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Photopromoted Free Radical Silylation of 2-Aryl-2H-indazoles with Silanes.
Tian, Yunfei; Zheng, Luping; Guo, Dongyu; Miao, Yuyan; Li, Lijun; Fu, Weijun; Li, Zejiang.
Afiliação
  • Tian Y; College of Chemistry and Chemical Engineering, Key Laboratory of Fuction-Oriented Porous Materials of Henan Province, Luoyang Normal University, Luoyang, Henan 471934, P. R. China.
  • Zheng L; College of Chemistry and Chemical Engineering, Key Laboratory of Fuction-Oriented Porous Materials of Henan Province, Luoyang Normal University, Luoyang, Henan 471934, P. R. China.
  • Guo D; Key Laboratory of Medicinal Chemistry and Molecular Diagnosis of the Ministry of Education, State Key Laboratory of New Pharmaceutical Preparations and Excipients, College of Chemistry & Materials Science, and Key Laboratory of Chemical Biology of Hebei Province, Hebei University, Baoding, Hebei
  • Miao Y; College of Chemistry and Chemical Engineering, Key Laboratory of Fuction-Oriented Porous Materials of Henan Province, Luoyang Normal University, Luoyang, Henan 471934, P. R. China.
  • Li L; Key Laboratory of Medicinal Chemistry and Molecular Diagnosis of the Ministry of Education, State Key Laboratory of New Pharmaceutical Preparations and Excipients, College of Chemistry & Materials Science, and Key Laboratory of Chemical Biology of Hebei Province, Hebei University, Baoding, Hebei
  • Fu W; College of Chemistry and Chemical Engineering, Key Laboratory of Fuction-Oriented Porous Materials of Henan Province, Luoyang Normal University, Luoyang, Henan 471934, P. R. China.
  • Li Z; Key Laboratory of Medicinal Chemistry and Molecular Diagnosis of the Ministry of Education, State Key Laboratory of New Pharmaceutical Preparations and Excipients, College of Chemistry & Materials Science, and Key Laboratory of Chemical Biology of Hebei Province, Hebei University, Baoding, Hebei
J Org Chem ; 88(23): 16671-16678, 2023 Dec 01.
Article em En | MEDLINE | ID: mdl-37968942
ABSTRACT
Photoinduced silylation of silanes with 2-aryl-2H-indazoles was developed under mild conditions, which could efficiently result in diverse 3-silylated 2H-indazoles with good substrate scopes. A series of scaled-up to gram level and radical capture operations were performed in this system. Meanwhile, a bioactive molecule was tolerated well under typical conditions.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Revista: J Org Chem Ano de publicação: 2023 Tipo de documento: Article
Texto completo
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PubMed Links
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Revista: J Org Chem Ano de publicação: 2023 Tipo de documento: Article