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Cu(II)/Proline-Catalyzed Reductive Coupling of Sulfuryl Chloride and P(O)-H for P-S-C Bond Formation.
Zhang, Xinghua; Wang, Dungai; An, Duo; Han, Boshi; Song, Xiang; Li, Liang; Zhang, Gaoqi; Wang, Lixian.
Afiliación
  • Zhang X; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • Wang D; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • An D; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • Han B; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • Song X; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • Li L; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • Zhang G; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
  • Wang L; School of Chemical and Environmental Engineering, Shanghai Institute of Technology , 100 Hai-Quan Road, Shanghai 201418, China.
J Org Chem ; 83(3): 1532-1537, 2018 02 02.
Article en En | MEDLINE | ID: mdl-29313344
ABSTRACT
A considerably improved method for the Cu-catalyzed coupling of sulfuryl chloride with P(O)-H was described. Using commercially available l-proline as the ligand decreased the precatalyst loading, broadened the substrate scope and greatly promoted the efficiency of the coupling reaction. Moreover, gram-scale preparation, easy-to handle and recyclable catalyst featured this transformation.
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Texto completo: 1 Bases de datos: MEDLINE Idioma: En Revista: J Org Chem Año: 2018 Tipo del documento: Article País de afiliación: China
Texto completo
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Texto completo: 1 Bases de datos: MEDLINE Idioma: En Revista: J Org Chem Año: 2018 Tipo del documento: Article País de afiliación: China