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1.
J Esthet Restor Dent ; 2024 Sep 03.
Artigo em Inglês | MEDLINE | ID: mdl-39228147

RESUMO

OBJECTIVE: The purpose of this in vitro study was to evaluate the effect of staining, glazing, and polishing on the survival probability of monolithic crowns manufactured with preshaded stabilized zirconia with 5 mol% of yttrium oxide (5Y-TZP). MATERIALS AND METHODS: Monolithic crowns in the shape of an upper canine (1.5 mm of thickness) were manufactured by CAD/CAM, adhesively cemented on metallic foundation, and divided into 6 groups (n = 21): C (control), S (staining), G (glazing), P (polishing), SG (staining and glazing), and SP (staining and polishing). The survival probability was determined by step-stress accelerated life testing with a load applied to the palatine concavity of the crown. First, the specimens were subjected to a single-load to fracture test (SLF) and next to the fatigue test (5 Hz, thermocycling immersed in water varying 5-55°C), including the light (n = 9), moderate (n = 6), and aggressive (n = 3) loading profiles (load ranged between 20% and 60% of SLF). The survival probability was calculated considering the cycles for failure (CFF) and fatigue failure load (FFL) and illustrated using a Kaplan-Meier graph. The comparison among groups was performed using a Log-Rank test (α = 0.05). RESULTS: The mean value of SLF was 586.7 N. There was no difference among groups in survival probability, considering CFF and FFL. CONCLUSION: Staining, glazing, and polishing can be performed safely without damaging the mechanical behavior of 5Y-TZP monolithic crowns. CLINICAL SIGNIFICANCE: Staining is used to characterize and improve the esthetic of zirconia monolithic crowns. It can be used to reproduce the color gradient in the cervical region of the crown and pigmented grooves. This study showed that staining, glazing, and polishing did not affect the survival probability and the use of finishing procedures (glazing or polishing) after staining did not improve the survival probability of zirconia monolithic crowns.

2.
Entropy (Basel) ; 24(10)2022 Oct 01.
Artigo em Inglês | MEDLINE | ID: mdl-37420425

RESUMO

In this paper, we discuss the statistical analysis of a simple step-stress accelerated competing failure model under progressively Type-II censoring. It is assumed that there is more than one cause of failure, and the lifetime of the experimental units at each stress level follows exponential distribution. The distribution functions under different stress levels are connected through the cumulative exposure model. The maximum likelihood, Bayesian, Expected Bayesian, and Hierarchical Bayesian estimations of the model parameters are derived based on the different loss function. Based on Monte Carlo Simulations. We also get the average length and the coverage probability of the 95% confidence intervals and highest posterior density credible intervals of the parameters. From the numerical studies, it can be seen that the proposed Expected Bayesian estimations and Hierarchical Bayesian estimations have better performance in terms of the average estimates and mean squared errors, respectively. Finally, the methods of statistical inference discussed here are illustrated with a numerical example.

3.
Luminescence ; 29(7): 933-7, 2014 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-24677412

RESUMO

In order to obtain reliability information for a white organic light-emitting diode (OLED), two constant and one step stress tests were conducted with its working current increased. The Weibull function was applied to describe the OLED life distribution, and the maximum likelihood estimation (MLE) and its iterative flow chart were used to calculate shape and scale parameters. Furthermore, the accelerated life equation was determined using the least squares method, a Kolmogorov-Smirnov test was performed to assess if the white OLED life follows a Weibull distribution, and self-developed software was used to predict the average and the median lifetimes of the OLED. The numerical results indicate that white OLED life conforms to a Weibull distribution, and that the accelerated life equation completely satisfies the inverse power law. The estimated life of a white OLED may provide significant guidelines for its manufacturers and customers.


Assuntos
Luz , Compostos Orgânicos/química , Análise dos Mínimos Quadrados , Iluminação , Software
4.
Math Biosci Eng ; 20(12): 21407-21431, 2023 Dec 01.
Artigo em Inglês | MEDLINE | ID: mdl-38124603

RESUMO

In this paper, a new generalization of the one parameter Rayleigh distribution called the Power Rayleigh (PRD) was employed to model the life of the tested units in the step-stress accelerated life test. Under progressive Type-I interval censored data, the cumulative exposure distribution was considered to formulate the life model, assuming the scale parameter of PRD has the inverse power function at each stress level. Point estimates of the model parameters were obtained via the maximum likelihood estimation method, while interval estimates were obtained using the asymptotic normality of the derived estimators and the bootstrap resampling method. An extensive simulation study of $ k = 4 $ levels of stress in different combinations of the life test under different progressive censoring schemes was conducted to investigate the performance of the obtained point and interval estimates. Simulation results indicated that point estimates of the model parameters are closest to their initial true values and have relatively small mean squared errors. Accordingly, the interval estimates have small lengths and their coverage probabilities are almost convergent to the 95% significance level. Based on the Fisher information matrix, the D-optimality and the A-optimality criteria are implemented to determine the optimal design of the life test by obtaining the optimum inspection times and optimum stress levels that improve the estimation procedures and give more efficient estimates of the model parameters. Finally, the developed inferential procedures were also applied to a real dataset.

5.
Math Biosci Eng ; 20(2): 1674-1694, 2023 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-36899503

RESUMO

This article discusses the problem of estimation with step stress partially accelerated life tests using Type-II progressively censored samples. The lifetime of items under use condition follows the two-parameters inverted Kumaraswamy distribution. The maximum likelihood estimates for the unknown parameters are computed numerically. Using the property of asymptotic distributions for maximum likelihood estimation, we constructed asymptotic interval estimates. The Bayes procedure is used to calculate estimates of the unknown parameters from symmetrical and asymmetric loss functions. The Bayes estimates cannot be obtained explicitly, therefor the Lindley's approximation and the Markov chain Monte Carlo technique are used to obtaining the Bayes estimates. Furthermore, the highest posterior density credible intervals for the unknown parameters are calculated. An example is presented to illustrate the methods of inference. Finally, a numerical example of March precipitation (in inches) in Minneapolis failure times in the real world is provided to illustrate how the approaches will perform in practice.

6.
J Appl Stat ; 49(13): 3344-3360, 2022.
Artigo em Inglês | MEDLINE | ID: mdl-36225269

RESUMO

In this paper, we consider a two-stage sequential estimation procedure to estimate the parameters of a cumulative exposure model under an accelerated testing scenario. In particular, we focus on a step-stress model where the stress level changes after a pre-specified number of failures occur, which is also random. This is termed as a 'random stress change time' in the literature. We further aim to estimate these parameters using maximum precision and hence use a certain variance optimality criteria. Our proposed two-stage estimation procedures follow interesting efficiency properties and their applicability is seen through extensive simulation analyses and a pseudo-real data example from reliability studies.

7.
Polymers (Basel) ; 15(1)2022 Dec 29.
Artigo em Inglês | MEDLINE | ID: mdl-36616506

RESUMO

Compared with the constant stress accelerated aging test, the step stress accelerated aging test reduces the accelerated aging test time by increasing the aging temperature step by step to obtain the aging failure life of rubber in a shorter time, but its data processing method is not mature enough. In this paper, a simplified step is proposed to process the step stress accelerated aging data. The identification of the acceleration factor is transformed into an optimization problem to avoid the error accumulation problem caused by fitting the data at each temperature. Considering the non-Arrhenius phenomenon in the rubber aging process, a modified Arrhenius equation was used to extrapolate the acceleration factor at low temperatures to calculate the prediction curves for the degradation of polyurethane rubber properties at low temperatures. The life prediction results of the constant stress accelerated aging test and step stress accelerated aging test were compared, and the dispersion coefficient between the two results was between 0.9 and 1. The results obtained by the two methods were in good agreement, which proved the correctness and feasibility of the method used in this paper.

8.
Math Biosci Eng ; 19(10): 9773-9791, 2022 07 08.
Artigo em Inglês | MEDLINE | ID: mdl-36031968

RESUMO

The procedure of selecting the values of hyper-parameters for prior distributions in Bayesian estimate has produced many problems and has drawn the attention of many authors, therefore the expected Bayesian (E-Bayesian) estimation method to overcome these problems. These approaches are used based on the step-stress acceleration model under the Exponential Type-I hybrid censored data in this study. The values of the distribution parameters are derived. To compare the E-Bayesian estimates to the other estimates, a comparative study was conducted using the simulation research. Four different loss functions are used to generate the Bayesian and E-Bayesian estimators. In addition, three alternative hyper-parameter distributions were used in E-Bayesian estimation. Finally, a real-world data example is examined for demonstration and comparative purposes.


Assuntos
Teorema de Bayes , Simulação por Computador
9.
J Adv Prosthodont ; 13(6): 385-395, 2021 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-35003554

RESUMO

PURPOSE: To characterize the microstructure of three yttria partially stabilized zirconia ceramics and to compare their hardness, indentation fracture resistance (IFR), biaxial flexural strength (BFS), and fatigue flexural strength. MATERIALS AND METHODS: Disc-shaped specimens were obtained from 3Y-TZP (Vita YZ HT), 4Y-PSZ (Vita YZ ST) and 5Y-PSZ (Vita YZ XT), following the ISO 6872/2015 guidelines for BFS testing (final dimensions of 12 mm in diameter, 0.7 and 1.2 ± 0.1 mm in thicknesses). Energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD) and scanning electron microscopy (SEM) analyses were performed, and mechanical properties were assessed by Vickers hardness, IFR, quasi-static BFS and fatigue tests. RESULTS: All ceramics showed similar chemical compositions, but mainly differed in the amount of yttria, which was higher as the amount of cubic phase in the diffractogram (5Y-PSZ > 4Y-PSZ > 3Y-TZP). The 4Y- and 5Y-PSZ specimens showed surface defects under SEM, while 3Y-TZP exhibited greater grain uniformity on the surface. 5Y-PSZ and 3Y-TZP presented the highest hardness values, while 3Y-TZP was higher than 4Y- and 5Y-PSZ with regard to the IFR. The 5Y-PSZ specimen (0.7 and 1.2 mm) showed the worst mechanical performance (fatigue BFS and cycles until failure), while 3Y-TZP and 4Y-PSZ presented statistically similar values, higher than 5Y-PSZ for both thicknesses (0.7 and 1.2 mm). Moreover, 3Y-TZP showed the highest (1.2 mm group) and the lowest (0.7 mm group) degradation percentage, and 5Y-PSZ had higher strength degradation than 4Y-PSZ group. CONCLUSION: Despite the microstructural differences, 4Y-PSZ and 3Y-TZP had similar fatigue behavior regardless of thickness. 5Y-PSZ had the lowest mechanical performance.

10.
Dent Mater ; 37(5): 875-881, 2021 05.
Artigo em Inglês | MEDLINE | ID: mdl-33715863

RESUMO

OBJECTIVE: Continuous efforts have been made to hasten the zirconia densification process without compromising properties. This study evaluated the long-term structural durability of microwave speed-sintered zirconia (MWZ) relative to a conventionally sintered zirconia (CZ). METHODS: As-machined dental 3Y-TZP discs (Ø12 × 1.2 mm) were speed sintered at 1450 °C for 15 min using an industrial microwave oven, while conventional sintering was conducted in a standard dental furnace at 1530 °C for 2 h. Both were followed by natural cooling. The total sintering time was 105 min for MWZ and 600 min for CZ. Groups were compared regarding density, grain size, phase composition, and fracture resistance. Structural durability was investigated employing two fatigue protocols, step-stress and dynamic fatigue. RESULTS: Compared to CZ, MWZ exhibited a slightly lower density (MWZ = 5.98 g/cm3, CZ = 6.03 g/cm3), but significantly smaller grain sizes (MWZ = 0.53 ± 0.09 µm, CZ = 0.89 ± 0.10 µm), lower cubic-zirconia contents (MWZ = 15.3%, CZ = 22.7%), and poorer translucency properties (TP) (MWZ = 13 ± 1, CZ = 29 ± 0.8). However, the two materials showed similar flexural strength (MWZ = 978 ± 112 MPa, CZ = 1044 ± 161 MPa). Additionally, step-stress testing failed to capture the fatigue effect in 3Y-TZP, whereas dynamic fatigue revealed structural degradation due to moisture-assisted slow-crack-growth (SCG). Finally, MWZ possessed a slightly higher Weibull modulus (MWZ = 7.9, CZ = 6.7) but similar resistance to SCG (MWZ = 27.5, CZ = 24.1) relative to CZ. SIGNIFICANCE: Dental 3Y-TZP with similar structural durability can be fabricated six-times faster by microwave than conventional sintering.


Assuntos
Materiais Dentários , Ítrio , Teste de Materiais , Micro-Ondas , Propriedades de Superfície , Tecnologia , Zircônio
11.
J Mech Behav Biomed Mater ; 113: 104091, 2021 01.
Artigo em Inglês | MEDLINE | ID: mdl-33032009

RESUMO

The aim of the study was to compare the outcomes for the fatigue mechanical behavior of bonded simplified lithium disilicate restorations, with and without an internal adjustment by grinding with diamond bur in running two fatigue tests: Staircase and Step-stress testing approaches. Ceramic discs (IPS e.max CAD) were prepared (Ø = 10 mm; thickness = 1.0 mm), submitted to an in-lab simulation of CAD/CAM milling (#60 SiC paper) and allocated into 2 groups according to the internal adjustment by grinding of the cementation surface: no adjustment (CTRL); or grinding with a coarse diamond bur (GR). Adhesive cementation (Multilink N) was performed onto epoxy resin discs (Ø = 10 mm; thickness = 2 mm) after ceramic/epoxy surface treatments. The cemented assemblies of each group were randomly assigned into 2 subgroups considering two fatigue tests (n = 15): Staircase - SC (250,000 cycles; 20 Hz), or Step-stress - SS (10,000 cycles per step; 20 Hz). Roughness, topographic and fractographic analyses were additionally performed. Statistical analyses were carried out using the Dixon and Mood method for Staircase data, and Kaplan-Meier and Mantel-Cox (log-rank) tests for Step-stress data. Ceramic restorations having its intaglio surface ground (GR group: SC test = 306.67 N; SS test = 646.67 N) presented lower fatigue failure load (FFL) values than the CTRL group (SC test = 879.28 N; SS test = 1090.00 N), regardless of the fatigue testing approach. The percentage of mean FFL decrease comparing the CTRL to GR group was higher for SC (65.1%) than the SS (40.7%) approach. However, a different total number of cycles was applied for each method. Both fatigue tests were able to detect the negative effect of internal adjustments of lithium disilicate glass-ceramic simplified restorations on their mechanical behavior. Therefore, both methods can be applied for similar evaluations (fatigue testing for ceramic restorations).


Assuntos
Cerâmica , Porcelana Dentária , Desenho Assistido por Computador , Falha de Restauração Dentária , Análise do Estresse Dentário , Teste de Materiais , Propriedades de Superfície
12.
J Appl Stat ; 48(4): 623-645, 2021.
Artigo em Inglês | MEDLINE | ID: mdl-35706988

RESUMO

In this paper, a multiple step-stress model is designed and analyzed when the data are Type-I censored. Lifetime distributions of the experimental units at each stress level are assumed to follow a two-parameter Weibull distribution. Further, distributions under each of the stress levels are connected through a tampered failure-rate based model. In a step-stress experiment, as the stress level increases, the load on the experimental units increases and hence the mean lifetime is expected to be shortened. Taking this into account, the aim of this paper is to develop the order restricted inference of the model parameters of a multiple step-stress model based on the frequentist approach. An extensive simulation study has been carried out and two real data sets have been analyzed for illustrative purposes.

13.
J Mech Behav Biomed Mater ; 108: 103831, 2020 08.
Artigo em Inglês | MEDLINE | ID: mdl-32469725

RESUMO

OBJECTIVES: Controversy exists about whether the elastic modulus (E) mismatch between the loading indenter and ceramic materials influences fatigue testing results. The research hypotheses were that for porcelain veneered Y-TZP crowns 1) A low modulus Steatite indenter (SB) leads to higher fatigue reliability compared to a high modulus tungsten carbide indenter (WC); 2) Different surface damage patterns are expected between low and high modulus indenters after sliding contact fatigue testing. All ceramic crowns will exhibit similar step-stress accelerated life testing (SSALT) contact fatigue reliability (hypothesis 1) and failure characteristics (hypothesis 2) when using high stiffness tungsten carbide (WC, E = 600 GPa) vs. enamel like steatite (SB, E = 90 GPa) indenters. METHODS: Manufacturer (3M Oral Care) prepared Y-TZP-veneered all-ceramic molar crowns were bonded to aged resin composite reproductions of a standard tooth preparation and subjected to mouth-motion SSALT fatigue (n = 18 per indenter type). Failure was defined either as initial inner cone crack (IC), or final fracture (FF) when porcelain fractured (chipping). Selected IC specimens that did not progress to FF were embedded in epoxy resin and sectioned for fractographic analysis. RESULTS: The distribution of failures across the load and cycle profiles lead to similar calculated Weibull Use Level Probability Plots with overlap of the 2-sided 90% confidence bounds. The calculated reliability for IC and FF was equivalent at a mission of 300 N or 700 N load and 50,000 cycles, although the WC indenter had a trend for lower reliability for IC at 700 N. Both indenters produced similar patterns of wear and cracking on crown surfaces. Fractographic landmarks showed competing failure modes, but sliding contact partial inner cone cracks were the most dominant for both groups. SIGNIFICANCE: The more compliant Steatite indenter had similar veneered crown fatigue reliability and failure modes to those found with use of a high stiffness tungsten carbide indenter (hypotheses 1 and 2 rejected).


Assuntos
Cerâmica , Coroas , Resinas Compostas , Porcelana Dentária , Falha de Restauração Dentária , Análise do Estresse Dentário , Teste de Materiais , Reprodutibilidade dos Testes
14.
J Mech Behav Biomed Mater ; 94: 144-154, 2019 06.
Artigo em Inglês | MEDLINE | ID: mdl-30897502

RESUMO

To evaluate the fatigue failure load (FFL), number of cycles for failure (CFF) and survival probabilities of lithium-disilicate (LD) monolithic crowns manufactured by two processing techniques (pressing vs. CAD/CAM) adhesively cemented to a dentin-analogue material, considering two surface treatments (conventional vs. simplified). Surface characteristics (topography, roughness and fractal dimensions) were also assessed. Forty (40) monolithic crowns were manufactured considering two specific processing techniques for each ceramic system: LDCAD - CAD/CAM lithium-disilicate (IPS e.max CAD, Ivoclar Vivadent); LDPRESS - pressed lithium-disilicate (IPS e.max Press, Ivoclar Vivadent). The crowns were adhesively cemented (Multilink Automix System, Ivoclar Vivadent) onto dentin analogue preparations considering two distinct protocols of surface treatments (conventional - hydrofluoric acid etching + silane application [HF+Sil] or simplified - etching with one-step primer (Monobond Etch&Prime, Ivoclar Vivadent) [EP]). The cemented assembly was stored in distilled water at 37 °C for 3 days and fatigue tests were run (step-stress approach: load ranging from 400 to 2000 N, step-size of 100 N, 15,000 cycles/step, 20 Hz). Fractography, surface topography, roughness, and fractal dimension analyses were performed. LDPRESS[EP] group depicted higher FFL, CFF and survival probabilities in comparison to LDCAD groups, regardless of the conditioning method. A tendency of higher Weibull modulus (mechanical reliability) was observed when using [EP] for both LDPRESS and LDCAD. SEM and AFM analysis showed very distinct initial surface patterns for the distinct processing techniques considered (LDCAD with higher fractal dimension and lower roughness than LDPRESS), and both surface treatments distinctly affected these surface characteristics. All failures were radial cracks originating at the ceramic-cement interface. Pressed lithium-disilicate monolithic crowns showed better fatigue performance in comparison to CAD/CAM milled crowns, especially when they were treated with self-etching ceramic primer. The surface treatment with self-etching primer led to similar fatigue performance when compared to hydrofluoric acid plus silane application for the same processing technique, but it tended to provide higher mechanical reliability.


Assuntos
Cerâmica/química , Desenho Assistido por Computador , Coroas , Porcelana Dentária/química , Estresse Mecânico , Adesividade , Teste de Materiais , Propriedades de Superfície
15.
Materials (Basel) ; 12(19)2019 Sep 25.
Artigo em Inglês | MEDLINE | ID: mdl-31557803

RESUMO

III-nitride-based ultraviolet light emitting diode (UV LED) has numerous attractive applications in air and water purification, UV photolithography, and in situ activation of drugs through optical stimulus, solid state lighting, polymer curing, and laser surgery. However, the unclear failure mechanisms and uncertainty reliability have limited its application. Therefore, a design of an appropriate reliability test plan for UV LEDs has become extremely urgent. Compared to traditional reliability tests recommended in LED lighting industry, the step-stress accelerated degradation test (SSADT) is more cost-effective and time-effective. This paper compares three SSADT testing plans with temperature and driving currents as stepwise increasing loads to determine an appropriate test strategy for UV LEDs. The study shows that: (1) the failure mechanisms among different SSADT tests seem to be very different, since the driving current determines the failure mechanisms of UV LEDs more sensitively, and (2) the stepped temperature accelerated degradation test with an appropriate current is recommended for UV LEDs.

16.
Dent Mater ; 34(6): e128-e137, 2018 06.
Artigo em Inglês | MEDLINE | ID: mdl-29653724

RESUMO

OBJECTIVE: To characterize the mechanical properties of different coating methods of DLC (diamond-like carbon) onto dental implant abutment screws, and their effect on the probability of survival (reliability). METHODS: Seventy-five abutment screws were allocated into three groups according to the coating method: control (no coating); UMS - DLC applied through unbalanced magnetron sputtering; RFPA-DLC applied through radio frequency plasma-activated (n=25/group). Twelve screws (n=4) were used to determine the hardness and Young's modulus (YM). A 3D finite element model composed of titanium substrate, DLC-layer and a counterpart were constructed. The deformation (µm) and shear stress (MPa) were calculated. The remaining screws of each group were torqued into external hexagon abutments and subjected to step-stress accelerated life-testing (SSALT) (n=21/group). The probability Weibull curves and reliability (probability survival) were calculated considering the mission of 100, 150 and 200N at 50,000 and 100,000 cycles. RESULTS: DLC-coated experimental groups evidenced higher hardness than control (p<0.05). In silico analysis depicted that the higher the surface Young's modulus, the higher the shear stress. Control and RFPA showed ß<1, indicating that failures were attributed to materials strength; UMS showed ß>1 indicating that fatigue contributed to failure. High reliability was depicted at a mission of 100N. At 200N a significant decrease in reliability was detected for all groups (ranging from 39% to 66%). No significant difference was observed among groups regardless of mission. Screw fracture was the chief failure mode. SIGNIFICANCE: DLC-coating have been used to improve titanium's mechanical properties and increase the reliability of dental implant-supported restorations.


Assuntos
Parafusos Ósseos , Carbono/química , Materiais Revestidos Biocompatíveis/química , Dente Suporte , Diamante/química , Fenômenos Biomecânicos , Falha de Restauração Dentária , Análise do Estresse Dentário , Módulo de Elasticidade , Dureza , Teste de Materiais , Reprodutibilidade dos Testes , Estresse Mecânico , Propriedades de Superfície , Titânio/química
17.
J Prosthodont Res ; 62(1): 24-30, 2018 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-28427837

RESUMO

PURPOSE: The aim of this study was to evaluate fatigue resistance of dental fixtures with two different fixture-abutment connections by in vitro fatigue testing and in silico three-dimensional finite element analysis (3D FEA) using original computer-aided design (CAD) models. METHODS: Dental implant fixtures with external connection (EX) or internal connection (IN) abutments were fabricated from original CAD models using grade IV titanium and step-stress accelerated life testing was performed. Fatigue cycles and loads were assessed by Weibull analysis, and fatigue cracking was observed by micro-computed tomography and a stereomicroscope with high dynamic range software. Using the same CAD models, displacement vectors of implant components were also analyzed by 3D FEA. Angles of the fractured line occurring at fixture platforms in vitro and of displacement vectors corresponding to the fractured line in silico were compared by two-way ANOVA. RESULTS: Fatigue testing showed significantly greater reliability for IN than EX (p<0.001). Fatigue crack initiation was primarily observed at implant fixture platforms. FEA demonstrated that crack lines of both implant systems in vitro were observed in the same direction as displacement vectors of the implant fixtures in silico. CONCLUSIONS: In silico displacement vectors in the implant fixture are insightful for geometric development of dental implants to reduce complex interactions leading to fatigue failure.


Assuntos
Desenho Assistido por Computador , Dente Suporte , Projeto do Implante Dentário-Pivô , Implantes Dentários , Análise do Estresse Dentário/métodos , Análise de Elementos Finitos , Teste de Materiais/métodos , Simulação por Computador , Estresse Mecânico
18.
J Mech Behav Biomed Mater ; 87: 288-295, 2018 11.
Artigo em Inglês | MEDLINE | ID: mdl-30103110

RESUMO

This study aims to evaluate the flexural fatigue strength and survival estimates of an Y-TZP monolithic ceramic after grinding and aging. Ceramic discs (1.2 mm thickness × 15.0 mm diameter - ISO, 6872, 2015) of zirconia (Zirlux FC2 - Ardent; Ivoclar Vivadent) were made and randomly allocated into 6 groups (n = 10), according to grinding and aging factors: Ctrl - as-sintered; Ctrl Sto - as-sintered and dry stored at room temperature for 2 years; Ctrl Aut Sto - as-sintered, submitted to autoclaved aging (134 °C, 2 bar, 20 h) and then dry stored for 2 years; and similar conditions for ground samples (Ground; Ground Sto; Ground Aut Sto). Grinding was performed with diamond burs (#3101G, KG Sorensen) coupled to a contra-angle torque multiplier attached to a low speed motor under constant irrigation. Fatigue testing followed a step-stress approach. Data from strength and number of cycles until fracture were recorded and analyzed through Kaplan-Meier and Mantel-Cox tests. Both grinding and aging increase monoclinic phase content. The topography was altered by grinding but not by aging procedures. Grinding did not alter the fatigue strength (Ctrl = Ground), while aging increase it only for ground groups (Ground Sto, Ground Aut Sto). Aged conditions (Ctrl Sto; Ground Sto; Ctrl Aut Sto; Ground Aut Sto) showed increased survival probabilities for both flexural fatigue strength and cycles for failure. Therefore, despite promoting monoclinic phase increase, aging and grinding did not deleteriously affect the fatigue behavior of Y-TZP ceramics.


Assuntos
Cerâmica/química , Teste de Materiais , Estresse Mecânico , Ítrio/química , Zircônio/química , Propriedades de Superfície , Fatores de Tempo
19.
Dent Mater ; 34(10): 1578-1584, 2018 10.
Artigo em Inglês | MEDLINE | ID: mdl-30049596

RESUMO

OBJECTIVE: The aim of this study was to evaluate long-term fatigue behavior using an in vitro step-stress accelerated life test (SSALT), and to determine the crack initiation point using in silico finite element analysis for computer-aided designed and manufactured (CAD/CAM) molar crowns fabricated from three commercial CAD/CAM resin composite blocks: Cerasmart (CS; GC, Tokyo, Japan), Katana Avencia Block (KA; Kuraray Noritake Dental, Niigata, Japan), and Shofu Block HC (HC; Shofu, Kyoto, Japan). METHODS: Fifty-one mandibular first molar crowns luted on a resin core die were embedded in acrylic resin and covered with a polyvinyl chloride tube. Single compressive tests were performed for five crowns. SSALT was conducted for 36 crowns using three profiles and reliabilities at 120,000 cycles, and a Weibull analysis was conducted. The maximum principal strain of each CAD/CAM resin composite crown model was analyzed by three-dimensional finite element analysis. RESULTS: Fracture loads of CS and KA (3784±144N and 3915±313N) were significantly greater than that of HC (2767±227N) (p<0.05). Fracture probabilities at 120,000 cycles were 24.6% (CS), 13.7% (KA), and 14.0% (HC). Maximum principal strain was observed around the mesiolingual cusps of CS and KA and the distobuccal cusp of HC. SIGNIFICANCE: CAD/CAM resin composite molar crowns containing nano-fillers with a higher fraction of resin matrix exhibited higher fracture loads and greater longevity, suggesting that these crowns could be used as an alternative to ceramic crowns in terms of fatigue behavior.


Assuntos
Resinas Compostas/química , Desenho Assistido por Computador , Coroas , Falha de Restauração Dentária , Planejamento de Prótese Dentária , Análise do Estresse Dentário , Análise de Elementos Finitos , Teste de Materiais , Microscopia Eletrônica de Varredura , Dente Molar , Difração de Raios X
20.
J Mech Behav Biomed Mater ; 71: 244-249, 2017 07.
Artigo em Inglês | MEDLINE | ID: mdl-28365541

RESUMO

PURPOSE: To assess the probability of survival (reliability) and failure modes of narrow implants with different diameters. MATERIALS AND METHODS: For fatigue testing, 42 implants with the same macrogeometry and internal conical connection were divided, according to diameter, as follows: narrow (Ø3.3×10mm) and extra-narrow (Ø2.9×10mm) (21 per group). Identical abutments were torqued to the implants and standardized maxillary incisor crowns were cemented and subjected to step-stress accelerated life testing (SSALT) in water. The use-level probability Weibull curves, and reliability for a mission of 50,000 and 100,000 cycles at 50N, 100, 150 and 180N were calculated. For the finite element analysis (FEA), two virtual models, simulating the samples tested in fatigue, were constructed. Loading at 50N and 100N were applied 30° off-axis at the crown. The von-Mises stress was calculated for implant and abutment. RESULTS: The beta (ß) values were: 0.67 for narrow and 1.32 for extra-narrow implants, indicating that failure rates did not increase with fatigue in the former, but more likely were associated with damage accumulation and wear-out failures in the latter. Both groups showed high reliability (up to 97.5%) at 50 and 100N. A decreased reliability was observed for both groups at 150 and 180N (ranging from 0 to 82.3%), but no significant difference was observed between groups. Failure predominantly involved abutment fracture for both groups. FEA at 50N-load, Ø3.3mm showed higher von-Mises stress for abutment (7.75%) and implant (2%) when compared to the Ø2.9mm. CONCLUSIONS: There was no significant difference between narrow and extra-narrow implants regarding probability of survival. The failure mode was similar for both groups, restricted to abutment fracture.


Assuntos
Implantes Dentários , Falha de Restauração Dentária , Análise do Estresse Dentário , Coroas , Planejamento de Prótese Dentária , Humanos , Incisivo , Teste de Materiais , Probabilidade , Reprodutibilidade dos Testes , Estresse Mecânico
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