Microstructure and properties of pitch-based carbon composites
J Microsc
; 196(# (Pt 2)): 213-24, 1999 Nov.
Article
em En
| MEDLINE
| ID: mdl-10540274
ABSTRACT
Pitches prepared in the laboratory by thermal treatment and air-blowing of a commercial coal-tar pitch were used as matrix precursors of carbon composites using granular petroleum coke, foundry coke, amorphous graphite and anthracite. Pitches were characterized by standard procedures (elemental analysis, softening point, solubility tests and carbon yield) and light microscopy (mesophase content). Pitch pyrolysis behaviour was monitored by thermogravimetric analysis and from the optical texture of cokes. Pitch wettability to the different carbons, at different temperatures, was also studied. Experimental conditions selected for the preparation of composites were based on pitch composition and properties. The main microstructural features of composites were determined by light microscopy and scanning electron microscopy. Composite properties were described in terms of their density, porosity and compressive strength, and related to composite microstructure and the characteristics of the precursors. Thermal treatment and air-blowing of pitch improved carbon composite structure and properties. The lowest porosities and best mechanical properties were observed in those composites obtained with the thermally treated pitches combined with foundry coke and anthracite.
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Coleções:
01-internacional
Base de dados:
MEDLINE
Idioma:
En
Revista:
J Microsc
Ano de publicação:
1999
Tipo de documento:
Article
País de afiliação:
Espanha