Your browser doesn't support javascript.
loading
Mostrar: 20 | 50 | 100
Resultados 1 - 4 de 4
Filtrar
Mais filtros

Base de dados
Tipo de documento
Assunto da revista
País de afiliação
Intervalo de ano de publicação
1.
Microsc Microanal ; 20(6): 1708-14, 2014 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-25387606

RESUMO

The impact of lubricants on pole-tip recession and surface morphology of hard disk drive heads in the precision lapping process was investigated with atomic force microscopy, scanning electron microscopy, and auger electron spectroscopy. In particular, the effects of deionized water, hydrocarbon oil, ethanediol, isopropanol, and ethanol lubricants were evaluated. The results reveal that proper selection of lubricant is critical for achieving optimal performance in the lapping process. A mixture of 68% hydrocarbon oil, 30% isopropanol, and 2% octadecenoic acid was found to yield the most favorable results, displaying a writer shield recession, first shield of reader recession, and surface roughness of 0.423, 0.581, and 0.242 nm, respectively.

2.
ScientificWorldJournal ; 2014: 326427, 2014.
Artigo em Inglês | MEDLINE | ID: mdl-25045730

RESUMO

Nanodiamonds, which are the main components of slurry in the precision lapping process of magnetic heads, play an important role in surface quality. This paper studies the mechanistic features of nanodiamond embedment into a Sn plate in the lapping process. This is the first study to develop mathematical models for nanodiamond embedment. Such models can predict the optimum parameters for particle embedment. From the modeling calculations, the embedded pressure satisfies p 0 = (3/2) · (W/πa (2)) and the indentation depth satisfies δ = k1√P/HV. Calculation results reveal that the largest embedded pressure is 731.48 GPa and the critical indentation depth δ is 7 nm. Atomic force microscopy (AFM), scanning electron microscopy (SEM), and Auger electron spectroscopy (AES) were used to carry out surface quality detection and analysis of the disk head. Both the formation of black spots on the surface and the removal rate have an important correlation with the size of nanodiamonds. The results demonstrate that an improved removal rate (21 nm · min(-1)) can be obtained with 100 nm diamonds embedded in the plate.


Assuntos
Magnetismo , Nanodiamantes/química , Nanodiamantes/ultraestrutura , Microscopia de Força Atômica , Microscopia Eletrônica de Varredura , Nanoestruturas/química , Nanoestruturas/ultraestrutura
3.
Materials (Basel) ; 16(23)2023 Nov 23.
Artigo em Inglês | MEDLINE | ID: mdl-38068034

RESUMO

An investigation on the fracture of a mold, comparing it with a normal part using specific techniques, such as EDX, SEM, and AES, is presented in this study. The EDX analysis revealed that the composition of the normal part was consistent with that of low-carbon steel, mainly comprising Fe and C. In contrast, the fractured part exhibited cracks due to nonconforming nonmetallic inclusions and reticular carbides, with fractures resulting from microporosity agglomeration and cleavage fracture. The SEM and AES analyses further presented the causes of mold fracture, highlighting the mechanism by which the dimples on the specimen edge contributed to the fracture. The EDX analysis confirmed that the mold experienced thermal brittleness during use. To enhance mold durability and extend its lifespan, a pulse electrodeposition method was employed to create a NiCo alloy coating as a replacement for the Cr layer on the metal surface. The coating exhibited a smooth and scratch-free surface. The prepared NiCo special coating significantly increased the mold yield strength by approximately 313.8%, facilitated a 13% increase in plastic deformation, and reduced the fracture strain by 25%, effectively preventing mold fracture and improving its service life.

4.
Nanomaterials (Basel) ; 12(16)2022 Aug 12.
Artigo em Inglês | MEDLINE | ID: mdl-36014628

RESUMO

This work concentrated on the improvement of the surface roughness of a magnetic head, through the use of an ultrafine nanodiamond slurry, and a novel floating grinding process, which optimize different experimental factors required for the fine grinding of a magnetic head. The preparation of the grinding plate was confirmed by the observation of the surface change, depth detection, and flatness after ultrafine nanodiamonds were embedded into it by a Keyence high-power microscope at a 20 K magnification. The flatness was measured by a TOTO instrument. The optimum conditions were found to be a pit ratio reach of 30:70 and a plate flatness (average) of 1.8 µm. The rotation speed and vibration frequency were 0.3 and 10 rpm, respectively, for the grinding process. The morphology, size, and elemental composition of blackspots were investigated by SEM, AES, AFM, and transmission electron microscopy (TEM) analysis, which showed that the diameter of the diamonds in the slurry was important for grinding surface improvement. A novel method was proposed in this study to fine grind a magnetic head using a small-sized diamond slurry (100 nm) in conjunction with a novel float lapping method. Comparison experiments were performed under both normal conditions and improved conditions. The results show that by using the novel float lapping method with a small-sized diamond slurry, the minimum roughness was obtained. The finest roughness obtained for the slider surface reached 0.165 nm without blackspots or scratches.

SELEÇÃO DE REFERÊNCIAS
Detalhe da pesquisa