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1.
Materials (Basel) ; 14(4)2021 Feb 06.
Artículo en Inglés | MEDLINE | ID: mdl-33562135

RESUMEN

Cube texture and microstructural evolution of as-cast non-oriented silicon steel (1.3% Si) during cold rolling and annealing were studied. The results showed that the as-cast microstructure with grain size in the range of 100-500 µm had a weak texture. The strong orientation was mainly located at {100} and {110} planes. A significant content of shear-deformed grains oriented with {110}<110> were obtained by cold-rolling, and many regions oriented with Cube texture were distributed in the shear bands. During cold-rolling, the orientation of the shear-deformed microstructure tilted towards the {111}<112> orientation, while the matrix orientation retained {110}<110>. On further cold-rolling, the residual part of {110}<110> experienced shear deformation, forming more shear bands, strengthening the Cube orientation. During annealing, Cube orientation grains nucleated in the shear bands leading to strong Cube texture, and corresponding B50 was 1.83T/1.79T.

2.
Materials (Basel) ; 13(19)2020 Sep 25.
Artículo en Inglés | MEDLINE | ID: mdl-32992969

RESUMEN

In this study, we address the challenge of obtaining high strength at ambient and elevated temperatures in fire-resistant Ti-Mo-V steel with ferrite microstructures through thermo-mechanical controlled processing (TMCP). Thermally stable interphase precipitation of (Ti, Mo, V)C was an important criterion for retaining strength at elevated temperatures. Electron microscopy indicated that interphase precipitation occurred during continuous cooling after controlled rolling, where the volume fraction of interphase precipitation was controlled by the laminar cooling temperature. The interphase precipitation of MC carbides with an NaCl-type crystal structure indicated a Baker-Nutting (B-N) orientation relationship with ferrite. When the steel was isothermally held at 600 °C for up to 3 h, interphase precipitation occurred during TMCP with high thermal stability. At the same time, some random precipitation took place during isothermal holding. The interphase precipitation increased the elastic modulus of the experimental steels at an elevated temperature. It is proposed that fire-resistant steel with thermally stable interphase precipitation is preferred, which enhances precipitation strengthening and dislocation strengthening at elevated temperatures.

3.
Materials (Basel) ; 11(7)2018 Jul 08.
Artículo en Inglés | MEDLINE | ID: mdl-29986532

RESUMEN

The use of twin-roll strip casting for the preparation of non-oriented silicon steel has attracted widespread attention in recent years, but related reports are limited. In this study, both one- and two-stage cold rolling with three intermediate annealing temperatures were employed to produce strip cast non-oriented silicon steel. The evolution of the microstructure and texture through the processing routes and its effect on magnetic properties were studied. Compared with one-stage rolling, two-stage rolling increased the in-grain shear bands and the retention of Cube texture in the cold rolled sheets, thereby promoting the nucleation of favorable Goss and Cube grains and restraining the nucleation of harmful {111}<112> grains. With the increase in intermediate annealing temperature, the η-fiber texture in annealed sheets was gradually enhanced, and the average grain size was increased, leading to significant improvement of magnetic properties.

4.
Materials (Basel) ; 11(10)2018 Oct 19.
Artículo en Inglés | MEDLINE | ID: mdl-30347775

RESUMEN

To elucidate the hot deformation characteristics of TiAl alloys, flow stress prediction, microstructural evolution and deformation mechanisms were investigated in Ti-44Al-5Nb-1Mo-2V-0.2B alloy by isothermal compression tests. A constitutive relationship using the Arrhenius model involving strain compensation and back propagation artificial neural network (BP-ANN) model were developed. A comparison of two models suggested that the BP-ANN model had excellent capabilities and was more accurate in predicting flow stress. Based on the microstructural analysis, bending and elongation of colonies, γ and B2 grains were the main microstructural constituents at low temperature and high strain rate. Dynamic recrystallization (DRX) of γ and dynamic recovery (DRY) of ß/B2 were the main deformation mechanisms. With the increase of temperature and decrease of strain rate, phase transformation played an important role. The flake-like γ precipitates in B2 grains, and a coarsening of γ lamellae via α lath dissolution during compression were observed. Additionally, the flow softening process commenced with dislocation pile-up and formation of sub-grain boundaries, followed by grain refinement, twins and nano-lamellar nucleation. Continuous DRX and phase transformation promoted the formability of Ti-44Al-5Nb-1Mo-2V-0.2B alloy.

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