Trace detection of cadmium (II) ions based on an excessively tilted fiber grating.

Cadmium (Cd2+) ion is one of the most crucial industrial pollutants that cause serious harm to the human body. We proposed and experimentally demonstrated a highly sensitive Cd2+ sensor based on hydrogel coated excessively tilted fiber grating. The hydrogel with the functional monomer of the allyl thiourea can specifically bind to Cd2+, and hence forming a complex. The grating excites high order cladding modes, and ensures a sufficient interaction between the light and hydrogel binding to Cd2+, providing highly sensitive monitoring. The results show that the sensor can detect 0-160 pM Cd2+ in aqueous solution. The maximum sensitivity is 10600 nm/µM, and the minimum detection concentration is 20 pM (about 0.004 ppb), which is much less than that of the international standard (3 ppb). The proposed sensor exhibits high sensitivity, ultra-low detection limit, specificity, and a compact structure, offering potential as a tool for Cd2+ detection in aqueous solution.

Sub-millimeter resolution and high-precision φ-OFDR using a complex-domain denoising method.

Phase noise is one of the main obstacles to achieve high spatial resolution, high precision, and large measurement range in φ-OFDR. Here, we proposed a complex-domain denoising method to achieve unwrapping of phase signals. In this method, the wrapped phase was used to construct a complex signal, and then both real and imaginary parts are denoised by using a wavelet packet. The two sets of denoised signals are reconstructed into a complex form, allowing to obtain an unwrapped phase. Additionally, the spatial position correction algorithm addresses the phase decoherence from strain accumulation. Finally, a high numerical aperture optical fiber is used to enhance the Rayleigh scattering intensity by 15 dB. The comprehensive approach yields remarkable results: a sensing resolution of 0.89 mm, a root mean square error of 1.5 µÎµ, and a maximum strain sensing capability of 2050 µÎµ.

Acousto-optic reconfigurable filter based on vector mode fusion in dispersion-compensating fiber.

An acousto-optic reconfigurable filter (AORF) is proposed and demonstrated based on vector mode fusion in dispersion-compensating fiber (DCF). With multiple acoustic driving frequencies, the resonance peaks of different vector modes in the same scalar mode group can be effectively fused into a single peak, which is utilized to obtain arbitrary reconfiguration of the proposed filter. In the experiment, the bandwidth of the AORF can be electrically tuned from 5 nm to 18 nm with superposition of different driving frequencies. The multi-wavelength filtering is further demonstrated by increasing the interval of the multiple driving frequencies. The bandpass/band-rejection can also be electrically reconfigured by setting the combination of driving frequencies. The proposed AORF gains the feature of reconfigurable filtering types, fast and wide tunability, and zero frequency shift, which is advantageous for high-speed optical communication networks, tunable lasers, fast optical spectrum analyzing and microwave photonics signal processing.

High-performance distributed dynamic strain sensing by synthesizing φ-OTDR and BOTDR.

We propose and demonstrate a high-performance distributed dynamic absolute strain sensing technique by synthesizing φ-OTDR and BOTDR. The technique synthesizes the relative strain obtained by the φ-OTDR part and the initial strain offset estimated by fitting the relative strain with the absolute strain signal from the BOTDR part. As a result, it provides not only the characteristics of high sensing accuracy and high sampling rate like φ-OTDR, but also the absolute strain measurement and the large sensing dynamic range like BOTDR. The experiment results indicate the proposed technique can realize the distributed dynamic absolute strain sensing with a sensing dynamic range of over 2500 µÉ›, a peak-to-peak amplitude of 1165 µÉ›, and a wide frequency response range from 0.1 to over 30 Hz over a sensing range of about 1 km.

High-spatial-resolution distributed acoustic sensor based on the time-frequency-multiplexing OFDR.

We proposed and experimentally demonstrated a high-spatial-resolution distributed acoustic sensor based on time-frequency-multiplexing (TFM) optical frequency domain reflectometry (OFDR). The TFM technique enhances the frequency response of OFDR by multiplexing the time-frequency channels and suppresses the crosstalk in the meantime. Phase demodulation is employed to achieve high sensitivity, and the impact of end effect in OFDR is studied and suppressed by a dedicated linear interpolation. In the results, a 10.5 kHz vibration is measured with 22 cm spatial resolution and 20 dB signal-to-noise ratio on a 1 km fiber. By adjusting the parameters, the system also shows a good DAS performance on a 33 kHz vibration with up to 200 kHz sampling rate.

Optical Frequency Domain Reflectometry Based on Multilayer Perceptron.

We proposed an optical frequency domain reflectometry based on a multilayer perceptron. A classification multilayer perceptron was applied to train and grasp the fingerprint features of Rayleigh scattering spectrum in the optical fiber. The training set was constructed by moving the reference spectrum and adding the supplementary spectrum. Strain measurement was employed to verify the feasibility of the method. Compared with the traditional cross-correlation algorithm, the multilayer perceptron achieves a larger measurement range, better measurement accuracy, and is less time-consuming. To our knowledge, this is the first time that machine learning has been introduced into an optical frequency domain reflectometry system. Such thoughts and results would bring new knowledge and optimization to the optical frequency domain reflectometer system.

Distributed pH sensing based on hydrogel coated single mode fibers and optical frequency domain reflectometry.

We propose a distributed pH sensor based on an optical frequency domain reflectometry using a PEGDA-based pH-sensitive hydrogel coated on a single mode fiber. The volume of hydrogel increased as pH value of the surrounding fluid decreased, which converts the pH value to the axial strain in the fiber. Taking capacity of distributed strain measurement with high spatial resolution in optical frequency domain reflectometry, the pH value of the external medium is distributed measured by the wavelength shifts of the local Rayleigh backscattering spectra. The basic hydrogel with different molecular weight was optimized to balance the sensitivity, the response time and also the stability. In the experiment, the range of the pH value from 2 to 6 was measured with a sampling resolution of 1.7 mm, a sensitivity of -199 pm/pH and a response time of 14 min when the hydrogel coating diameter is 2 mm. Such a distributed pH sensing system has a potential to detect and locate some chemical or biological substances in a large-scale environment.

Enhancing spatial resolution of BOTDR sensors using image deconvolution.

We propose to employ the image deconvolution technique for Brillouin optical time domain reflectometry (BOTDR) systems to achieve a flexible and enhanced spatial resolution with pump pulses longer than phonon lifetime. By taking the measured Brillouin gain spectrum (BGS) distribution as an image blurred by a point spread function (PSF), the image deconvolution algorithm based on the two-dimensional Wiener filtering can mitigate the ambiguity effect on the Brillouin response. The deconvoluted BGS distribution reveals detailed sensing information within shorter fiber segments, improving the inferior spatial resolution and simultaneously maintaining other sensing performance parameters. Thanks to the proposed technique, a typical BOTDR sensor with 40 ns pump pulses reaches a submetric spatial resolution as high as 10 cm. Compared to the differential-spectrum-based BOTDR retrieving the same spatial resolution, the image deconvolution technique shows advantages in system complexity and measurement uncertainty. Moreover, the proposed technique is promising to improve the spatial resolution of other distributed optical fiber sensing (DOFS) techniques such as BOTDR systems with complex pump modulation methods.

Ultra-narrow linewidth vertical-cavity surface-emitting laser based on external-cavity weak distributed feedback.

We demonstrate an ultra-narrow linewidth vertical-cavity surface-emitting laser (VCSEL) based on external-cavity weak distributed feedback from Rayleigh backscattering (RBS). A single longitudinal mode VCSEL with the linewidth as narrow as 435 Hz and a contrast of 55 dB are experimentally achieved by RBS fiber with a feedback level of RBS signal of -27.6 dB. By adjusting the thermal resistance of the VCSEL from 4.5 kΩ to 7.0 kΩ, the laser wavelength can be tuned from 1543.324 nm to 1542.06 nm with a linear tuning slope of -0.506 nm/kΩ. In the tuning process, the linewidth fluctuates in the range of 553-419 Hz.

Tens of hertz ultra-narrow linewidth fiber ring laser based on external weak distributed feedback.

We suggest and demonstrate a single-frequency fiber ring laser with an ultra-narrow linewidth based on an external weak distributed feedback. A π phase-shifted fiber Bragg grating (PSFBG) is used to improve mode selection and enable single-longitudinal mode (SLM) laser operation. The linewidth is then further strongly compressed using a signal generated by a weak distributed feedback structure (WDFS) and injected into the main laser cavity to suppress spontaneous emission. The resulting ultra-narrow linewidth fiber ring laser achieves a side-mode suppression ratio (SMSR) of ∼72 dB, and low white frequency noise of ∼10.3 Hz2/Hz, which correspond to an instantaneous linewidth of ∼32.3 Hz in the normal operating condition of the laser. Our linewidth compression mechanism not only solves the problems associated with deep linewidth compression in long-cavity fiber laser, but also fosters the development of practical and reliable all-fiber structures. Our laser source is characterized by low cost, high coherence, and low noise, which are highly desirable features in coherent optical detection, high-resolution spectrometers, microwave photonics, and optical sensing.

Ultra-narrow-linewidth DFB laser array based on dual-cavity feedback.

Herein, we propose a structure to simultaneously compress the distributed feedback (DFB) laser array's linewidth. The proposed structure is meticulously designed to ensure single longitudinal mode operation via the interference phenomenon between the laser's primary cavity and the dual-cavity feedback. Given the weak feedback effect for each wavelength in the laser array, the proposed structure could realize the intense compression of the laser linewidths. The study results show that the side-mode suppression ratios of each DFB laser are over 40 dB, and the linewidths have been compressed from 3 MHz to ∼800 Hz. Thus, we believe the idea of an overall compression linewidth scheme in the present study can be adopted for integrated laser arrays.

Control of polarization switching in a VCSEL via resonant feedback from a whispering-gallery-mode cavity.

We report a method for flexibly switching the dominant polarization of a vertical-cavity surface-emitting laser (VCSEL) by introducing polarization-resolved resonant optical feedback from a whispering-gallery-mode (WGM) cavity to the lasing cavity. Switching between the originally dominant mode and a side mode is experimentally demonstrated under different bias currents once one of them is locked to the resonance mode of the WGM cavity. In addition to a controllable polarization state, the reported VCSEL also demonstrates a linewidth as narrow as tens of kilohertz, which is highly desirable for many applications, including high-speed data communication, light detection and ranging (lidar), and absorption spectroscopy.

Ion-Imprinted Chitosan-Based Localized Surface Plasmon Resonance Sensor for Ni2+ Detection.

Heavy metals are important sources of environmental pollution and cause disease in organisms throughout the food chain. A localized surface plasmon resonance sensor was proposed and demonstrated to realize Ni2+ detection by using ion-imprinted chitosan. Au nanoparticles were coated on the multimode fiber to excite the local surface plasmon resonance, and Ni2+-imprinted chitosan was then functionalized by using the dip coating technique. Ethylene diamine tetra-acetic acid was used to release the Ni2+ ions and hence form countless voids. Ni2+ was refilled into the voids to increase the refractive index of the sensing material, thus realizing the measurement of Ni2+ by monitoring the wavelength shift in the localized surface plasmon resonant peak. The coating thickness of the Ni2+-chitosan gel was optimized to obtain greater sensitivity. Experimental results show that the proposed Ni2+ sensor has a sensitivity of 185 pm/µM, and the limit of detection is 0.512 µM. The comparison experiments indicated that the ion-imprinted chitosan has better selectivity than pure chitosan.

High-Resolution and Large-Sensing-Range Liquid-Level Sensor Based on Optical Frequency Domain Reflectometry and No-Core Fiber.

Liquid-level sensors are required in modern industrial and medical fields. Optical liquid-level sensors can solve the safety problems of traditional electrical sensors, which have attracted extensive attention in both academia and industry. We propose a distributed liquid-level sensor based on optical frequency domain reflectometry and with no-core fiber. The sensing mechanism uses optical frequency domain reflectometry to capture the strong reflection of the evanescent field of the no-core fiber at the liquid-air interface. The experimental results show that the proposed method can achieve a high resolution of 0.1 mm, stability of ±15 µm, a relatively large measurement range of 175 mm, and a high signal-to-noise ratio of 30 dB. The sensing length can be extended to 1.25 m with a weakened signal-to-noise ratio of 10 dB. The proposed method has broad development prospects in the field of intelligent industry and extreme environments.

Submetric Spatial Resolution ROTDR Temperature Sensor Assisted by Wiener Deconvolution.

A submetric spatial resolution Raman optical time-domain reflectometry (ROTDR) temperature sensor assisted by the Wiener deconvolution postprocessing algorithm has been proposed and experimentally demonstrated. Without modifying the typical configuration of the ROTDR sensor and the adopted pump pulse width, the Wiener demodulation algorithm is able to recover temperature perturbations of a smaller spatial scale by deconvoluting the acquired Stokes and anti-Stokes signals. Numerical simulations have been conducted to analyze the spatial resolution achieved by the algorithm. Assisted by the algorithm, a typical ROTDR sensor adopting pump pulses of 20 ns width can realize the distributed temperature sensing with a spatial resolution of 0.5 m and temperature accuracy of 1.99 °C over a 2.1-km sensing fiber.

Intensity-modulated bend sensor by using a twin core fiber: theoretical and experimental studies.

A new optical fiber bend sensor is proposed and demonstrated based on a sandwich structure created by splicing a segment of twin core fiber (TCF) between two segments of single mode fibers (SMFs). One core of the TCF is aligned with the cores of two segments of SMFs. An incident beam is directed into the TCF by the lead-in SMF. Light couples back and forth between two cores. The bend sensing performance of the sensor is investigated by intensity-modulated method. The intensity of the operation wavelength is modulated by the change of refractive index and geometrical deformation in the bent TCF. Experimental results show such a bend sensor achieves sensitivity of +0.671 /m-1 and resolution of 0.003 m-1 in the range of 0 to 1.25 m-1. In addition, the sensitivity and bend measurement range can be flexibly adjusted through selection of the length of TCF and sensing configuration. As such, the proposed sensor can be further developed for large or small bend ranges measurement.

Vector optical-chirp-chain Brillouin optical time-domain analyzer based on complex principal component analysis.

A vector optical-chirp-chain (OCC) Brillouin optical time-domain analyzer (BOTDA) based on complex principal component analysis (CPCA) is proposed and experimentally demonstrated by employing a four-tone OCC probe with two orthogonal polarization states. The polarization-fading-free complex Brillouin spectrum (CBS) of the vector OCC-BOTDA is obtained by combining the amplitude and phase response spectra of the probe wave at both Brillouin gain and loss region. We utilize the CPCA method to determine the Brillouin frequency shift (BFS) directly using the measured CBS, and the sensing accuracy is improved by a factor of up to 1.4. The distributed temperature sensing is demonstrated over a 20 km standard single-mode fiber with a 6 m spatial resolution and less than 1 MHz frequency uncertainty under 10 times of trace averaging.

Distributed directional torsion sensing based on an optical frequency domain reflectometer and a helical multicore fiber.

We propose and experimentally demonstrate a distributed directional torsion sensor based on an optical frequency domain reflectometer (OFDR) using a helical multicore fiber (MCF). A theoretical model is first established to reveal that the ability of the torsion direction discrimination stems from the fiber design of the central-offset cores with helical structure and the shorter helical pitch holds higher sensitivity. Such a distributed torsion sensor is then experimentally realized by using an OFDR system with an adjacent sensing distance of 9.4 mm. Comparative experiments with three different MCFs fully prove the theoretical predication. Finally, a distributed directional torsion sensor is realized with a linear sensitivity of 1.9 pm/(rad/m) by using the helical MCF with a helical pitch of 6 mm. Such a torsion sensing system would find potential applications in the fields of bionic robotics, 3-D shape sensing, oil drilling and so on.

A fluorometric optical fiber nanoprobe for copper(II) by using AgInZnS quantum dots.

An optical fiber nanoprobe is presented for fluorometric determination of copper(II). The method based on the use of water-dispersible AgInZnS quantum dots (QDs) deposited at the end of an optical fiber in a poly(vinyl alcohol) matrix. The fluorescnece of the QDs, best measured at excitation/emisssion wavelengths of 365/570 nm, is quenched by Cu(II) due to both static and electron transfer from the QDs to Cu(II). This is experimentally confirmed by photoluminescence and UV-vis absorption spectra, and measurement of luminescence lifetimes. The probe is highly selective and possesses a linear detection range that extends from 2.5 to 800 nM. Graphical abstractSchematic representation of an optical fiber nanoprobe based on hydrophilic AgInZnS quantum dots for fluorometric determination of copper(II). The fluorescence is quenched by Cu(II) due to static quenching and dynamic quenching. It has a detection range of 2.5-800 nM.

Nonlinear Hydraulic Pressure Response of an Improved Fiber Tip Interferometric High-Pressure Sensor.

We demonstrate a silica diaphragm-based fiber tip Fabry-Perot interferometer (FPI) for high-pressure (40 MPa) sensing. By using a fiber tip polishing technique, the thickness of the silica diaphragm could be precisely controlled and the pressure sensitivity of the fabricated FPI sensor was enhanced significantly by reducing the diaphragm thickness; however, the relationship between the pressure sensitivity and diaphragm thickness is not linear. A high sensitivity of -1.436 nm/MPa and a linearity of 0.99124 in hydraulic pressure range of 0 to 40 MPa were demonstrated for a sensor with a diaphragm thickness of 4.63 µm. The achieved sensitivity was about one order of magnitude higher than the previous results reported on similar fiber tip FPI sensors in the same pressure measurement range. Sensors with a thinner silica diaphragm (i.e., 4.01 and 2.09 µm) rendered further increased hydraulic pressure sensitivity, but yield a significant nonlinear response. Two geometric models and a finite element method (FEM) were carried out to explain the nonlinear response. The simulation results indicated the formation of cambered internal silica surface during the arc discharge process in the fiber tip FPI sensor fabrication.