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Bioorg Med Chem Lett ; 25(22): 5232-6, 2015 Nov 15.
Artículo en Inglés | MEDLINE | ID: mdl-26459214

RESUMEN

Glutamate carboxypeptidase II (GCPII) is a zinc metalloprotease on the surface of astrocytes which cleaves N-acetylaspartylglutamate to release N-acetylaspartate and glutamate. GCPII inhibitors can decrease glutamate concentration and play a protective role against apoptosis or degradation of brain neurons. Herein, we report the synthesis and structural analysis of novel carborane-based GCPII inhibitors. We determined the X-ray crystal structure of GCPII in complex with a carborane-containing inhibitor at 1.79Å resolution. The X-ray analysis revealed that the bulky closo-carborane cluster is located in the spacious entrance funnel region of GCPII, indicating that the carborane cluster can be further structurally modified to identify promising lead structures of novel GCPII inhibitors.


Asunto(s)
Compuestos de Boro/síntesis química , Inhibidores Enzimáticos/síntesis química , Inhibidores Enzimáticos/farmacología , Glutamato Carboxipeptidasa II/antagonistas & inhibidores , Urea/análogos & derivados , Compuestos de Boro/química , Compuestos de Boro/farmacología , Cristalografía por Rayos X , Inhibidores Enzimáticos/química , Glutamato Carboxipeptidasa II/ultraestructura , Humanos , Urea/síntesis química , Urea/química , Urea/farmacología
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