Improving the chromatographic selectivity of ß-lactam residue analysis in milk using phenyl-column chemistry prior to detection by tandem mass spectrometry.

Di Rocco, Melissa; Moloney, Mary; Haren, Deirdre; Gutierrez, Montserrat; Earley, Seán; Berendsen, Bjorn; Furey, Ambrose; Danaher, Martin

Di Rocco, Melissa; Moloney, Mary; Haren, Deirdre; Gutierrez, Montserrat; Earley, Seán; Berendsen, Bjorn; Furey, Ambrose; Danaher, Martin.

Afiliação

Di Rocco M; Food Safety Department, Teagasc Food Research Centre, Ashtown, Dublin 15, Ireland. melissa.dirocco@teagasc.ie.
Moloney M; Mass Spectrometry Research Group, Department of Physical Sciences, Cork Institute of Technology, Bishopstown, Cork, T12 P928, Ireland. melissa.dirocco@teagasc.ie.
Haren D; Food Safety Department, Teagasc Food Research Centre, Ashtown, Dublin 15, Ireland.
Gutierrez M; Food Safety Department, Teagasc Food Research Centre, Ashtown, Dublin 15, Ireland.
Earley S; Veterinary Public Health Regulatory Laboratory, Department of Agriculture, Food and the Marine, Backweston, Celbridge, W23 X3PH, Ireland.
Berendsen B; Veterinary Public Health Regulatory Laboratory, Department of Agriculture, Food and the Marine, Backweston, Celbridge, W23 X3PH, Ireland.
Furey A; Wageningen Food Safety Research, Department of Veterinary Drug Residues, Wageningen University & Research, 6708, Wageningen, The Netherlands.
Danaher M; Mass Spectrometry Research Group, Department of Physical Sciences, Cork Institute of Technology, Bishopstown, Cork, T12 P928, Ireland.

Anal Bioanal Chem ; 412(18): 4461-4475, 2020 Jul.

Article em En | MEDLINE | ID: mdl-32447520

Assuntos

Antibacterianos/análise; Resíduos de Drogas/análise; Leite/química; Espectrometria de Massas em Tandem/métodos; beta-Lactamas/análise; Animais; Bovinos; Cromatografia Líquida de Alta Pressão/métodos; Cromatografia Líquida/métodos; Análise de Alimentos/métodos; Contaminação de Alimentos/análise; Limite de Detecção; Reprodutibilidade dos Testes; Extração em Fase Sólida/métodos

Palavras-chave

Bovine milk; Chromatographic selectivity; Phenyl-hexyl; UHPLC-MS/MS; ß-Lactam antibiotics

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Texto completo: 1 Base de dados: MEDLINE Assunto principal: Resíduos de Drogas / Leite / Beta-Lactamas / Espectrometria de Massas em Tandem / Antibacterianos Tipo de estudo: Diagnostic_studies / Prognostic_studies Limite: Animals Idioma: En Revista: Anal Bioanal Chem Ano de publicação: 2020 Tipo de documento: Article País de afiliação: Irlanda

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