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Biomed Chromatogr ; 38(11): e5989, 2024 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-39171645

RESUMO

Epilepsy (EP) is one of the most common neurological diseases in the world. Anemarrhena asphodeloides Bunge. (AA), as a typical heat-cleaning medicine, has been proven to possess the antiepileptic effect in clinical and experimental studies. Anemarrhena asphodeloides steroidal saponins (AAS) are main components. However, the therapeutic effects and underlying mechanisms of AAS against EP are not been fully elucidated. In this study, 63 steroidal saponins were discovered in AAS by UPLC-Q-TOF/MS analysis. Pharmacological and behavioral analysis demonstrated that AAS could significantly lower the Racine classification and reduce the frequency of generalized spike rhythm the rate of tetanic seizures in kainic acid-induced epileptic rats. Hematoxylin and eosin and Nissl staining-indicated AAS could significantly improve hippocampal injury and neuron loss in epileptic rats. TMT proteomic analysis discovered 26 different expressed proteins (DEPs), which were identified as the rescue proteins. After bioinformatic analysis, Heat Shock Protein 90 Alpha Family Class B Member 1 (Hsp90ab1) and Tyrosine 3-Monooxygenase (Ywhab) were screened as key DEPs and verified by western blotting. AAS could significantly inhibited the up-regulation of Hsp90ab1 and Ywhab in EP rats; these two proteins might be the key targets of AAS in treating EP.


Assuntos
Anemarrhena , Anticonvulsivantes , Epilepsia , Ácido Caínico , Proteômica , Ratos Sprague-Dawley , Saponinas , Espectrometria de Massas em Tandem , Animais , Saponinas/farmacologia , Saponinas/química , Ratos , Epilepsia/induzido quimicamente , Epilepsia/tratamento farmacológico , Epilepsia/metabolismo , Masculino , Proteômica/métodos , Ácido Caínico/toxicidade , Anemarrhena/química , Espectrometria de Massas em Tandem/métodos , Anticonvulsivantes/farmacologia , Anticonvulsivantes/química , Modelos Animais de Doenças , Extratos Vegetais/farmacologia , Extratos Vegetais/química , Proteoma/análise , Proteoma/efeitos dos fármacos , Cromatografia Líquida de Alta Pressão/métodos
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