Fiber optic sensor for nondestructive detection of microbial growth on a silk surface.

To nondestructively detect the mold growth process on silk, a coaxial concave reflection conical fiber optic sensor was developed using conical quartz fibers, fiber connectors, fiber couplers, and a plastic fixator. We established a theoretical model of this sensor and studied the influence of its structural parameters on its sensitivity, characterized the morphology of Aspergillus niger, and detected its growth process on a silk surface. A linear relationship between the sensor's output signal and the mold height was found. The sensor sensitivity, maximum detection error, and low limit of detection were 2.4 E-5 AU/µm, 7.83%, and 10 µm, respectively.

Interfacial thermal conductance between atomically thin boron nitride and graphene.

Atomically thin hexagonal boron nitride (BN) is a promising dielectric substrate for graphene and other two-dimensional (2D) materials for performance enhancement and heat dissipation. However, the interfacial heat conductance between atomically thin BN and graphene has not been experimentally studied yet. Here, we report that the interfacial thermal conductance between high-quality graphene and trilayer BN is 9.64 ± 2.12 MW m-2 K-1 in the temperature range of 293-393 K, indicating that the interfacial thermal conductance is depressed when the heterostructure thickness is smaller than the wavelength of the low-frequency phonons, e.g. ZA in BN.

Reflective fiber-optic sensor for on-line nondestructive monitoring of Aspergillus on the surface of cultural paper relics.

A reflective fiber-optic sensor was created to realize on-line nondestructive monitoring of the growth process of Aspergillus on the surface of cultural paper relics. The sensor consisted of one tapered input and six output optical fibers. The operating principle of the device was established. The sensitivity of the sensor was checked. Sensors were used to monitor the growth of Aspergillus niger, Aspergillus flavus, and Aspergillus tamarrii on the papers. The morphology of Aspergillus was characterized. The sensor reveals a linear relationship between the output signal of the sensor and the thickness of Aspergillus biofilm with a detection limit of 10 µm.

Gas Purge Microextraction Coupled with Stable Isotope Labeling-Liquid Chromatography/Mass Spectrometry for the Analysis of Bromophenols in Aquatic Products.

A green, sensitive, and accurate method was developed for the extraction and determination of bromophenols (BPs) from aquatic products by using organic solvent-free gas purge microsyringe extraction (GP-MSE) technique in combination with stable isotope labeling (SIL) strategy. BPs were extracted by NaHCO3 buffer solution, with recoveries varying from 92.0% to 98.5%. The extracted solution was analyzed by SIL strategy, during which analytes and standards were labeled by 10-methyl-acridone-2-sulfonyl chloride (d0-MASC) and its deuterated counterpart d3-MASC, respectively. The labeling reaction was finished within 10 min with good stability. The liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) sensitivity of BPs was greatly enhanced due to the mass-enhancing property of MASC, while the matrix effect was effectively minimized by the SIL strategy. The limits of detection (LODs) were in the range of 0.10-0.30 µg/kg, while the limits of quantitations (LOQs) were in the range of 0.32-1.0 µg/kg. The proposed method also showed great potential in the qualitative analysis of other bromophenols in the absence of standard.