Self-aligned nanoscale SQUID on a tip.

A nanometer-sized superconducting quantum interference device (nanoSQUID) is fabricated on the apex of a sharp quartz tip and integrated into a scanning SQUID microscope. A simple self-aligned fabrication method results in nanoSQUIDs with diameters down to 100 nm with no lithographic processing. An aluminum nanoSQUID with an effective area of 0.034 microm2 displays flux sensitivity of 1.8 x 10(-6) Phi(0)/Hz(1/2) and operates in fields as high as 0.6 T. With projected spin sensitivity of 65 micro(B)/Hz(1/2) and high bandwidth, the SQUID on a tip is a highly promising probe for nanoscale magnetic imaging and spectroscopy.

Stray-Field Imaging of a Chiral Artificial Spin Ice during Magnetization Reversal.

Artificial spin ices are a class of metamaterials consisting of magnetostatically coupled nanomagnets. Their interactions give rise to emergent behavior, which has the potential to be harnessed for the creation of functional materials. Consequently, the ability to map the stray field of such systems can be decisive for gaining an understanding of their properties. Here, we use a scanning nanometer-scale superconducting quantum interference device (SQUID) to image the magnetic stray field distribution of an artificial spin ice system exhibiting structural chirality as a function of applied magnetic fields at 4.2 K. The images reveal that the magnetostatic interaction gives rise to a measurable bending of the magnetization at the edges of the nanomagnets. Micromagnetic simulations predict that, owing to the structural chirality of the system, this edge bending is asymmetric in the presence of an external field and gives rise to a preferred direction for the reversal of the magnetization. This effect is not captured by models assuming a uniform magnetization. Our technique thus provides a promising means for understanding the collective response of artificial spin ices and their interactions.

Vectorial scanning force microscopy using a nanowire sensor.

Self-assembled nanowire (NW) crystals can be grown into nearly defect-free nanomechanical resonators with exceptional properties, including small motional mass, high resonant frequency and low dissipation. Furthermore, by virtue of slight asymmetries in geometry, a NW's flexural modes are split into doublets oscillating along orthogonal axes. These characteristics make bottom-up grown NWs extremely sensitive vectorial force sensors. Here, taking advantage of its adaptability as a scanning probe, we use a single NW to image a sample surface. By monitoring the frequency shift and direction of oscillation of both modes as we scan above the surface, we construct a map of all spatial tip-sample force derivatives in the plane. Finally, we use the NW to image electric force fields distinguishing between forces arising from the NW charge and polarizability. This universally applicable technique enables a form of atomic force microscopy particularly suited to mapping the size and direction of weak tip-sample forces.

A scanning superconducting quantum interference device with single electron spin sensitivity.

Superconducting quantum interference devices (SQUIDs) can be used to detect weak magnetic fields and have traditionally been the most sensitive magnetometers available. However, because of their relatively large effective size (on the order of 1 µm), the devices have so far been unable to achieve the level of sensitivity required to detect the field generated by the spin magnetic moment (µB) of a single electron. Here we show that nanoscale SQUIDs with diameters as small as 46 nm can be fabricated on the apex of a sharp tip. The nano-SQUIDs have an extremely low flux noise of 50 nΦ0 Hz(-1/2) and a spin sensitivity of down to 0.38 µB Hz(-1/2), which is almost two orders of magnitude better than previous devices. They can also operate over a wide range of magnetic fields, providing a sensitivity of 0.6 µB Hz(-1/2) at 1 T. The unique geometry of our nano-SQUIDs makes them well suited to scanning probe microscopy, and we use the devices to image vortices in a type II superconductor, spaced 120 nm apart, and to record magnetic fields due to alternating currents down to 50 nT.