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1.
J Dent ; 125: 104271, 2022 10.
Artigo em Inglês | MEDLINE | ID: mdl-36041673

RESUMO

OBJECTIVES: The aim of this retrieval study was to analyze the fracture features and identify the fracture origin of zirconia-based single crowns that failed during clinical use. METHODS: Thirty-five fractured single crowns were retrieved from dental practices (bi-layered, n = 15; monolithic, n = 20). These were analyzed according to fractographic procedures by optical and scanning electron microscopy to identify fracture patterns and fracture origins. The fracture origins were closely examined. The crown margin thickness and axial wall height were measured. RESULTS: Three types of failure modes were observed: total fractures, marginal semilunar fractures, and incisal chippings. Most of the crowns (23) had fracture origins at the crown margin and seven of them had defects in the fracture origin area. The exact fracture origin was not possible to identify due to missing parts in four crowns. The crown wall thickness was 20% thinner and wall height 30% shorter in the fracture origin area compared to the opposite side. CONCLUSIONS: The findings in this study show that fractography can reveal fracture origins and fracture modes of both monolithic and bi-layered dental zirconia. The findings indicate that the crown margin on the shortest axial wall is the most common fracture origin site. CLINICAL SIGNIFICANCE: Crown design factors such as material thickness at the margin, axial wall height and preparation type affects the risk of fracture. It is important to ensure that the crown margins are even and flawless.


Assuntos
Porcelana Dentária , Falha de Restauração Dentária , Cerâmica , Coroas , Planejamento de Prótese Dentária , Análise do Estresse Dentário , Teste de Materiais , Zircônio
2.
Biomater Investig Dent ; 8(1): 160-169, 2021.
Artigo em Inglês | MEDLINE | ID: mdl-34693294

RESUMO

AIM: The aim of this study was to evaluate the effect of cement on the fracture load of monolithic zirconia crowns with different yttria content (3 and 5 mol%). METHODS: A total of 62 monolithic zirconia crowns, 40 3Y-zirconia crowns (Prettau® Zirconia, Zirkonzahn) and 22 5Y-zirconia crowns (Prettau® 4 Anterior®, Zirkonzahn) were produced to a shallow chamfer molar preparation. The 3Y-crowns were divided into four groups and attached to composite abutment duplicates (SDR® flow+, Dentsply DeTrey GmbH) using the following four cementation techniques; (1) Self-adhesive resin-based cement, (2) Pre-treatment with air-abrasion and self-adhesive resin-based cement, (3) Zinc phosphate cement, (4) Glass-ionomer cement. The 5Y-crowns were divided into two groups and attached to the duplicates with; (1) Self-adhesive resin-based cement, or (2) Air-abrasion pre-treatment and self-adhesive resin-based cement. All crowns were loaded axially (0.5 mm/min) on the occlusal surface until fracture occurred. RESULTS: Among the 3Y-zirconia groups, the zinc phosphate cement group fractured at lower loads compared to the resin-based cement groups, with and without air-abrasion, (p < .012). Among the 5Y-groups the air-abraded crowns fractured at statistically significant lower loads compared to the untreated crowns (p < .028). Load at fracture values were significantly different between the two zirconia materials (p < .001), with fracture loads ranging from 3873 to 7500 N in the 3Y-groups, and 2100 to 4948 N in the 5Y-groups. CONCLUSIONS: Resin-based cementation increased the fracture load compared to non-adhesive cementation. The 3Y-crowns fractured at almost twice the loads of the 5Y-crowns. Pre-treatment with air abrasion reduced the strength of the 5Y-crowns only, showing the importance of differentiating the treatment of the two materials.

3.
Dent Mater ; 37(9): 1425-1436, 2021 09.
Artigo em Inglês | MEDLINE | ID: mdl-34330519

RESUMO

OBJECTVE: Several pre-cementation procedures have been advocated to enhance adhesion between zirconia and resin-based cement. There is, however, limited documentation on how these pre-treatments affect the strength of zirconia crowns as most tests are performed on discs or bars. The aim was to assess the effect of pre-cementation procedures on fracture mode, fracture strength and cement retention on zirconia. METHODS: Two dental zirconia materials with different yttria content were assessed (<4 and>5 mol%). Both discs (n = 45) and crown-shaped specimens (n = 30) of the two materials were pretreated with either air-abrasion or hot-etching with KHF2 and compared with untreated controls with regards to surface roughness, crystallography, wettability, cement adhesion and fracture strength. RESULTS AND SIGNIFICANCE: Air-abrasion improves adhesion and strength of zirconia with moderate yttria content (<4 mol%). Acid etching with heated KHF2 showed the best effect on strength and cement retention on zirconia with higher yttria content (>5 mol%). Application of KHF2 was, however, complicated on crown-shaped specimens. Pre-treatment and cementation protocols should be optimized for different dental zirconias to improve both strength and retention.


Assuntos
Cimentação , Colagem Dentária , Cerâmica , Corrosão Dentária , Análise do Estresse Dentário , Teste de Materiais , Cimentos de Resina , Propriedades de Superfície , Ítrio , Zircônio
4.
Dent Mater ; 37(8): e427-e434, 2021 08.
Artigo em Inglês | MEDLINE | ID: mdl-33910755

RESUMO

OBJECTIVE: Monolithic zirconia crowns have become a viable alternative to conventional layered restorations. The aim of this study was to evaluate whether the taper, and thus wall thickness, of the abutment or pre-defined cement space affect the fracture resistance or fracture mode of monolithic zirconia crowns. METHODS: A model tooth was prepared with a taper of 15° and a shallow circumferential chamfer preparation (0.5 mm). Two additional models were made based on the master model with a taper of 10° and 30° using computer-aided design software. Twenty monolithic 3rd generation translucent zirconia crowns were produced for each model with pre-defined cement space set to either 30 µm or 60 µm (n = 60). The estimated cement thickness was assessed by the replica method. The cemented crowns were loaded centrally in the occlusal fossa at 0.5 mm/min until fracture. Fractographic analyses were performed on all fractured crowns. RESULTS: The load at fracture was statistically significant different between the groups (p < 0.05). The crowns with 30° taper fractured at lower loads than those with 10° and 15° taper, regardless of the cement space (p < 0.05). The fracture origin for 47/60 crowns (78%) was in the cervical area, close to the top of the curvature in the mesial or distal crown margin. The remaining fractures started at the internal surface of the occlusal area and propagated cervically. SIGNIFICANCE: The fracture resistance of the monolithic zirconia crowns was lower for crowns with very large taper compared to 10 and 15° taper even though the crown walls were thicker.


Assuntos
Porcelana Dentária , Planejamento de Prótese Dentária , Desenho Assistido por Computador , Coroas , Falha de Restauração Dentária , Análise do Estresse Dentário , Teste de Materiais , Zircônio
5.
Eur J Oral Sci ; 128(6): 526-534, 2020 12.
Artigo em Inglês | MEDLINE | ID: mdl-33058363

RESUMO

Higher yttria content enhances the translucency and appearance of dental zirconia materials. Alterations in material composition also affect mechanical properties. The aim of this study was to compare the fracture load after artificial short-term aging of monolithic, full-contour zirconia crowns with different amounts of yttria-stabilization. Sixty crowns (thirty super high translucent crowns (5Y-Z) and thirty high translucent crowns (3Y-Z)) were produced to fit a model of a premolar with a shallow chamfer preparation. The crowns were cemented with self-adhesive resin cement on composite abutments. For each zirconia type, three groups of crowns (n = 10) were allocated to: (i) cyclic loading (200 N, 1 Hz, 30,000 cycles), (ii) hydrothermal aging (3 × 20 min, 134°C 3.2 bar), or (iii) no treatment (control). Surviving crowns from the aging process were quasistatically loaded until fracture. The 3Y-Z crowns had statistically significantly higher fracture values (3,449 N) than the 5Y-Z crowns (1,938 N). The aging procedures did not affect load at fracture. Fractographic analysis showed that fractures started either at the crown margin or at the occlusal intaglio area. Higher yttria content leads to a reduction in material strength and damage tolerance, and this should be reflected in recommendations for clinical use.


Assuntos
Cerâmica , Zircônio , Coroas , Porcelana Dentária , Planejamento de Prótese Dentária , Falha de Restauração Dentária , Análise do Estresse Dentário , Teste de Materiais
6.
Biomater Investig Dent ; 7(1): 126-133, 2020 Aug 25.
Artigo em Inglês | MEDLINE | ID: mdl-32939457

RESUMO

PURPOSE: High-translucent dental zirconia has been introduced as a suitable material for anterior monolithic restorations. The material composition differs from traditional 3Y-TZP both with regard to yttria content and grain size. Little is known regarding how these alterations affect other properties than translucency and flexural strength. The aim of this study was to evaluate the crack propagation resistance and hardness of dental zirconias with different yttria content and different manufacturing methods. MATERIALS AND METHODS: Measurement of hardness (HV2/5) and crack propagation from the indents (damage tolerance) was performed using a hardness tester(Vicker) on a flat polished surface of five crowns from six different commercial dental zirconias; one hard-machined 3Y-TZP, three soft-machined 3-5% yttria-stabilized zirconias and two soft-machined zirconias with ≥5% yttria content. RESULTS: Damage control varied greatly among dental zirconias with different compositions and fabrication methods. The hard-machined 3Y-TZP had better crack propagation resistance than soft-machined, 3-5% yttria-stabilized zirconias. CONSLUSION: The ultra-translucent zirconias with ≥5% yttria content had the lowest crack propagation resistance. Hardness is not a suitable indicator for damage tolerance.

7.
Addit Manuf ; 362020 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-32793425

RESUMO

Additive manufacturing (AM) of ceramics, particularly of zirconia, is becoming of increasing interest due to the substantial freedom available in the design and fabrication process. However, due to the novelty of the field and the challenges associated with printing dense bulk ceramics suitable for structural applications, thorough investigations that explore the effects of printing on the mechanical performance are limited. Previous work has identified anisotropy in the mechanical properties and attributed it to the layer-by-layer deposition. However, substantiated fractographic evidence detailing the origins and effects of layer lines on the probability of failure are limited. This study investigates the mechanical properties of a dense (>99 %TD), partially stabilized zirconia fabricated by a digital light projection printing method following ASTM standards. Hardness and strength evaluations were conducted, followed by a Weibull analysis and fractography. The investigation entailed five unique build directions and a conventionally manufactured reference material that was used as a control. Although the strengths were comparable to the reference material for some orientations, fracture frequently initiated at layer lines and related defects in all orientations. The findings indicate that if the layer lines can be prevented or engineered, the strength of vat printed ceramics can be improved substantially.

8.
Dent Mater ; 36(4): 560-569, 2020 04.
Artigo em Inglês | MEDLINE | ID: mdl-32063392

RESUMO

OBJECTIVES: This study investigated the effects of tungsten-carbide grinding on the surface characteristics and mechanical strength of dental 3 mol% yttria-stabilized zirconia (3Y-TZP). METHODS: Two types of tungsten-carbide burs (TC), 6-blade (TC1) and 8-blade (TC2) were used to grind 3Y-TZP, in a dental air-turbine handpiece with water-cooling and were also subjected to air-particle abrasion (APA): TC1 + APA and TC2 + APA; and rubber polishing (RP): TC1 + RP and TC2 + RP; one group received only rubber-polishing RP. The control group received no treatment. Surface characterization was examined by surface roughness (Ra) and atomic force microscopy. Specimens were also observed with scanning electron microscopy (SEM) and X-ray-diffraction (XRD) for microstructure and crystalline phases. A piston-on-three-balls biaxial-flexural strength (BFS) test was performed with 15 samples-per-group and the broken specimen were observed under SEM to investigate the fracture origin pattern. One-way ANOVA, Kruskal-Wallis test and Weibull analysis were performed at α = 0.05. RESULTS: Groups TC1 and TC2 had the lowest mean BFS (p < 0.05) with up to 74 % reduction in strength. APA and RP both significantly increased the mean BFS after tungsten-carbide grinding but was still less than the control (p < 0.05). Compared to the control, the mean BFS was significantly reduced for all groups except for the RP group (p < 0.05). APA and rubber-polishing following TC2 grinding had significant higher mean BFS than those following TC1 grinding respectively (p < 0.05). SEM revealed distinct micro-cracks after tungsten-carbide grinding. SIGNIFICANCE: Tungsten-carbide burs (6- and 8-blade) are not recommended for zirconia grinding due to the significant reduction of biaxial-flexural strength and observed micro-structural surface and subsurface damage.


Assuntos
Polimento Dentário , Zircônio , Cerâmica , Materiais Dentários , Teste de Materiais , Microscopia Eletrônica de Varredura , Propriedades de Superfície , Compostos de Tungstênio , Ítrio
9.
J Endod ; 45(2): 189-193, 2019 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-30711176

RESUMO

INTRODUCTION: Although the strength and toughness of dentin decrease with age, no study has explored if restorative treatments are a contributing factor. METHODS: Multiple extracted teeth were obtained from randomly selected donors and categorized according to donor age and prior root canal treatment. The microstructure and chemical composition of radicular dentin were evaluated using scanning electron microscopy and Raman spectroscopy, respectively, and the strength was evaluated in 4-point flexure to failure. Data were compared using the Student t test. RESULTS: Dentin from the root canal-restored teeth exhibited significantly lower strength (P < .05) than tissue from age- and donor-matched unrestored tooth pairs. Although there was no significant difference in the mineral-to-collagen ratio between the 2 groups, dentin obtained from the root canal-treated teeth exhibited more extensive collagen cross-linking and lower tubule occlusion ratios than the unrestored tooth pairs. CONCLUSIONS: There is a decrease in the strength of radicular dentin with aging, but prior root canal treatment increases the extent of degradation.


Assuntos
Envelhecimento , Análise do Estresse Dentário , Dentina , Resistência à Flexão , Tratamento do Canal Radicular , Resistência ao Cisalhamento , Fraturas dos Dentes/etiologia , Idoso , Colágeno/análise , Dentina/química , Dentina/ultraestrutura , Humanos , Microscopia Eletrônica de Varredura , Pessoa de Meia-Idade , Minerais/análise , Tratamento do Canal Radicular/efeitos adversos , Análise Espectral Raman
10.
Eur J Oral Sci ; 127(1): 89-96, 2019 02.
Artigo em Inglês | MEDLINE | ID: mdl-30467907

RESUMO

Zirconia-based restorations are showing an increase as the clinicians' preferred choice at posterior sites because of the strength and esthetic properties of such restorations. However, all-ceramic restorations fracture at higher rates than do metal-based restorations. Margin design is one of several factors that can affect the fracture strength of all-ceramic restorations. The aim of this study was to assess the effect of preparation and crown margin design on fracture resistance. Four groups of bilayer zirconia crowns (with 10 crowns in each group) were produced by hard- or soft-machining technique, with the following four different margin designs: chamfer preparation (control); slice preparation; slice preparation with an additional cervical collar of 0.7 mm thickness; and reduced occlusal thickness (to 0.4 mm) on slice preparation with an additional cervical collar of 0.7 mm thickness. Additionally, 10 hard-machined crowns with slice preparation were veneered and glazed with feldspathic porcelain. In total, 90 crowns were loaded centrally in the occlusal fossa until fracture. The load at fracture was higher than clinically relevant mastication loads for all preparation and margin designs. The crowns on a chamfer preparation fractured at higher loads compared with crowns on a slice preparation. An additional cervical collar increased load at fracture for hard-machined crowns.


Assuntos
Coroas , Planejamento de Prótese Dentária , Falha de Restauração Dentária , Zircônio , Desenho Assistido por Computador , Análise do Estresse Dentário , Humanos , Teste de Materiais
11.
J Prosthet Dent ; 120(1): 156.e1-156.e7, 2018 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-29705672

RESUMO

STATEMENT OF PROBLEM: New additive manufacturing techniques for nonprecious alloys have made the fabrication of metal-ceramic fixed partial dentures (FPDs) less expensive and less time-consuming. However, whether the mechanical properties produced by these techniques are comparable is unclear. PURPOSE: The purpose of this in vitro study was to evaluate the mechanical properties of cobalt-chromium frameworks for FPDs fabricated by 3 different techniques. MATERIAL AND METHODS: Thirty frameworks for 3-unit FPDs were fabricated by traditional casting, computer-aided design and computer-aided manufacturing (CAD-CAM) milling, and selective laser melting (SLM), with n=10 in each group. The frameworks were weighed, and distal and mesial connector areas measured. The frameworks were cemented and loaded centrally (0.5 mm/s) until deformation above 1 mm occurred. Stiffness was measured as the slope of the axis between 500 and 2000 N. Microhardness was measured on sectioned specimens by Vickers indentation. The microstructure was also analyzed by scanning electron microscopy. One-way ANOVA with Tukey post hoc analysis was used to compare the groups (α=.05). RESULTS: The framework design differed among the groups, making a comparison of strength impossible. The milled frameworks appeared bulky, while the cast and SLM frameworks were more slender. Statistically significant differences were found in microhardness, stiffness, wall thickness, weight, and connector size (P<.05), and a significant correlation was found between hardness and stiffness (-0.4, P<.005). CONCLUSIONS: Fabrication method affects the design, stiffness, microhardness, and microstructure of cobalt-chromium FPD frameworks. The SLM frameworks were stiffer and harder than the cast and milled specimens.


Assuntos
Ligas de Cromo/química , Desenho Assistido por Computador , Planejamento de Dentadura , Prótese Parcial Fixa , Ligas Metalo-Cerâmicas/química , Cobalto/química , Análise do Estresse Dentário , Dureza , Técnicas In Vitro , Teste de Materiais , Fenômenos Mecânicos , Microscopia Eletrônica de Varredura , Maleabilidade
12.
Dent Mater ; 34(6): 922-931, 2018 Jun.
Artigo em Inglês | MEDLINE | ID: mdl-29673708

RESUMO

BACKGROUND: Promising results of initial clinical trials with yttria-stabilized zirconia have led to more extensive use of zirconia in dental implant superstructures. The applications have extended to abutments and complex individually designed crown-abutment one-piece structures. Little is known about their clinical success and the primary cause of failures. PURPOSE: The aim of this study was to identify the cause of fracture of retrieved implant-retained one-piece prostheses that failed during clinical use. METHODS: Nine fractured restorations were analyzed with fractographic methods and their fracture origins were identified. RESULTS: All but two of the fractures originated in an area of tight contact between the implant or titanium screw and the abutment base. Results of the evaluation showed that zirconia-based implant restorations with very thin walls in the region connecting the prosthesis to the implant are vulnerable to damage from the screw retaining process and fracture from non-axial loads. Two restorations failed due to veneer fractures. SIGNIFICANCE: The findings suggest that large crowns on narrow implants or implants with internal fixation should preferably not be made with zirconia abutments, or that a new design approach should be considered.


Assuntos
Coroas , Implantes Dentários , Prótese Dentária Fixada por Implante , Falha de Restauração Dentária , Ítrio/química , Zircônio/química , Materiais Dentários/química , Análise do Estresse Dentário , Teste de Materiais , Noruega
13.
J Prosthet Dent ; 120(3): 327-330, 2018 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-29627215

RESUMO

Two zirconia-based 4-unit restorations intended for the same patient fractured during the veneering process even though the prolonged cooling protocol recommended by the manufacturers was used. Fractographic analyses revealed that both restorations fractured as a result of thermal shock, but at different times during production. Further investigation is necessary to optimize the firing protocols for large zirconia-based restorations and avoid fracture due to thermal shock.


Assuntos
Prótese Dentária Fixada por Implante/efeitos adversos , Falha de Restauração Dentária , Facetas Dentárias/efeitos adversos , Temperatura Alta/efeitos adversos , Zircônio/efeitos adversos , Adulto , Implantes Dentários/efeitos adversos , Humanos , Masculino , Zircônio/uso terapêutico
14.
J Dent ; 72: 14-20, 2018 05.
Artigo em Inglês | MEDLINE | ID: mdl-29452242

RESUMO

OBJECTIVES: The aim of this study was to assess the clinical outcomes and patient satisfaction with monolithic zirconia crowns in patients with severe tooth wear (≥1/3 of the tooth crown) in the aesthetic zone. METHODS: The historical prospective study sample consisted of 13 patients previously treated with a total of 84 monolithic zirconia crowns. The patients had been treated in a private clinic in Bergen, Norway, in the period 2012 to 2014. All patients were men, aged 35-67 years (mean age 56.3 years) and had been in need of prosthetic rehabilitation because of severe tooth wear in the aesthetic zone. Technical complications as well as biologic findings were registered when the crowns had been in function one to three years (mean 20 months). The patients completed a self-administered questionnaire regarding satisfaction with aesthetic and function. RESULTS: No biological complications were registered in 79 of the crowns (94%), and technical complications were registered in only two patients. All patients were satisfied with the aesthetic and function of the monolithic zirconia crowns and would choose the same treatment modality if they were to be treated again. CONCLUSIONS: Within the limitations of this study, we conclude that the rate of clinical complications was low and that the patients were satisfied with the aesthetic as well as the function of the monolithic zirconia crowns. CLINICAL SIGNIFICANCE: Monolithic zirconia crowns may provide a valid treatment modality in the aesthetic zone in patients with severe tooth wear.


Assuntos
Bruxismo/complicações , Coroas/efeitos adversos , Materiais Dentários/efeitos adversos , Desgaste de Restauração Dentária , Estética Dentária/psicologia , Desgaste dos Dentes/etiologia , Zircônio/efeitos adversos , Adulto , Idoso , Desenho Assistido por Computador , Planejamento de Prótese Dentária , Falha de Restauração Dentária , Humanos , Masculino , Pessoa de Meia-Idade , Noruega , Satisfação do Paciente , Estudos Prospectivos , Propriedades de Superfície , Inquéritos e Questionários , Desgaste dos Dentes/diagnóstico por imagem , Desgaste dos Dentes/reabilitação , Resultado do Tratamento
15.
Dent Mater ; 33(9): 1012-1020, 2017 09.
Artigo em Inglês | MEDLINE | ID: mdl-28662859

RESUMO

OBJECTIVE: Dental all-ceramic restorations of zirconia, with and without an aesthetic veneering layer, have become a viable alternative to conventional metal-ceramic restorations. The aim of this study was to evaluate whether factors of the production methods or the material compositions affect load at fracture, fracture modes, internal fit or crown margins of monolithic zirconia crowns. METHODS: Sixty crowns made from six different commercially available dental zirconias were produced to a model tooth with a shallow circumferential chamfer preparation. Internal fit was assessed by the replica method. The crown margin quality was assessed by light microscopy on an ordinal scale. The cemented crowns were loaded centrally in the occlusal fossa with a horizontal steel cylinder with a diameter of 13mm at 0.5mm/min until fracture. Fractographic analysis was performed on the fractured crowns. RESULTS: There were statistically significant differences among the groups regarding crown margins, internal fit and load at fracture (p<0.05, Kruskall Wallis). Fracture analyses revealed that all fractures started cervically and propagated to the occlusal surface similar to clinically observed fractures. There was statistically significant correlation between margin quality and load at fracture (Spearman's rank correlation, p<0,05). SIGNIFICANCE: Production method and material composition of monolithic zirconia crowns affect internal fit, crown margin quality and the load at fracture. The hard-machined Y-TZP zirconia crowns had the best margin quality and the highest load at fracture. Reduction of margin flaws will improve fracture strength of monolithic zirconia crowns and thereby increase clinical success.


Assuntos
Coroas , Porcelana Dentária , Zircônio , Materiais Dentários , Planejamento de Prótese Dentária , Falha de Restauração Dentária , Análise do Estresse Dentário , Humanos , Teste de Materiais
16.
J Endod ; 43(9): 1494-1498, 2017 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-28712639

RESUMO

INTRODUCTION: The incidence of vertical root fracture in endodontically treated teeth increases with patient age. This study evaluated the microstructure, chemical composition, and mechanical properties of radicular dentin as a function of aging. METHODS: Single-rooted teeth were obtained from adult donors ranging from age 15 to older than 80 years. Beams were extracted from the middle third of the root and subjected to 4-point flexure to failure to evaluate strength of dentin in terms of donor age. Based on the strength distribution, the fatigue strength of root tissue from young (≤30 years) and old (≥55 years) donor teeth was evaluated via cyclic flexure loading. The microstructure and chemical composition of radicular dentin from the 2 groups were evaluated as a function of distance from the root apex using microscopy and Raman spectroscopy, respectively. RESULTS: The strength decreased with age by approximately 25 MPa per decade, which resulted in a significant difference (P ≤ .0001) between the young (199 ± 36 MPa) and old (122 ± 11 MPa) groups. There was also a significant difference (P ≤ .0001) in fatigue strength between the young and old age groups. Both the mineral-to-collagen ratio and degree of cross-linking increased with age, with the largest changes identified in the apical and middle thirds, respectively. CONCLUSIONS: There is a reduction in the damage tolerance of radicular dentin with increasing age. This degradation appears to result from changes in the microstructure, corresponding chemical composition, and increase in collagen cross-linking with age, and is most severe near the root apex.


Assuntos
Dentina/lesões , Fraturas dos Dentes/etiologia , Raiz Dentária/lesões , Adolescente , Adulto , Fatores Etários , Idoso , Idoso de 80 Anos ou mais , Humanos , Técnicas In Vitro , Pessoa de Meia-Idade , Adulto Jovem
17.
Acta Biomater Odontol Scand ; 3(1): 47-52, 2017 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-28642931

RESUMO

Purpose: Some patients experience adverse reactions to poly(methyl methacrylate)-based (PMMA) dentures. Polyamide (PA) as an alternative to PMMA has, however, not been well documented with regard to water sorption and water solubility. The aim of this in vitro study was to measure water sorption and water solubility of two PA materials compared with PMMA, and to evaluate the major components released from the PA materials and the effect on hardness of the materials. Methods: Ten discs (40.0 mm diameter, 2.0 mm thick) of each material (PA: Valplast and Breflex; PMMA: SR Ivocap HIP) were prepared according to manufacturers' recommendations. The specimens were tested for water sorption and water solubility, according to a modification of ISO 20795-1:2008. Released substances were analysed by gas chromatography/mass spectrometry (GC/MS). Results: There were statistically significant differences among the materials regarding water sorption, water solubility and time to water saturation. Breflex had the highest water sorption (30.4 µg/mm3), followed by PMMA-material (25.8 µg/mm3) and Valplast (13.6 µg/mm3). Both PA materials had statistically significant lower water solubility than the PMMA. Both PA had a net increase in weight. Analysis by GC/MS identified release of the compound 12-aminododecanolactam from the material Valplast. No release was found from the Breflex material. Conclusions: The PA denture materials show differences in water sorption and solubility, but within the limits of the standard requirements. The PA showed a net increase in weight after long-term water sorption. The clinical implications of the findings are not elucidated.

18.
J Prosthet Dent ; 115(5): 630-6, 2016 May.
Artigo em Inglês | MEDLINE | ID: mdl-26775244

RESUMO

STATEMENT OF PROBLEM: The effect of anatomic contour design in all or parts of zirconia crowns is uncertain regarding clinical reliability and survival rates. PURPOSE: The purpose of this in vitro study was to compare the load at fracture of monolithic, anatomic contour zirconia crowns with bilayered crowns with and without a cervical zirconia collar. MATERIAL AND METHODS: Thirty zirconia crowns were fabricated for a shallow chamfer molar preparation, 10 with a normal core-veneer design, 10 with a core-veneer design with an additional cervical collar of zirconia, and 10 with a monolithic, anatomic contour design. Veneering ceramic was applied to the first 20 specimens to create an anatomic form. All crowns were cemented to epoxy abutments and loaded until complete fracture with a clinically relevant test method. The fracture modes and load at fracture were recorded. RESULTS: Statistically significant differences were found in the load at fracture and fracture modes among the test groups (P<.001). All fractures except one initiated in the crown margin, mostly in the proximal region. The mean load at fracture was 4091 N for the normal core-veneer design, 4712 N for the collar design, and 6517 N for the monolithic, anatomic contour design. CONCLUSIONS: Monolithic, anatomical contour design gave higher loads at fracture than traditional core-veneer design. Crowns with a cervical zirconia collar had higher load at fracture than the core-veneer design, but lower than the monolithic crowns.


Assuntos
Coroas/efeitos adversos , Falha de Restauração Dentária , Zircônio , Cerâmica , Planejamento de Prótese Dentária , Análise do Estresse Dentário , Humanos , Suporte de Carga
19.
J Mech Behav Biomed Mater ; 53: 93-103, 2016 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-26318570

RESUMO

OBJECTIVES: The causes of in vivo fractures of all-ceramic dental crowns are not yet fully understood. The fracture origins often occur in the cervical margin in the approximal area, but the reason for this is unclear. The aim of this study was to evaluate the fracture origin of 22 of clinically-failed alumina crowns. METHODS: The fracture surfaces of alumina crowns fractured in vivo were inspected by optical microscopy to evaluate the fracture patterns and identify the cause of fracture. Fracture maps were constructed as needed to interpret the patterns of breakage and to back track to a fracture origin area. A scanning electron microscope (SEM) was used to characterize the fracture origins of the 22 cases where the origin site was available. RESULTS: The most common fracture origins were marginal defects either in the alumina core or in the veneer. The defects included thin, chipped, cracked or uneven crown margins and excess veneer on the inside of the crown. Multiple flaws were present along the margins in most specimens, but fracture origins were usually located in the region of the shortest axial wall. A few crowns had pores, contamination, or incomplete sintering that acted as fracture origins. SIGNIFICANCE: Production method, handling, design and material insufficiencies influence the fracture of dental ceramic crowns. Machining defects and other margin flaws seem to be the most detrimental factors for alumina crowns. Feather-edge or sharp margins should be avoided. Smooth and moderately thick crown margins would probably dramatically improve the durability.


Assuntos
Óxido de Alumínio , Coroas , Análise de Falha de Equipamento , Fenômenos Mecânicos
20.
Int J Prosthodont ; 28(4): 357-9, 2015.
Artigo em Inglês | MEDLINE | ID: mdl-26218016

RESUMO

PURPOSE: Despite the high fracture strength of modern dental core ceramics, fractures are a common cause of clinical failures. The aim of this study was to use a clinically relevant test method to evaluate the effect of the curvature of the cervical crown margins on load at fracture. MATERIALS AND METHODS: Thirty zirconia crowns and 30 glass-ceramic crowns were produced for three premolar preparations with variation in the approximal crown margin curvature: low curvature (r=12 mm), moderate curvature (r=2.5 mm), and high curvature (r=1.5). The crowns were loaded until fracture with a method that mimics clinical fracture modes. RESULTS: Statistically significant differences were found among both crown margin curvature and material groups (P<.001). Most fractures originated from pre-existing flaws. CONCLUSION: A moderate to low curvature of the crown margins increases crown strength compared with a high curvature.


Assuntos
Cerâmica , Coroas , Falha de Restauração Dentária , Humanos
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