RESUMEN
Mn:PIN-PMN-PT piezocrystal is investigated to determine whether its enhanced energy density makes it a candidate transducer material for power ultrasonics applications. To this end, the electromechanical and vibrational characteristics of a simple configuration of a bolted Langevin transducer (BLT) and then an ultrasonic surgical device, both incorporating Mn:PIN-PMN-PT piezocrystal, are compared with the same transducer configurations incorporating a conventional hard PZT piezoceramic commonly used in high-power ultrasonic transducers. The material properties of Mn:PIN-PMN-PT are determined using a single sample characterisation technique and these are used in finite element analysis (FEA) to design and then fabricate the BLT and ultrasonic surgical device, tuned to the first and second longitudinal modes at 20 kHz respectively. FEA is similarly used for the hard PZT versions. It is found that the superior elastic compliance of Mn:PIN-PMN-PT results in a higher radial piezo-stack deformation than the hard PZT under ultrasonic excitation of the BLT. However, the resulting longitudinal displacement amplitude of the two BLTs and two ultrasonic surgical devices is found to be equal, despite the higher figure of merit (Qkeff2) of those incorporating Mn:PIN-PMN-PT. The electrical impedance is measured at increasing excitation levels to evaluate the quality factor, Q. It is found that damping in the BLT with hard PZT is negligibly affected in the excitation range considered; however, the BLT incorporating Mn:PIN-PMN-PT exhibits a large reduction in Q. These findings indicate that, for measurements in air, the advantages of the high figure of merit of the piezocrystal material are not realised in a high-power transducer due to significantly increased damping at high excitation levels. To compare the vibrational response of the two ultrasonic surgical devices, L-C electrical impedance matching was implemented to maximise the efficiency of energy transfer from the source to the transducer under load. Results suggest that similar responses occurred for the two surgical devices in cutting tests using a low strength bone mimic material. However, the Mn:PIN-PMN-PT device exhibited better performance in cutting through higher strength ex-vivo chicken femur.
RESUMEN
Stabilization of topological spin textures in layered magnets has the potential to drive the development of advanced low-dimensional spintronics devices. However, achieving reliable and flexible manipulation of the topological spin textures beyond skyrmion in a two-dimensional magnet system remains challenging. Here, we demonstrate the introduction of magnetic iron atoms between the van der Waals gap of a layered magnet, Fe3GaTe2, to modify local anisotropic magnetic interactions. Consequently, we present direct observations of the order-disorder skyrmion lattices transition. In addition, non-trivial topological solitons, such as skyrmioniums and skyrmion bags, are realized at room temperature. Our work highlights the influence of random spin control of non-trivial topological spin textures.
RESUMEN
The impact of Pb on the environment and human health and recent restrictions on its use in electronic devices are generating demand for Pb-free piezoelectric materials. Examples are now available commercially, but the full elastic-piezoelectric-dielectric (EPD) matrices needed for device design, including over a range of operating conditions, have not yet been published. The standard IEEE EPD matrix measurement method needs four sample geometries, making it inconvenient and increasing errors. Here, we present an alternative method combining resonant ultrasound spectroscopy with optimization algorithms to measure the EPD matrix from a single exact cube sample. The Levenberg-Marquardt (LM) and Nelder-Mead (NM) optimizations are compared in refining the independent parameters. Both give convergent solutions, but the LM algorithm is more accurate and efficient. The single-sample approach was used to obtain results from Pb-free Na1/2Bi1/2TiO3 (PIC 700, PI Ceramics, Lederhose, Germany) piezoceramic ( ∞ mm sample symmetry) characterized with the standard IEEE method at ambient temperature and with the single-sample method at ambient temperature and additionally up to 80 °C. The results are validated with the laser Doppler vibrometry via mode shape reconstruction and comparison with finite-element analysis (FEA). They demonstrate that convenient measurement of the EPD matrix of Pb-free materials with temperature dependence is possible, providing a crucial capability for the adoption of these materials in devices.