Residual thickness enhanced core-removed D-shaped single-mode fiber and its application for VOC evaporation monitoring.

A core-removed D-shaped structure with different residual thickness (RT) was manufactured on a single mode silica fiber (SMF) to enhance the sensitivity by using of ultra-precise polishing technology. With six different RTs ranging from ∼55 µm to ∼28 µm, the RT enhancement effect in a D-shaped SMF was researched in detail. The influence of the RT on its transmission spectra was investigated both theoretically and experimentally. Considering a compromise between the multimode interference efficiency and optical power loss, an optimum RT value of 34.09 µm was achieved. The obtained refractive index (RI) sensitivity was 10243 nm/RIU in the RI range of 1.430-1.444, corresponding to a RI resolution of 1.9×10-6 RIU. A high-performance all-fiber sensor was developed to monitor the evaporation process volatile organic compounds (VOCs) based on the RT-enhanced D-shaped SMF. As proof of concept, a 2-hour continuous monitoring was carried to monitor the chloroform and alcohol mixture. As a result, the evaporation of alcohol and chloroform were clearly identified and monitored. The developed RT-enhanced D-shaped fiber sensor provides an alternative way for chemical process monitoring and industrial applications.

Application of Micro Quartz Tuning Fork in Trace Gas Sensing by Use of Quartz-Enhanced Photoacoustic Spectroscopy.

A novel quartz-enhanced photoacoustic spectroscopy (QEPAS) sensor based on a micro quartz tuning fork (QTF) is reported. As a photoacoustic transducer, a novel micro QTF was 3.7 times smaller than the usually used standard QTF, resulting in a gas sampling volume of ~0.1 mm3. As a proof of concept, water vapor in the air was detected by using 1.39 µm distributed feedback (DFB) laser. A detailed analysis of the performance of a QEPAS sensor based on the micro QTF was performed by detecting atmosphere H2O. The laser focus position and the laser modulation depth were optimized to improve the QEPAS excitation efficiency. A pair of acoustic micro resonators (AmRs) was assembled with the micro QTF in an on-beam configuration to enhance the photoacoustic signal. The AmRs geometry was optimized to amplify the acoustic resonance. With a 1 s integration time, a normalized noise equivalent absorption coefficient (NNEA) of 1.97 × 10-8 W·cm-1·Hz-1/2 was achieved when detecting H2O at less than 1 atm.

Influence of Tuning Fork Resonance Properties on Quartz-Enhanced Photoacoustic Spectroscopy Performance.

A detailed investigation of the influence of quartz tuning forks (QTFs) resonance properties on the performance of quartz-enhanced photoacoustic spectroscopy (QEPAS) exploiting QTFs as acousto-electric transducers is reported. The performance of two commercial QTFs with the same resonance frequency (32.7 KHz) but different geometries and two custom QTFs with lower resonance frequencies (2.9 KHz and 7.2 KHz) were compared and discussed. The results demonstrated that the fundamental resonance frequency as well as the quality factor and the electrical resistance were strongly inter-dependent on the QTF prongs geometry. Even if the resonance frequency was reduced, the quality factor must be kept as high as possible and the electrical resistance as low as possible in order to guarantee high QEPAS performance.

Orbital angular momentum sidebands of vortex beams transmitted through a thin metamaterial slab.

A pure vortex beam carrying m-order orbital angular momentum (OAM) will be deformed when transmitting through a thin slab, and "neighboring" sideband {m + 1} and {m-1} modes will emerge. The emergence of the OAM sideband is accompanied with OAM-dependent Goos-Hänchen (GH) shift. When the energies carried by the {m} mode of the transmitted beam and by the sideband modes are identical, the OAM-dependent shifts reach their upper limits, |m|w0/2(|m| + 1)1/2, where w0 is the incident beam waist. The epsilon-near-zero metamaterial is found to be suitable to achieve the upper-limited OAM-dependent GH shifts. These findings provide a deeper insight into the beam shifts of vortex beams and have potential applications in the optical sensing, detection of OAM, and other OAM-based applications.

Theoretical investigation of optical modulators based on graphene-coated side- polished fiber.

The effective mode index (EMI) of a graphene-coated side-polished fiber (GSPF) is calculated numerically. Whereby, the influences of graphene atom layer number, residual radius of SPF, light frequency, scattering rate of graphene, and temperature on the EMI are investigated comprehensively. Two types of mechanisms for the electro-optical absorption modulation are found for such GSPF-based modulator. One mechanism is Pauli blocking effect (PBE) and the other is plasmonic attenuation effect (PAE). With the optimal design parameters, a PBE-based modulator is theoretically predicted to have a 0.0072 dB/µm modulation depth, 2.92 V driving voltage swing, 6.35 nJ/bit power consumption, and 56.2 THz optical modulation bandwidth. It is also predicted that a PAE-based modulator could have a 0.0056 dB/µm modulation depth, 0.6 V driving voltage swing, 0.27 nJ/bit power consumption, and 2.5 THz optical modulation bandwidth. By further optimization, the modulator performance such as the relatively high power consumption and the narrow operation bandwidth can be improved. Owing to their seamless connection to optical fiber networks, the GSPF-based modulators have great potential to be used in fast and high-capacity optical communication systems.

High performance all-fiber temperature sensor based on coreless side-polished fiber wrapped with polydimethylsiloxane.

A novel fiber structure, coreless side-polished fiber (CSPF) that is wrapped by polydimethylsiloxane (PDMS), is demonstrated to be highly sensitive to temperature because of the high refractive index sensitivity of the CSPF and the large thermal optic coefficient of the PDMS. Our numerical and experimental results show that the several dips in the transmitted spectra of PDMSW-CSPF is originated from the multimode interference (MMI) in the CSPF and will blueshift with the increase of temperature. Furthermore, for such a PDMSW-CSPF, we investigate its temperature sensing characteristics and the influences of residual thickness (RT) and dip wavelength on the sensitivity both numerically and experimentally. In the temperature range of 30~85°C, the PDMSW-CSPF with RT = 43.26 µm exhibits a high temperature sensitivity of -0.4409 nm/°C, the high linearity of 0.9974, and the high stability with low standard deviation of 0.141 nm. Moreover, in the cycle experiments, where the environmental temperature was set to automatically increase and then decrease, the PDMSW-CSPF exhibits a low relative deviation of sensitivity (RSD) of down to ± 0.068%. Here, the RSD is defined as the ratio of sensitivity deviation to the average sensitivity measured in the heating/cooling cycle experiments. The lower RSD indicates that PDMSW-CSPF has better reversibility than other fiber structure. The investigations also show that the sensitivity of the PDMSW-CSPF could be enhanced further by reducing the residual thickness and choosing the dip at a longer wavelength.

Graphene-based tunable Imbert-Fedorov shifts and orbital angular momentum sidebands for reflected vortex beams in the terahertz region.

Upon reflection, a light beam embedded with m-order orbital angular momentum (OAM) will undergo the Imbert-Fedorov (IF) shift, which induces OAM sidebands. The energies of the neighboring {-m-1} and {-m+1} sideband modes of the reflected beam are always equal. Controllable OAM sidebands are theoretically achieved by introducing a monolayer graphene in a three-layer structure composed of air, hexagonal boron nitride, and metal. By modulating the Fermi energy of graphene, the OAM-dependent IF shift can be tuned from positive to negative values, and the OAM sideband modes can be suppressed or enhanced, since the reflectivity for perpendicular and parallel polarizations vary with the Fermi energy. These findings provide an alternative method for the control of optical OAM in the terahertz region.

Large spatial and angular spin splitting in a thin anisotropic ε-near-zero metamaterial.

We show theoretically that after transmitted through a thin anisotropic ε-near-zero metamaterial, a linearly polarized Gaussian beam can undergo both transverse spatial and angular spin splitting. The upper limits of spatial and angular spin splitting are found to be the beam waist and divergence angle of incident Gaussian beam, respectively. The spin splitting of transmitted beam after propagating a distance z depends on both the spatial and angular spin splitting. By combining the spatial and angular spin splitting properly, we can maximize the spin splitting of propagated beam, which is nearly equal to the spot size of Gaussian beam w(z).

Coreless side-polished fiber: a novel fiber structure for multimode interference and highly sensitive refractive index sensors.

A novel fiber structure, coreless side-polished fiber (CSPF), is proposed and investigated to implement multimode interference (MMI) and high sensitive refractive index (RI) sensors. For such CSPF, the part of the cladding and the core of a single-mode fiber are side-polished off so as to make the remained cladding a D-shaped multimode waveguide. The excitation and evolution of MMI in the CSPF are simulated numerically. The simulation results show that the high-order modes excited within the D-shaped multimode waveguide are mainly TE0,1 (TM0,1)~TE0,6 (TM0,6) modes. Moreover, the RI sensing characteristics and the influences of residual thickness and dip wavelength on the sensitivity are investigated both numerically and experimentally. The experimental results show that the CSPF with a residual thickness of 43.1 µm can reach an ultra-high sensitivity of 28000 nm/RIU in the RI range of 1.442~1.444. It is also found that the sensitivity can be further increased by reducing the residual thickness and choosing the dip at a longer wavelength. Thanks to the ultra-high RI sensitivity and the ease of fabrication, the CSPF could provide a cost-effective platform to build high-performance fiber devices of various functions.

Reduced graphene oxide wrapped on microfiber and its light-control-light characteristics.

Reduced graphene oxide (rGO) sheet wrapped on the tapered region of microfiber is demonstrated to enhance the interaction between rGO and strong evanescent field of optical fiber. The 405 nm and 980 nm lasers are employed to illuminate the rGO to investigate the response characteristics of the optical transmitted power (λ = 1550 nm) in the MF. The transmitted optical power of the MF with rGO changes with ~1.7 dB relative variation when the violet light is ranging from 0 mW to 12 mW (~0.21dB/mW) in the outside-pumped experiment. And in the inside-pumped experiment, the change of the 980 nm laser power from 0 mW to 156.5 mW makes ~6 dB relative variation power of the transmitted optical powers of the MF with rGO. These results indicate the optical transmitted power of the MF with wrapped rGO can be manipulated by the 405 and 980 nm light (order of mW), which signifies the device can potentially be applied as all optically and versatilely controllable devices.

Enhanced optical sensitivity of molybdenum diselenide (MoSe2) coated side polished fiber for humidity sensing.

In this paper, a side-polished fiber (SPF) coated with molybdenum diselenide (MoSe2) is proposed, and its characteristic of relative humidity (RH) sensing is investigated. It is found in the experiment that an enhancement in RH sensitivity (0.321 dB/%RH) can be achieved in a very wide RH range of 32%RH to 73%RH for the proposed MoSe2 coated SPF (MoSe2CSPF). It is also shown that the MoSe2CSPF has a rapid response of 1s and recovery time of 4s, which makes the sensor capable of monitoring human breath. The experimental results suggest MoSe2 has a promising potential in photonics applications such as all-fiber optic humidity sensing networks.

Reduced graphene oxide for fiber-optic toluene gas sensing.

A fiber-optic toluene gas sensor based on reduced graphene oxide (rGO) is demonstrated and its sensing property is investigated experimentally and theoretically. The rGO film is deposited on a side polished fiber (SPF), allowing the strong interaction between rGO film and propagating field and making the SPF sensitive to toluene gas. It is found that the sensor has good linearity and reversibility and can work at room temperature with the response and the recovery time of 256 s and the detection limit of 79 ppm. Moreover, a theoretical model for the sensor is established to analyze the sensing mechanism. Theoretical analysis indicates this type of sensor could work in a wide range of toluene gas concentration and shows that a significant rise in its sensitivity can be expected by adjusting the doping level or chemical potential of graphene.

Tungsten disulfide (WS2) based all-fiber-optic humidity sensor.

We demonstrate a novel all-fiber-optic humidity sensor comprised of a WS2 film overlay on a side polished fiber (SPF). This sensor can achieve optical power variation of up to 6 dB in a relative humidity (RH) range of 35%-85%. In particular, this novel humidity fiber sensor has a linear correlation coefficient of 99.39%, sensitivity of 0.1213 dB/%RH, and a humidity resolution of 0.475%RH. Furthermore, this sensor shows good repeatability and reversibility, and fast response to breath stimulus. This WS2 based all-fiber optic humidity sensor is easy to fabricate, is compatible with pre-established fiber optic systems, and holds great potential in photonics applications such as in all-fiber optic humidity sensing networks.

[Design and Optimization of Surface Plasmon Resonance Sensor Based on Side Polished Single-Mode Fiber].

Fiber-coupling surface Plasmon resonance sensor has attractive advantages of information transmission such as small volume, anti-electric magnetic field interference, and online real-time remote detection. In order to improve the performance of the sensor, the effect of the residual fiber thickness and the silver film thickness to the sensitivity of the sensor and the depth of the resonance peaks and full width ar half maximum (FWHM) are analyzed respectively. The results show that the increasing fiber residual thickness weakens the SPR phenomenon, and that the increasing silver film thickness widens the resonance peak, while the sensitivity of the sensor does not change monotonously. Through the integration of refractive index sensing sensitivity and full width at half maximum, figure of merit is presented and regarded as the optimized objective. The optimal design is achieved in the case of the fiber residual thickness for 66. 5 µm, and the silver film thickness for 50 nm. The optimized design with the figure of merit of 98. 67 is expected to be applied in the bio-chemical sensing and analysis.

Optical fiber with nanostructured cladding of TiO2 nanoparticles self-assembled onto a side polished fiber and its temperature sensing.

We demonstrated temperature sensing of a fiber with nanostructured cladding, which was constructed by titanium dioxide TiO2 nanoparticles self-assembled onto a side polished optical fiber (SPF). Significantly enhanced interaction between the propagating light and the TiO2 nanoparticles (TN) can be obtained via strong evanescent field of the SPF. The strong light-TN interaction results in temperature sensing with a maximum optical power variation of ~4dB in SPF experimentally for an external environment temperature varying from -7.8°C to 77.6°C. The novel temperature sensing device shows a linear correlation coefficient of better than 99.4%, and a sensitivity of ~0.044 dB/°C. The TN-based all-fiber-optic temperature sensing characteristics was successfully demonstrated, and it is compatible with fiber-optic interconnections and high potential in photonics applications.

Reduced graphene oxide for fiber-optic humidity sensing.

Graphene-based electrical chemical vapor sensors can achieve extremely high sensitivity, whereas the comparatively slow sensing response and recovery, the research focused on only low concentration detection, have been known as drawbacks for many applications requiring rapid and high concentration detection. Here we report a novel graphene-based fiber-optic relative humidity (RH) sensor relying on fundamentally different sensing mechanism. The sensor can achieve power variation of up to 6.9 dB in high relative humidity range (70-95%), and display linear response with correlation coefficient of 98.2%, sensitivity of 0.31 dB/%RH, response speed of faster than 0.13%RH/s, and good repeatability in 75-95%RH. Theoretical analysis of sensing mechanism can explain the experimental result, and reveal the broad applying prospect of the sensor for other kinds of chemical vapor detection. This novel graphene-based optical sensor provides a beneficial complement to the existing electrical ones, and will promote the employment of graphene in chemical sensing techniques.

All-optically reconfigurable and tunable fiber surface grating for in-fiber devices: a wideband tunable filter.

A fiber surface grating (FSG) formed from a photosensitive liquid crystal hybrid (PLCH) film overlaid on a side-polished fiber (SPF) is studied and has been experimentally shown to be able to function as an all-optically reconfigurable and tunable fiber device. The device is all-optically configured to be a short period fiber surface grating (SPFSG) when a phase mask is used, and then reconfigured to be a long period FSG (LPFSG) when an amplitude mask is used. Experimental results show that both the short and long period FSGs can function as an optically tunable band-rejection filter and have different performances with different pump power and different configured period of the FSG. When configured as a SPFSG, the device can achieve a high extinction ratio (ER) of 21.5dB and a wideband tunability of 31nm are achieved. When configured as a LPFSG, the device can achieve an even higher ER of 23.4dB and a wider tunable bandwidth of 60nm. Besides these tunable performances of the device, its full width at half maximum (FWHM) can also be optically tuned. The reconfigurability and tunability of the fiber device open up possibilities for other all-optically programmable and tunable fiber devices.

[Performance of wavelength modulation surface plasmon resonance biosensor].

Surface plasmon resonance (SPR) is a rapid, label-free, high-precision technique of biological sensing and analysis. The investigation on the characteristics of provides theoretical basis and instructions for the applications of SPR A Kretschmann-structure surface plasmon resonance (SPR) biosensor based on wavelength modulation was developed, and also its sensing performances in the bulk solution was investigated. Measurements with different concentrations of bulk ethanol and ethylene glycol solutions show that the resonant wavelength shows a low sensitivity, but a higher linear response to the change in refractive index (RI), when RI is relatively smaller. With increasing refractive index , the sensitivity of resonance wavelength to changes in the refractive index increases. In the refractive index range of 1. 407 0-1. 430 RIU, sensitivity reaches to 11 487 nm RIU-1. The sensor resonance wavelength stability is 0. 213 8 nm, and the minimum resolution of refractive index approaches to 10-6 RIU. The advantages of the surface plasmon resonance sensor developed here results in simple operation, high sensitivity, wide detection range, low resolution, makes it an important candidate in chemical and biological sensing.

[Spectra modulated surface plasmon resonance sensor based on side polished multi-mode optical fiber].

Surface plasmon resonance, which utilizes the resonance of optical evanescent wave with the metal surface plasmon wave, has been developed into a high sensitivity, rapid, label-less measurement method for chemical and biological analysis. In order to improve the spectral sensitivity in refractive index for a side polished fiber surface plasmon resonance sensor, the whole cladding layer and part of core of a multimode fiber was polished off. Additionally, an extra chrome layer with relatively high refractive index was coated on the polished zone before a gold film. The results showed that the sensor can measure the refractive index range from 1.333 to 1. 431 RIU, with the average spectral sensitivity of 4.11 x 10(3) nm RIU(-1), which is better than the reported results. Especially, in the refractive index range of 1. 417 1. 431 RIU, the sensitivity reaches to 1.09 x 10(4) nm RIU(-1). The minimum resolution of approximately 3.6 x 10(-5) RIU was estimated by a combination analysis with the sensor sensitivity and stability. The superiorities possessed by the proposed sensor in high sensitivity, wide detection range, small size and good stability and reproducibility, etc., make it a good candidate for food testing, environmental monitoring, biomedical testing and other related fields.

Dynamics of polarization-tuned mirror symmetry breaking in a rotationally symmetric system.

Lateral momentum conservation is typically kept in a non-absorptive rotationally symmetric system through mirror symmetry via Noether's theorem when illuminated by a homogeneous light wave. Therefore, it is still very challenging to break the mirror symmetry and generate a lateral optical force (LOF) in the rotationally symmetric system. Here, we report a general dynamic action in the SO(2) rotationally symmetric system, originating from the polarization-tuned mirror symmetry breaking (MSB) of the light scattering. We demonstrate theoretically and experimentally that MSB can be generally applied to the SO(2) rotationally symmetric system and tuned sinusoidally by polarization orientation, leading to a highly tunable and highly efficient LOF (9.22 pN/mW/µm-2) perpendicular to the propagation direction. The proposed MSB mechanism and LOF not only complete the sets of MSB of light-matter interaction and non-conservative force only using a plane wave but also provide extra polarization manipulation freedom.