 4% acidified methanol. Cotton fabric was dyed at 50 °C, for 55 min and showed optimised dyeing conditions. Varying chemicals and bio-mordants have been used to achieve elegant shade. Chemical mordanting results revealed that 2% FeSO4as pre-mordant, and 6% TA as post-mordant while in bio- mordanting, 8% of pomegranate peel extract as pre-mordant and 2% pomegranate peel extract as post-mordant indicated a darker shade to mordanted fabrics. Bio-mordanting gave darker shade, and fastness which revealed that bio-mordants have improved the fastness characteristics. FTIR results revealed the confirmation of flavonoids as a colourant for cotton dyeing.

11.
Cureus ; 15(5): e38913, 2023 May.
Artículo en Inglés | MEDLINE | ID: mdl-37313098

RESUMEN

Acute pancreatitis (AP) is a rare event in pregnancy that is characterized by a sudden and severe inflammation of the pancreas. The clinical manifestation of AP during pregnancy is highly variable ranging from a mild form to a severe and potentially life-threatening presentation. We share a case of a 29-year-old female (gravida II, para I) who presented in her 33rd gestational week. The patient complained of upper abdominal pain and nausea. Her previous history revealed that she had four episodes of vomiting (food-containing, non-projectile) at home. Her uterine tone was normal, and her cervix was closed. Her white blood cell count was 13,000/mm3, and her C-reactive protein (CRP) level was 65 mg/L. She underwent an emergency laparotomy due to suspected acute appendicitis; however, no peritonitis was found intraoperatively. Further blood tests showed high levels of triglyceride at 87.5 mmol/L. The electrophoretic pattern of lipoprotein was consistent with type V hyperlipoproteinemia. An abdominal computed tomography (CT) confirmed the diagnosis of acute pancreatitis. During follow-up after one month, the patient showed triglyceride levels at 4.75 mmol/L and cholesterol at 6.07 mmol/L. Acute pancreatitis due to hypertriglyceridemia is a rare finding; nonetheless, it should be considered as a potential etiology in pregnant patients with nonobstructive abdominal pain.

12.
Environ Sci Pollut Res Int ; 30(10): 27073-27080, 2023 Feb.
Artículo en Inglés | MEDLINE | ID: mdl-36374386

RESUMEN

The awareness of sustainability and widespread utilization of green technologies in textile dye houses are revolutionizing not only textile industries but related fields. The current study is concerned with ultrasonic (US)-assisted utilization of extracts of Alkanna tinctoria (a source of natural alkanin dye) for wool dyeing. The extracts are obtained in various media, and both extracts and wool fabrics have been  US treated for 15-60 min. Dyeing is performed by applying variable parameters and utilizing herbal-based extracts as a source of bio-mordant, hence improving the fastness rating and enhancing color strength. Good color strength and fastness ratings are obtained using irradiated extract at 4 pH when the US-treated wool fabric is dyed at 65 °C for 60 min before and after chemical and bio-mordanting. For comparative studies, chemical mordants are also employed. In contrast to chemical mordants, the bio-mordants have made the dyeing process more sustainable with good to excellent fastness rating.


Asunto(s)
Colorantes , Lana , Animales , Textiles , Fibra de Lana , Ultrasonido
13.
Environ Sci Pollut Res Int ; 30(2): 4570-4581, 2023 Jan.
Artículo en Inglés | MEDLINE | ID: mdl-35972657

RESUMEN

The current study has been designed to observe the coloring efficacy of wild turmeric-based natural yellowish colorant for wool dyeing under microwave (MW) treatments. Extracts and fabrics have been exposed to MW treatment for up to 10 min. Surface morphology and changes in the fabric's chemical nature before and after radiation have been studied through SEM and FTIR, respectively. The results obtained after a series of experiments show that using 45 mL of aqueous extract (pH = 5) in the presence of 1.5g/100mL of table salt as an exhausting agent at 75°C for 45 min has displayed outstanding color depth (K/S) onto microwave-treated wool fabric. On applying biomordants, it has been found that acacia extract (1.5%), pomegranate (2%), and pistachio extracts (1.5%) before dyeing, whereas acacia (1%), pomegranate (1%), and pistachio extracts (2%) after dyeing, have shown colorfast shades of high strength. Comparatively, salts of Al (1.5%) and Fe (1%), and T.A (2%) before dyeing, while salts of Al (1%) and Fe (1.5%) and T.A (1.5%) after dyeing, have given the best results. Generally, it has been originated that salt of Fe (1.5%) as a post-chemical mordant and pomegranate extract (1.5%) as a post-bio-mordant have displayed wonderful color strength. It very well may be inferred that MW treatment, being naturally protected, has just superior the varying strength of colorants on wool fabric. Adding biomordants has transformed the strategy into a more sustainable one.


Asunto(s)
Colorantes , Curcumina , Animales , Curcuma , Fibra de Lana , Sales (Química) , Lana
14.
Sci Prog ; 106(3): 368504231188610, 2023.
Artículo en Inglés | MEDLINE | ID: mdl-37469182

RESUMEN

The purpose of this research is to evaluate the colouring performance of Amba Haldi-based natural extracted yellowish colour for the dyeing of wool fabric using ultrasonic (US) treatments. Before and after the US treatment, the colourant was separated in aqueous and acidic solutions for up to 60 min. Scanning electron microscopy and Fourier-transform infrared spectroscopy were used to investigate the surface morphology and chemical changes in the cloth before and after radiation. On the wool fabric that was ultrasonically treated at 75°C for 45 min, an acidic extract of Amba Haldi powder after US treatment for 20 min showed good colour depth (K/S). Acacia extract (2%), pomegranate extract (1.5%) and pistachio extract (1%), when used as pre-biomordants, were shown to have excellent colour strength. Acacia (1.5%) extract, pomegranate (2%) extract and pistachio (1.5%) extract were also used as post-biomordants. As pre-chemical mordants, Al salts (1%), Fe salts (1.5%) and tannic acid salts (2%), whereas Al salts (2%), Fe salts (1%) and tannic acid salts (2%), have produced successful results as post-chemical mordants. Overall, it was discovered that pomegranate extract (2%), used as a post-bio-mordant, and salt of Fe (1.5%), used as a post-chemical mordant, both exhibit exceptional colour strength. Ultrasonic treatment, a procedure that is harmless for the environment, has only served to increase the colour strength of dye on wool fabric, and the addition of bio-mordants has made the process more sustainable.

15.
Environ Sci Pollut Res Int ; 30(14): 42246-42254, 2023 Mar.
Artículo en Inglés | MEDLINE | ID: mdl-36645587

RESUMEN

During current times, the use of bio-colorants attained public acceptance as a sustainable alternative to synthetic ones which in turn reduced the environmental contamination. The present study focused on the green, safe, and clean technology for the resurgence of natural colorant from cocklebur (Xanthium strumarium L.) leaves and their application to cotton fabric. Natural colorants were extracted by employing an eco-friendly microwave-assisted extraction process using an aqueous and alkaline medium. Dyeing of cotton fabric was carried out using irradiated and unirradiated cotton fabric with irradiated and unirradiated natural dyes of cocklebur leaves. The results of extraction experiments revealed that 4 min microwave-assisted alkaline extract exhibited significantly outstanding color strength onto microwave-treated cotton fabric compared to aqueous one. Further to investigate the optimum dyeing conditions for cotton fabric, various dyeing variables such as dyeing time, dyeing temperature, dye concentration, and exhausting agent were monitored and found a superior result using a dye concentration of 45 ml, for dyeing cotton fabric at 75 °C for 50 min in the presence of 4 g/100 ml of table salt. For improvement in color strength and color fastness properties, the effects of various bio-mordants, such as eucalyptus bark, acacia bark, turmeric rhizome, and onion shells, and chemical mordants (aluminum and copper) on dyed cotton fabric were also evaluated. It was also observed that cotton fabric dyed with alkaline extract of cocklebur leaves using bio-mordants as pre-mordants (4% acacia, 4% eucalyptus, 2% onion) and post-mordants (3% onion, 3% eucalyptus, 4% acacia) exhibited the highest color strength and various hues with acceptable colorfastness properties against light, washing, and rubbing in comparison to chemical mordants. The ISO standard for fastness also revealed that bio-mordanting has enhanced the rating from good to excellent in comparison to chemical mordants. The results provide ample scope for the extraction of yellow natural dye from the cocklebur leaves for eco-friendly coloration of fabrics using bio-mordants.


Asunto(s)
Colorantes , Xanthium , Colorantes/química , Microondas , Hojas de la Planta , Extractos Vegetales
16.
Environ Sci Pollut Res Int ; 30(30): 74939-74951, 2023 Jun.
Artículo en Inglés | MEDLINE | ID: mdl-37209341

RESUMEN

Environment-friendly textile processing is the demand of the current global scenario, where the application of sustainable technologies such as microwave radiation has been gaining fame in all global fields due to their green and human-friendly nature. This study has been conducted to employ sustainable technology such as microwave (MW) rays for dyeing polyamide-based proteinous fabric using Acid Blue 07 dye. The fabric before and after MW treatment for up to 10 min has been dyed using an acid dye solution. Spectrophotometric analysis of the dye solution was performed before and after irradiation at a specific selected level. Using selected dyes and irradiation conditions, a series of 32 experiments using a central composite design has been employed. The shades made at selected conditions of irradiation and dyeing were assessed for colorfastness as per ISO standards. It was observed that for dyeing silk, 55 mL of Acid Blue 07 dye solution containing 1 g/100 mL salt solution at 65 °C for 55 min should be employed after MW treatment for 10 min. In comparison, for dyeing wool, 55 mL of Acid Blue 07 dye solution containing 2 g/100 mL salt solution at 65 °C for 55 min should be employed after MW treatment for 10 min. Physiochemical analysis shows that sustainable tool has not altered the chemical nature of fabric but has modified the fabric surface physically to enhance uptake ability. Colorfastness shows that the shades made have offered good resistance to fade and have given good to excellent ratings on the gray scale.


Asunto(s)
Colorantes , Seda , Animales , Humanos , Colorantes/análisis , Microondas , Fibra de Lana , Textiles/análisis , Lana/química
17.
Environ Sci Pollut Res Int ; 30(40): 92084-92094, 2023 Aug.
Artículo en Inglés | MEDLINE | ID: mdl-37479940

RESUMEN

Green products such as plant pigments in all filed are gaining fame globally due to their excellent ayurvedic and biological characteristics. In this study, microwave rays have been employed for the isolation of colorants from Anar Phali while bio-mordant have been included to get color-fast shades. The colorant was isolated in an acidic medium before and after microwave rays for 2 min. For getting darker shades with different tints, sustainable chemical and plant-based extracts as bio-mordant have been employed before and after bio coloration of wool yarn at given conditions. CIE Lab system computed in Colori-spectrophotometer (CS-410) was used to observe the change in color depth and tonal variation of dyed fabrics, and ISO standard methods have been employed to rate the colorfastness to light, washing, and rubbing at grey scale. It is concluded that microwave rays have an excellent sustainable efficacy to isolate colorant from Anar Phali powder for wool dyeing, whereas the addition of bio-mordants has made the process more sustainable and eco-friendly.


Asunto(s)
Betalaínas , Opuntia , Animales , Colorantes , Extractos Vegetales , Lana
18.
Sci Prog ; 106(4): 368504231215593, 2023.
Artículo en Inglés | MEDLINE | ID: mdl-37993993

RESUMEN

This research investigates the viability of using Syzygium aromaticum (clove) as a natural dye for wool yarn through the application of microwave treatment and optimization using central composite design (CCD). As concerns grow over the environmental impact of synthetic dyes and their detrimental disposal in water bodies, the search for eco-friendly alternatives becomes imperative to revolutionize the textile industry. Microwave-assisted extraction of the colorant from clove powder is explored as an efficient and sustainable method, minimizing solvent usage and energy consumption compared to conventional techniques. To enhance colorfastness properties while eliminating the need for toxic mordants, green alternatives such as Al, Fe, and tannic acid, combined with plant phenolics from red sumac, pomegranate rind, and weld, are employed. According to the analysis of CCD, the higher color strength value 18.1653 was achieved using pH = 3, time = 50 min, temperature = 70 °C, and salt concentration = 1.5 g/100 mL. The optimized dyeing conditions also showed a maximum level of colorfastness properties of 5 for light, 5 for wash, 5 for dry rubbing, and 4 for wet rubbing. The findings from Fourier-transform infrared spectroscopy and scanning electron microscopy analyses provide valuable insights into the chemical and morphological changes induced by microwave treatment and dyeing with clove extract. The results affirm the presence of eugenol as a potential active molecule responsible for the captivating color of clove flower buds, validating its suitability as a natural dye source for wool. This study highlights the promising potential of microwave-assisted extraction and plant-based biomolecules as innovative and environmentally friendly approaches in natural dyeing, paving the way for a more sustainable future in the textile industry. Embracing these eco-friendly practices allows the textile sector to reduce its ecological footprint and contribute to a cleaner and greener environment. Further research and implementation of these techniques can foster a more harmonious coexistence with nature, ensuring a healthier ecosystem for all.


Asunto(s)
Syzygium , Lana , Animales , Colorantes/química , Colorantes/farmacología , Syzygium/química , Microondas , Ecosistema
19.
Environ Sci Pollut Res Int ; 30(8): 21863-21871, 2023 Feb.
Artículo en Inglés | MEDLINE | ID: mdl-36279062

RESUMEN

For the current study, Bougainvillea flowers as environment friendly sustainable source of plant-based natural dye have been selected as an alternative to toxic synthetic dyes for dyeing of cotton and silk. Natural colorant from Bougainvillea flowers (Bougainvillea glabra) was extracted using aqueous and acidic extraction media. Maximum colorant was extracted in aqueous medium, and further it was used for cotton and silk dyeing. The optimum values of the dyeing parameters including dyeing time, dye to liquor ratio and salt level as exhausting agent were found to be 30 min, 35-mL liquor ratio and 3.0 g for cotton and for silk 45 min dyeing time, 45-mL liquor ratio and 3.0 g exhausting agent in aqueous dye extract. Bio mordanting has been applied to attain a variety of color shades. The utilization of 3% of henna, 4% of turmeric for silk pre-mordanting and for post-mordanting turmeric at 3% and henna at 4% for silk gave a darker shade. For cotton bio mordanting, 2% turmeric rhizome powder, 3% henna leaves powder extract as pre-mordant and 2% turmeric, 3% henna as post-mordant has developed a variety of shade. Overall, it has been found that natural colorant from Bougainvillea flowers is the new dye source for bio-coloration of natural fabrics, and addition of bio mordants has made the process more calming and eco-friendly.


Asunto(s)
Nyctaginaceae , Seda , Colorantes , Industria Textil , Polvos , Extractos Vegetales , Flores
20.
Environ Sci Pollut Res Int ; 30(5): 12453-12465, 2023 Jan.
Artículo en Inglés | MEDLINE | ID: mdl-36112291

RESUMEN

The world's move towards revival of eco-labelled products has created a huge urge to explore new means which are healthier for the global community. Among such means, plant-based bio-pigments for coloration of matrix are gaining worldwide fame, particularly in the textile sector. For the purpose of appraising new source of eco-friendly dyes, using microwave irradiation techniques, Coral Jasmine flowers have been explored for the bio-dyeing of wool. The colorant was extracted in acidic medium owing to nature of fabric, and both stuffs have been exposed to microwave treatment up to 5 min. Bio-coloration of MW irradiated and unirradiated wool was done using MW irradiated and unirradiated extract for observing high yield. Central composite design (CCD) as statistical method was utilized to see the significance of dyeing parameters chosen for mordanting to develop colorfast shades. Different concentrations of sustainable chemicals and bio-mordants as per weight of fabric were employed to introduce new shades with improved colorfastness properties. International standard textile methods determining shade permanency (fastness) have been employed onto selected dyed-mordanted fabrics. Good yield of colorant was observed when MW irradiated wool fabric was dyed at 75 °C for 45 min with extract of 7 pH, having 1.5g/100 mL of salt solution; the promising color yield was observed. As per gray scale ratings observed after ISO standard methods, pine nut as bio-mordant and iron salt as chemical mordant have developed colorfast shades. Conclusively, it can be recommended that methods for the isolation of colorants from new dye yielding plants, MW heating method as suitable clean technology and medicinal-based bio-mordants should be employed for getting permanent gamutes.


Asunto(s)
Jasminum , Lana , Animales , Lana/química , Colorantes/química , Flores , Extractos Vegetales/química
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