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A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources.
Steinke, I; Walther, M; Lehmkühler, F; Wochner, P; Valerio, J; Mager, R; Schroer, M A; Lee, S; Roseker, W; Jain, A; Sikorski, M; Song, S; Hartmann, R; Huth, M; Strüder, L; Sprung, M; Robert, A; Fuoss, P H; Stephenson, G B; Grübel, G.
Afiliação
  • Steinke I; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Walther M; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Lehmkühler F; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Wochner P; Max Plank-Institut für Festkörperforschung, Heisenbergstr. 1, 70569 Stuttgart, Germany.
  • Valerio J; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Mager R; Max Plank-Institut für Intelligente Systeme, Heisenbergstr. 3, 70569 Stuttgart, Germany.
  • Schroer MA; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Lee S; Frontier in Extreme Physics, Korea Research Institute of Standards and Science (KRISS), Daejeon 305-600, South Korea.
  • Roseker W; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Jain A; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Sikorski M; LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025, USA.
  • Song S; LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025, USA.
  • Hartmann R; PNSensor GmbH, Sckellstraße 3, 81667 München, Germany.
  • Huth M; PNSensor GmbH, Sckellstraße 3, 81667 München, Germany.
  • Strüder L; PNSensor GmbH, Sckellstraße 3, 81667 München, Germany.
  • Sprung M; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
  • Robert A; LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025, USA.
  • Fuoss PH; Argonne National Laboratory, Argonne, Illinois 60439, USA.
  • Stephenson GB; Argonne National Laboratory, Argonne, Illinois 60439, USA.
  • Grübel G; Deutsches Elektronen-Synchrotron (DESY), Notkestr. 85, 22607 Hamburg, Germany.
Rev Sci Instrum ; 87(6): 063905, 2016 Jun.
Article em En | MEDLINE | ID: mdl-27370468
In this paper we describe a setup for x-ray scattering experiments on complex fluids using a liquid jet. The setup supports Small and Wide Angle X-ray Scattering (SAXS/WAXS) geometries. The jet is formed by a gas-dynamic virtual nozzle (GDVN) allowing for diameters ranging between 1 µm and 20 µm at a jet length of several hundred µm. To control jet properties such as jet length, diameter, or flow rate, the instrument is equipped with several diagnostic tools. Three microscopes are installed to quantify jet dimensions and stability in situ. The setup has been used at several beamlines performing both SAXS and WAXS experiments. As a typical example we show an experiment on a colloidal dispersion in a liquid jet at the X-ray Correlation Spectroscopy instrument at the Linac Coherent Light Source free-electron laser.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Revista: Rev Sci Instrum Ano de publicação: 2016 Tipo de documento: Article País de afiliação: Alemanha
Texto completo
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XML
PubMed Links
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Revista: Rev Sci Instrum Ano de publicação: 2016 Tipo de documento: Article País de afiliação: Alemanha