45.5-tesla direct-current magnetic field generated with a high-temperature superconducting magnet.

Strong magnetic fields are required in many fields, such as medicine (magnetic resonance imaging), pharmacy (nuclear magnetic resonance), particle accelerators (such as the Large Hadron Collider) and fusion devices (for example, the International Thermonuclear Experimental Reactor, ITER), as well as for other diverse scientific and industrial uses. For almost two decades, 45 tesla has been the highest achievable direct-current (d.c.) magnetic field; however, such a field requires the use of a 31-megawatt, 33.6-tesla resistive magnet inside 11.4-tesla low-temperature superconductor coils1, and such high-power resistive magnets are available in only a few facilities worldwide2. By contrast, superconducting magnets are widespread owing to their low power requirements. Here we report a high-temperature superconductor coil that generates a magnetic field of 14.4 tesla inside a 31.1-tesla resistive background magnet to obtain a d.c. magnetic field of 45.5 tesla-the highest field achieved so far, to our knowledge. The magnet uses a conductor tape coated with REBCO (REBa2Cu3Ox, where RE = Y, Gd) on a 30-micrometre-thick substrate3, making the coil highly compact and capable of operating at the very high winding current density of 1,260 amperes per square millimetre. Operation at such a current density is possible only because the magnet is wound without insulation4, which allows rapid and safe quenching from the superconducting to the normal state5-10. The 45.5-tesla test magnet validates predictions11 for high-field copper oxide superconductor magnets by achieving a field twice as high as those generated by low-temperature superconducting magnets.

Quench Analyses of the MIT 1.3-GHz LTS/HTS NMR Magnet.

The MIT 1.3-GHz LTS/HTS NMR magnet is currently under development. The unique features of this magnet include a 3-nested formation for an 800-MHz REBCO insert (H800) and the no-insulation (NI) winding technique for H800 coils. Because when it is driven to the normal state, an NI REBCO magnet will respond electromagnetically, thermally, and mechanically that may result in permanent magnet damage, analysis of a quenching magnet is a key aspect of HTS magnet protection. We have developed a partial element equivalent circuit method coupled to a thermal and stress finite element method to analyze electromagnetic and mechanical responses of a nested-coil REBCO magnet each a stack of NI pancake coils. Using this method, quench simulations of the MIT 1.3-GHz LTS (L500)/HTS (H800) NMR magnet (1.3G), we have evaluated currents, strains, and torques of H800 Coil 1 to Coil 3 and L500, and center fields of 1.3G, L500, and H800. Our analyses show H800 is vulnerable to mechanical damage.

Assembly and Test of a 3-Nested-Coil 800-MHz REBCO Insert (H800) for the MIT 1.3 GHz LTS/HTS NMR Magnet.

We present assembly and test results of a 3-nested-coil 800-MHz (18.8 T) REBCO insert (H800) for the MIT 1.3 GHz LTS/HTS NMR magnet currently under completion. Each of the three H800 coils is a stack of no-insulation (NI) REBCO double-pancake coils (DPs). The innermost 8.7-T Coil 1 (26 DPs) was completed by mid-2016; the middle 5.6-T Coil 2 (32 DPs) was complet-ed in mid-2017; while the outermost 4.5-T Coil 3 (38 DPs) was completed in early 2018. Coils 1, 2 & 3 were assembled together in early 2018 as a 3-nested-coil, the H800, and tested, first in liquid nitrogen to a power supply current of 20 A, followed by testing in liquid helium to a power supply current of 251.3 A, the H800's design operating current. After roughly five minutes settling time at 251.3 A, the H800 quenched. In this paper we examine probable sources of quench initiation and simulate ensuing quench behavior. Remedial efforts to minimize the tendency towards quenching in the H800 are presented and discussed.

MIT 1.3-GHz LTS/HTS NMR Magnet: Post Quench Analysis and New 800-MHz Insert Design.

We present post-quench analyses of the MIT 800-MHz REBCO insert magnet (H800), unexpectedly quenched during operation in March 2018, and design study of a new 800-MHz HTS insert (H800N). The as-wound H800 was supposed to contribute 18.7 T and, with an LTS background magnet (L500), produce 30.5 T corresponding to a proton resonance frequency of 1.3 GHz. The H800 was operated at 4.2 K in liquid helium and, about 5 minutes after the power supply reached a target operating current of 251.3 A, it experienced a quench. Because the damage in the H800 was more widespread than it first appeared, we decided to design and build a new insert magnet, H800N. In designing H800N, we try to eliminate unanticipated flaws in our H800 design. H800N is to be more stable not to quench and more reliably survive against quench without permanent damage by: 1) adopting a single solenoid structure composed of 40 stacked double pancake coils with improved cross-over sections; 2) enhancing thermal stability; and 3) reducing excessive current margin for quench protection.

Construction and Test Results of Coils 2 and 3 of a 3-Nested-Coil 800-MHz REBCO Insert for the MIT 1.3-GHz LTS/HTS NMR Magnet.

We present construction and test results of Coils 2 and 3 of a 3-coil 800-MHz REBCO insert (H800) for the MIT 1.3 GHz LTS/HTS NMR magnet currently under construction. Each of three H800 coils (Coils 1-3) is a stack of no-insulation REBCO double pancakes (DPs). The innermost 8.67-T Coil 1 (26 DPs) was completed in 2016; the middle 5.64-T Coil 2 (32 DPs) has been wound, assembled, and tested; and for the outermost 4.44-T Coil 3, its 38 DPs have been wound and preliminary tests were performed to characterize each DP at 77 K. Included for Coil 2 are: 1) 77-K data of critical current, index, and turn-to-turn characteristic resistivity of each DP; 2) stacking order of the 32 DPs optimized to maximize the Coil 2 current margin and minimize its Joule dissipation in the pancake-to-pancake joints; 3) procedure to experimentally determine and apply a room-temperature preload to the DP stack; 4) 77-K and 4.2-K test results after each of 64 pancakes was over-banded with 75-µm-thick stainless steel tape for a radial thickness of 5 mm. Presented for each DP in Coil 3 are 77-K dada of critical current, index, and turn-to-turn characteristic resistivity.

A REBCO Persistent-Current Switch, Immersed in Solid Nitrogen, Operating at Temperatures near 10 K.

We present design and test results for a thermally-activated persistent-current switch (PCS) applied to a double pancake (DP) coil (151 mm ID, 172 mm OD), wound, using the no-insulation (NI) technique, from a 120-m long, 76-µm thick, 6-mm wide REBCO tape. For the experiments reported in this paper, the NI DP assembly was immersed in a volume of solid nitrogen (SN2), cooled to a base temperature of 10 K by conduction to a two-stage cryocooler, and energized at up to 630 A. The DP assembly operated in quasi-persistent mode, with the conductor tails soldered together to form a close-out joint with resistance below 6 nΩ. The measurements confirm PCS activation at heating powers below our 1-W design target, and a field decay time constant in excess of 900 h (i.e 0.1% h-1 field decay rate), limited by the finite resistance of the close-out joint.

Construction and Test Results of Coil 2 of a Three-Coil 800-MHz REBCO Insert for the 1.3-GHz High-Resolution NMR Magnet.

This paper focuses on the construction and test results of Coil 2 that is part of a trio of nested coils composing the REBCO 800 MHz insert. Upon its completion, the REBCO 800 MHz insert will be placed in the bore of a 500 MHz low temperature superconducting (LTS) NMR magnet (L500) to form the MIT 1.3 GHz high-resolution NMR magnet. Coil 2 is a stack of 32 double pancake (DP) coils wound with 6-mm wide REBCO tape using the no-insulation (NI) technique. Each pancake is wound on a stainless steel inner supporting ring to prevent the collapsing of its crossover due to the external pressure exerted by the winding pack. Coil 2 will be constructed in the following sequence: 1) after winding each DP will be individually tested in a bath of liquid nitrogen at atmospheric pressure to determine its current carrying capabilities; 2) DPs will be then assembled as a stack with interconnecting joints, and 3) as in Coil 1, each pancake will be overbanded with a stainless steel tape, this time to a thickness of 5 mm, thickness determined by a stress analysis previously performed. Finally the fully assembled Coil 2 will be tested in liquid nitrogen at 77 K and then in liquid helium at 4.2 K. We present here details of the stress analysis leading to the sizing of the DP inner supporting stainless steel ring and of the overbanding thickness required. Test results include coil index, critical current, charging time constant.

A REBCO Persistent-Current Switch (PCS): Test Results and Switch Heater Performance.

In this paper, we report preliminary results of our on-going effort to develop a superconducting persistent-current switch (PCS) for REBCO pancake coils that will be operated in liquid helium. In the first part of this paper, we briefly describe experimental results of our PCS operated in the temperature range 77-57 K, i.e., liquid-and solid-nitrogen environments. The rest we devote to a new PCS heater design in which we target a heating power of < 1 W in liquid helium.

Test of an 8.66-T REBCO Insert Coil with Overbanding Radial Build for a 1.3-GHz LTS/HTS NMR Magnet.

A 1.3-GHz/54-mm LTS/HTS NMR magnet, assembled with a 3-coil (Coils 1-3) 800-MHz HTS insert in a 500-MHz LTS NMR magnet, is under construction. The innermost HTS insert Coil 1 has a stack of 26 no-insulation (NI) double pancake (DP) coils wound of 6-mm wide and 75-µm thick REBCO tapes. In order to keep the hoop strains on REBCO tape < 0.6% at an operating current Iop of 250 A and in a field of 30.5 T, we overbanded each pancake in Coil 1 with a 6-mm wide, 76-µm thick 304 stainless steel strip: 7-mm thick radial build for the central 18 pancakes, while 6-mm thick for the outer 2×17 pancakes. In this paper, Coil 1 was successfully tested at 77K and 4.2 K. In the 77-K test, the measured critical current was 35.7 A, determined by an E-field criterion of 0.1 µV/cm. The center field magnet constant decreased from 34.2 mT/A to 29.3 mT/A, when Iop increased from 5 A to 40 A. The field distribution at different Iop along the z-axis was measured. The residual field distributions discharged from 10 A and 20 A were recorded. In the 4.2-K test, Coil 1 successfully generated a central field of 8.78 T at 255 A. The magnet constant is 34.4 mT/A, which is same as our designed value. The field homogeneity at the coil center within a ±15-mm region is around 1700 ppm. This large error field must be reduced before field shimming is applied.

An 800-MHz all-REBCO Insert for the 1.3-GHz LTS/HTS NMR Magnet Program-A Progress Report.

A critical component of the 1.3-GHz nuclear magnetic resonance magnet (1.3 G) program, currently ongoing at the Francis Bitter Magnet Laboratory, Plasma Science and Fusion Center, Massachusetts Institute of Technology, and now approaching its final stage, is the all high-temperature superconductor 800-MHz insert (H800). The insert consists of three nested double-pancake (DP) coils fabricated with 6-mm-wide REBCO conductor. Coil 1, the innermost coil of H800, has already been fabricated and tested at 77 and 4.2 K. In addition, one third of the DPs for Coil 2 have been wound and each DP individually fully tested. Work described here includes details of Coil 1 fabrication: DP winding, DP testing, assembling, joint performance, overbanding, and coil testing; winding details of DPs for Coil 2 and their testing are also included.

A Theoretical Design Approach for Passive Shimming of a Magic-Angle-Spinning NMR Magnet.

This paper presents a passive shimming design approach for a magic-angle-spinning (MAS) NMR magnet. In order to achieve a 1.5-T magic-angle field in NMR samples, we created two independent orthogonal magnetic vector fields by two separate coils: the dipole and solenoid. These two coils create a combined 1.5-T magnetic field vector directed at the magic angle (54.74° from the spinning axis). Additionally, the stringent magnetic field homogeneity requirement of the MAS magnet is the same as that of a solenoidal NMR magnet. The challenge for the magic-angle passive shimming design is to correct both the dipole and solenoid magnetic field spherical harmonics with one set of iron pieces, the so-called ferromagnetic shimming. Furthermore, the magnetization of the iron pieces is produced by both the dipole and solenoid coils. In our design approach, a matrix of 2 mm by 5 mm iron pieces with different thicknesses was attached to a thin-walled tube, 90-mm diameter and 40-mm high. Two sets of spherical harmonic coefficients were calculated for both the dipole and solenoid coil windings. By using the multiple-objective linear programming optimization technique and coordinate transformations, we have designed a passive shimming set that can theoretically reduce 22 lower-order spherical harmonics and improve the homogeneity of our MAS NMR magnet.

A Parametric Study on Overband Radial Build for a REBCO 800-MHz Insert of a 1.3-GHz LTS/HTS NMR Magnet.

A high-resolution 1.3-GHz/54-mm low-temperature superconducting/high-temperature superconducting (HTS) nuclear magnetic resonance magnet (1.3 G) is currently being built at Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology. One of its key components is an 800-MHz HTS insert (H800) comprising three nested coils. Each coil is a stack of double-pancake coils wound with 6-mm-wide 75-µm-thick REBCO tape. For this H800 generating its self-field of 18.6 T and being exposed to a total field as high as 30.5 T, overbanding each pancake coil is necessary to keep the conductor strain at < 0.6%. Although electromagnetic and mechanical details of the H800 had been considered during its design stage, a parametric study on the overband radial build considering winding tension effect should further confirm the results of our previous analysis. Thus, in this paper, based on Maxwell's equations and the equilibrium equations for mechanical deformation, we examine stress levels that the H800 experiences as H800 undergoes winding-energizing sequences during operation at 1.3 GHz. We also discuss the effects of overband radial build and winding tension on conductor stress in each coil. Finally, based on this analysis, we may further optimize the stainless-steel overbanding and winding tension on each H800 coil.

High-Resolution Magnetic Field Mapping System With an NMR Probe.

This paper presents a high-resolution magnetic field mapping system in development that is capable of collecting spatial magnetic field data for NMR magnets. An NMR probe was designed and built with a resonant frequency of 5.73 MHz. The measured Q-factor of the NMR probe is ~191 with a half-power bandwidth in the range of 5.72-5.75 MHz. An RF continuous-wave technique with magnetic field modulation was utilized to detect the power dispersion of water molecules. The zero-crossing frequency of the NMR dispersion signal corresponds to the magnetic field at the center of the water sample. An embedded system was developed to sweep the frequency and record the reflected RF power simultaneously. A numerically controlled digital oscillator is able to provide a precise frequency step as small as 0.02 Hz, which is equivalent to 4.7 e-7 mT for hydrogen atoms. An RF preamplifier was built to supply up to 4 W of RF power to a bidirectional coupler. The coupler supplies RF power to the NMR probe and channels reflect the RF power back to the detection circuit, which detects the reflected RF power from the NMR probe during the frequency sweep. The homogeneity of an NMR magnet can be determined by magnetic field data.

Tape-to-Tape Joint Resistances of a Magnet Assembled From (RE)BCO Double-Pancake Coils.

We present the results of tape-to-tape joint resistances in a 1.3-GHz/54-mm nuclear-magnetic-resonance magnet comprising a 500-MHz low-temperature-superconducting magnet and an 800-MHz high-temperature-superconducting insert (H800), which is currently in the fabrication stage at the Massachusetts Institute of Technology Francis Bitter Magnet Laboratory. The H800, which is a three-coil assembly of double-pancake coils and wound with a 6-mm-wide (RE)BCO tape (rare earth element), requires a total of 94 tape-to-tape joints. Specific results obtained are: 1) an extrapolation technique to predict the resistances of the tape-to-tape curved bridge joints from those of the curved lap joint samples with the same 6-mm-wide tape batch and joint area; 2) increased resistance owing to a small gap (< 0.4 mm) in the outer radii of the two adjacent pancakes, which is mainly caused by the variation in the (RE)BCO tape thickness (on the order of several micrometers); 3) a method to minimize solder-heating influences on the pancake current-carrying capacity; 4) the dependence of resistance on solder materials; and 5) the experience with the 25 joints on Coil 1, which is the first of three coils for our H800 insert (H800 Coil 1).

Strain in YBCO Double-Pancake Coil With Stainless Steel Overband Under External Magnetic Field.

This paper deals with the mechanical strain issue in a high-temperature superconducting (HTS) insert for a GHz-class (> 23.5 T) LTS/HTS NMR magnet. We present results, experimental and analytical, of hoop strains in a double-pancake (DP) test coil, wound with 6-mm wide YBCO coated conductor (CC) and equipped with strain gauges at their innermost and outermost turns. To keep the YBCO CC to within a 95% Ic retention, the conductor tensile strain must be limited to 0.6%. To satisfy this strain limit in our test DP coil, we wrapped 0.08-mm thick, 6-mm wide stainless steel strip over its outermost turn of an 4.8-mm overband radial build deemed sufficient by our stress analysis based on force equilibrium and generalized Hooke's law with plane stress approximation. A control test DP coil, actually the same test DP coil, without overbanding, was run under the same experimental condition. In each case the test DP coil was energized up to 350 A at 4.2 K in a background field of 4 T. We report the experiment and analysis, with discussion on the merit of overbanding as a means to limit hoop strain in high-field HTS inserts.

Construction and Persistent-Mode Operation of MgB2 Coils in the Range 10-15 K for a 0.5-T/240-mm Cold Bore MRI Magnet.

This paper presents construction and persistent-mode operation results of MgB2 coils for a 0.5-T/240-mm cold bore MRI magnet, wind-and-react with monofilament MgB2 wire at the MIT Francis Bitter Magnet Laboratory. The magnet, of respective inner and outer diameters of 276 and 290 mm and a total height of 460 mm, has center field of 0.5 T and current density of 11 kA/cm2. To limit the continuous length of Hyper Tech supplied MgB2 monofilament wire to ≤300 m, the magnet was divided into eight series-connected coils, each equipped with a persistent current switch and a superconducting joint. We have manufactured three coil modules. Before being tested as an assembly, each coil was tested individually to ensure its capacity to carry 100-A superconducting current in the range of 10-15 K. The three coils were then assembled, connected in series, and operated as a 3-coil assembly in persistent mode at nearly 100 A in the range of 10-15 K. We present results that include: 1) construction details; 2) component performances; and 3) a 3-coil assembly performance.

A 1.5-T Magic-Angle Spinning NMR Magnet: 4.2-K Performance and Field Mapping Test Results.

We present results of full-current testing at 4.2 K of a z-axis 0.866-T solenoid and an x-axis 1.225-T dipole coil that comprise a 1.5-T/75-mm room temperature bore magic-angle-spinning nuclear magnetic resonance magnet developed at the MIT Francis Bitter Magnet Laboratory. Also included in the paper are results of the magnet performance when the magnet assembly is immersed, to enhance its thermal mass, in solid nitrogen, and operated in the temperature range of 4.2-4.3 K.

Operation of a 130-MHz/9-mm Compact HTS Annulus Magnet With a Micro-NMR Probe.

In this paper, we report final operation results of our compact annulus NMR magnet, named YP2800, with a homemade micro-NMR probe in a bath of liquid helium at 4.2 K. YP2800 comprises of a stack of 2800 YBCO "plate annuli," 0.08 mm thick, either 46 mm or 40 mm square, each having a 26-mm hole machined at the center. By the field-cooling technique, YP2800 was energized at 130 MHz (3.05 T); an overall peak-to-peak homogeneity of 487 ppm within |z| < 5 mm was measured at a moment when a field drift of 11 ppm/h was reached in three days after field cooling. Due to a small (9.2 mm) bore size, no commercial probes could fit into the bore; an 8.5-mm micro-NMR probe was designed and constructed. Following a general description of YP2800 and design construction details of the micro probe, this paper presents NMR signals captured by the probe for a dimethyl sulfoxide sample of ϕ 4.4 and 5 mm long at a base frequency of 130 MHz with a half-peak width of 60 kHz; the corresponding frequency impurity of 461 ppm is chiefly due to a spatial field error, i.e., 487 ppm in the target space.

Designs and Tests of Shaking Coils to Reduce Screening Currents Induced in HTS Insert Coils for NMR Magnet.

Two types of shaking coils are focused on reducing screening currents induced in solenoid coils wound with high-temperature superconducting (HTS) tapes. One is a pair of copper shaking coils coaxially located inside and outside the HTS coil to apply an ac magnetic field in the axial direction. The other is an HTS shaking coil with notch located only outside the HTS coil to minimize the radial components of local ac fields applied to windings of the HTS coil as small as possible. It is found that the copper shaking coils yield the allowable amount of power dissipation in liquid helium. The effectiveness of the HTS shaking coil to reduce screening-current-induced fields generated by another magnetized HTS coil is also experimentally validated in liquid nitrogen using a commercially available coated conductor with narrow width.

A High-Resolution 1.3-GHz/54-mm LTS/HTS NMR Magnet.

A high-resolution 1.3-GHz/54-mm low-temperature superconducting/high-temperature superconducting (HTS) nuclear magnetic resonance magnet (1.3 G) is currently in the final stage at the Massachusetts Institute of Technology Francis Bitter Magnet Laboratory. Its key component is a three-coil (Coils 1-3) 800-MHz HTS insert comprising 96 no-insulation (NI) double-pancake coils, each wound with a 6-mm-wide GdBCO tape. In this paper, after describing the overall 1.3-G system, we present innovative design features incorporated in 1.3 G: 1) an NI winding technique applied to Coils 1-3 and its adverse effect in the form of charging time delay; 2) persistent-mode HTS shims; 3) a "shaking" magnet; and 4) preliminary results of Coil 1 operated at 4.2 K.