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Synthesis of 5α-androstane-3α,17ß-diol 17-O-glucuronide histaminyl conjugate for immunoassays.
Vins, Petr; Cerný, Ivan; Miksátková, Petra; Drasar, Pavel.
Afiliación
  • Vins P; Department of Chemistry of Natural Products, University of Chemistry and Technology, Technická 5, CZ 166 28 Praha 6, Czech Republic.
  • Cerný I; Department of Chemistry of Natural Products, University of Chemistry and Technology, Technická 5, CZ 166 28 Praha 6, Czech Republic.
  • Miksátková P; Department of Chemistry of Natural Products, University of Chemistry and Technology, Technická 5, CZ 166 28 Praha 6, Czech Republic.
  • Drasar P; Department of Chemistry of Natural Products, University of Chemistry and Technology, Technická 5, CZ 166 28 Praha 6, Czech Republic. Electronic address: Pavel.Drasar@vscht.cz.
Steroids ; 109: 56-9, 2016 May.
Article en En | MEDLINE | ID: mdl-26898541
ABSTRACT
Simple method of preparation of 5α-androstane-3α,17ß-diol 17-O-glucuronide N-histaminyl amide was developed for the construction of immunoanalytical kit. Improved method of glucuronide derivative synthesis was used, followed by hydroxybenzotriazole-dicyclohexylcarbodiimide coupling with histamine.
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Texto completo: 1 Bases de datos: MEDLINE Asunto principal: Inmunoensayo / Histamina / Androstano-3,17-diol Idioma: En Revista: Steroids Año: 2016 Tipo del documento: Article País de afiliación: República Checa
Texto completo
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Texto completo: 1 Bases de datos: MEDLINE Asunto principal: Inmunoensayo / Histamina / Androstano-3,17-diol Idioma: En Revista: Steroids Año: 2016 Tipo del documento: Article País de afiliación: República Checa