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1.
Materials (Basel) ; 17(10)2024 May 15.
Artículo en Inglés | MEDLINE | ID: mdl-38793428

RESUMEN

Friction stir processing (FSP) is a solid-state treating method to enhance the mechanical properties of materials by altering their microstructure. In this study, FSP was applied to the AZ91 magnesium alloy cladding layer prepared using cold metal transition (CMT) technology, and the purpose was to investigate the effect of the traverse speed of the H13 steel stirring head under a constant rotation speed on the microstructure and mechanical properties of the cladding layer. The results demonstrated that FSP could effectively decrease the grain size of the cladding layer and lead to the dispersion and dissolution of the coarse ß-Mg17Al12 second phase into the α-Mg matrix. The mechanical characteristics of the processed cladding layer were significantly enhanced compared to the unprocessed cladding layer due to the grain refinement and second-phase strengthening induced by FSP. When the stirring head rotation speed was set at 300 r/min, the average microhardness and tensile properties of the specimens showed a tendency of initially increasing and then dropping as the traverse speed increased. The cladding layer, obtained at a traverse speed of 60 mm/min, displayed optimal mechanical properties with an average microhardness, tensile strength, and elongation of 85.6 HV0.1, 278.5 MPa, and 13.4%, respectively.

2.
Materials (Basel) ; 17(12)2024 Jun 12.
Artículo en Inglés | MEDLINE | ID: mdl-38930245

RESUMEN

Friction stir processing (FSP) was performed on an AZ91 magnesium alloy cladding layer fabricated by a cold metal transfer (CMT) technique. Electrochemical properties and immersion corrosion behavior of the cladding layer before and after FSP in 3.5 wt.% NaCl solution were investigated. After applying the FSP, the corrosion potential and corrosion current density of the cladding layer increased from -1.455 V to -1.397 V and decreased from 4.135 µA/cm2 to 1.275 µA/cm2, respectively. The results of OM and SEM displayed the refinement of grains and the dispersion of ß-Mg17Al12 second phase in the friction stir processed (FSPed) cladding layer and more severe corrosion of the unprocessed sample. The corrosion rate of the FSPed cladding layer was lower, and a more compact corrosion product film was formed on the surface of the FSPed cladding layer. EDS results and XRD patterns showed that the corrosion products was mainly composed of Mg(OH)2. The increase in Al content in the α-Mg matrix, grain refinement, and fragmentation and dispersion of the ß-Mg17Al12 second phase induced by FSP were the main factors that led to the improvement in corrosion resistance of the cladding layer of the AZ91 magnesium alloy fabricated by CMT.

3.
Materials (Basel) ; 16(8)2023 Apr 19.
Artículo en Inglés | MEDLINE | ID: mdl-37110072

RESUMEN

The droplet transfer behavior and stability of the swing arc additive manufacturing process of AZ91 magnesium alloy based on the cold metal transfer (CMT) technique were studied by analyzing the electrical waveforms and high-speed droplet images as well as the forces on the droplet, and the Vilarinho regularity index for short-circuit transfer (IVSC) based on variation coefficients was used to characterize the stability of the swing arc deposition process. The effect of the CMT characteristic parameters on the process stability was investigated; then, the optimization of the CMT characteristic parameters was realized based on the process stability analysis. The results show that the arc shape changed during the swing arc deposition process; thus, a horizontal component of the arc force was generated, which significantly affected the stability of the droplet transition. The burn phase current I_sc_wait presented a linear function relation with IVSC, while the other three characteristic parameters, i.e., boost phase current I_boost, boost phase duration t_I_boost and short-circuiting current I_sc2, all had a quadratic correlation with IVSC. A relation model of the CMT characteristic parameters and IVSC was established based on the rotatable 3D central composite design; then, the optimization of the CMT characteristic parameters was realized using a multiple-response desirability function approach.

4.
Materials (Basel) ; 16(11)2023 May 29.
Artículo en Inglés | MEDLINE | ID: mdl-37297185

RESUMEN

Based on the cold metal transfer (CMT) technique, a deposited wall of AZ91 magnesium alloy was fabricated by weaving wire and arc additive manufacturing (WAAM), the shaping, microstructure, and mechanical properties of the sample with the weaving arc were characterized and discussed by compared with the sample without the weaving arc, and the effects of the weaving arc on grain refinement and property enhancement of the AZ91 component by CMT-WAAM process were investigated. After introducing the weaving arc, the effective rate of the deposited wall could be increased from 84.2% to 91.0%, and the temperature gradient of the molten pool could be reduced with an increase in constitutional undercooling. The equiaxed α-Mg grains became more equiaxial due to the dendrite remelting, and the ß-Mg17Al12 phases distributed uniformly induced by the forced convection after introducing the weaving arc. Compared to the deposited component fabricated by the CMT-WAAM process without the weaving arc, the average ultimate tensile strength and elongation of the component by weaving the CMT-WAAM process both increased. The weaving CMT-WAAM component showed isotropy and has better performance than the traditional cast AZ91 alloy.

5.
Materials (Basel) ; 13(18)2020 Sep 10.
Artículo en Inglés | MEDLINE | ID: mdl-32927856

RESUMEN

High-quality joining of dissimilar alloys between Fe-36Ni alloy and 304L stainless steel is essential in the manufacturing of LNG tanker. In this study, lap joints of Fe-36Ni and 304L dissimilar alloys were fabricated by a pulsed gas tungsten arc welding (P-GTAW) process. The effects of low-frequency pulse on the appearance, microstructure and mechanical properties of the Fe-36Ni/304L lap joints was investigated. With the increase of frequency, the feature sizes of α (the transition angle of the upper surface of Fe-36Ni to the surface of the weld bead) and R (shortest distance between weld root and weld surface) exhibited downtrend and uptrend, respectively, while La (the maximum weld width of lower sheet) and P (the maximum weld penetration of lower sheet) changed in a smaller range. Fusion zone (FZ) is mainly composed of γ phase and M23C6 during solidification, and M23C6 particles are distributed on the grain boundaries of the cells, which reduced the mechanical properties of joint. The average hardness between 110 HV1 and 136 HV1 is lower than that of the base metals. Fractures of all joints located at the Fe-36Ni side near the weld, and a dimple fracture in all samples indicated a ductile fracture. This study found that the heat input values remain 198.86 J mm-1 and increased pulse frequency can improve the maximum tensile force. The average maximum tensile force of the lap weld is 11.95 kN when pulsed frequency is 15 Hz.

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